Miniature cylindrical metal powder sintered wick heat pipe （sintered heat pipe） is an ideal component with super-high thermal efficiency for high heat flux electronics cooling. The sintering process for sintered wic...Miniature cylindrical metal powder sintered wick heat pipe （sintered heat pipe） is an ideal component with super-high thermal efficiency for high heat flux electronics cooling. The sintering process for sintered wick is important for its quality. The sintering process was optimally designed based on the equation of the heat transfer limit of sintered heat pipe. Four-step sintering process was proposed to fabricate sintered wick. The sintering parameters including sintering temperature, sintering time, sintering atmosphere and sintering position were discussed. The experimental results showed that the proper sintering temperature was 950 ℃ for Cu powder of 159μm and 900 ℃ for Cu powders of 81 and 38 μm, respectively, while the wick thickness was 0.45 mm and sintering time was 3 h. The optimized sintering time was 3 h for 0.45 and 0.6 mm wick thickness and 1 h for 0.75 mm wick thickness, respectively, when copper powder diameter was 159μm and sintering temperature was 950 ℃. Redox reduction reaction between H2 and CuO during sintering could produce segmentation cracks in Cu powders as a second structure. Sintering at vertical position can effectively avoid the generation of gap between wick and the inner wall of pipe.展开更多
Water invasion is a common phenomenon in gas reservoirs with active edge-and-bottom aquifers.Due to high reservoir heterogeneity and production parameters,carbonate gas reservoirs feature exploitation obstacles and lo...Water invasion is a common phenomenon in gas reservoirs with active edge-and-bottom aquifers.Due to high reservoir heterogeneity and production parameters,carbonate gas reservoirs feature exploitation obstacles and low recovery factors.In this study,combined core displacement and nuclear magnetic resonance(NMR)experiments explored the reservoir gas−water two-phase flow and remaining microscopic gas distribution during water invasion and gas injection.Consequently,for fracture core,the water-phase relative permeability is higher and the co-seepage interval is narrower than that of three pore cores during water invasion,whereas the water-drive recovery efficiency at different invasion rates is the lowest among all cores.Gas injection is beneficial for reducing water saturation and partially restoring the gas-phase relative permeability,especially for fracture core.The remaining gas distribution and the content are related to the core properties.Compared with pore cores,the water invasion rate strongly influences the residual gas distribution in fracture core.The results enhance the understanding of the water invasion mechanism,gas injection to resume production and the remaining gas distribution,so as to improve the recovery factors of carbonate gas reservoirs.展开更多
[ Objective] The aim was to establish a method for the determination of Rhodamine B in food by HPLC-UV. [ Metkod] Rhodamine B was extracted with acetone/hexane from food samples. After concentrated and purified by alu...[ Objective] The aim was to establish a method for the determination of Rhodamine B in food by HPLC-UV. [ Metkod] Rhodamine B was extracted with acetone/hexane from food samples. After concentrated and purified by alumina cartridge, the Rhodamine B content in the food was determined by using high performance liquid chromatography with ultraviolet visible detector. [ Result] Within tile concentration range of 0.005 - 2.000 mg/kg, the peak area of Rhodamine B presented good linear relation with the concentration, and the related coefficient was 0.999 98. With high average recovery rate, the detection limit of the method was 0.005 mg/kg[ Concision] It is a fast and accurate method with high sensitivity to detect Rhodamine B in food.展开更多
Here we propose a method for determination of Avermectin residual content in milk and beef content. After extracting and processing the sample, use high performance liquid chromatography （HPLC） for determination. Mo...Here we propose a method for determination of Avermectin residual content in milk and beef content. After extracting and processing the sample, use high performance liquid chromatography （HPLC） for determination. Mobile phase is： V（Methanol）： V（Water）=90： 10; determination wavelength is 245 nm; flow rate is 0.8 mL/min. Avermectin is completely separated in 17min, linear range is 5 - 0.3 g/L, correlation coefficient is 0.9997, average recovery rates of Avermectin in milk and beef are respectively 91.20 %- 100.32 % and 89.93 %-99.15 %, the relative standard deviations are respectively less than 7% and 4%. This method is simple, sensitive and accurate, so is suitable for determination of Avermectin residues in milk and beef, and it can meet domestic and foreign testing requirements.展开更多
基金Project(50905119)supported by the National Natural Science Foundation of ChinaProject(20120171120036)supported by New Teachers'Fund for Doctor Stations,Ministry of Education,ChinaProject(S2012040007715)supported by Natural Science Foundation of Guangdong Province,China
文摘Miniature cylindrical metal powder sintered wick heat pipe （sintered heat pipe） is an ideal component with super-high thermal efficiency for high heat flux electronics cooling. The sintering process for sintered wick is important for its quality. The sintering process was optimally designed based on the equation of the heat transfer limit of sintered heat pipe. Four-step sintering process was proposed to fabricate sintered wick. The sintering parameters including sintering temperature, sintering time, sintering atmosphere and sintering position were discussed. The experimental results showed that the proper sintering temperature was 950 ℃ for Cu powder of 159μm and 900 ℃ for Cu powders of 81 and 38 μm, respectively, while the wick thickness was 0.45 mm and sintering time was 3 h. The optimized sintering time was 3 h for 0.45 and 0.6 mm wick thickness and 1 h for 0.75 mm wick thickness, respectively, when copper powder diameter was 159μm and sintering temperature was 950 ℃. Redox reduction reaction between H2 and CuO during sintering could produce segmentation cracks in Cu powders as a second structure. Sintering at vertical position can effectively avoid the generation of gap between wick and the inner wall of pipe.
基金Project(2016ZX05017)supported by the China National Science and Technology Major Project
文摘Water invasion is a common phenomenon in gas reservoirs with active edge-and-bottom aquifers.Due to high reservoir heterogeneity and production parameters,carbonate gas reservoirs feature exploitation obstacles and low recovery factors.In this study,combined core displacement and nuclear magnetic resonance(NMR)experiments explored the reservoir gas−water two-phase flow and remaining microscopic gas distribution during water invasion and gas injection.Consequently,for fracture core,the water-phase relative permeability is higher and the co-seepage interval is narrower than that of three pore cores during water invasion,whereas the water-drive recovery efficiency at different invasion rates is the lowest among all cores.Gas injection is beneficial for reducing water saturation and partially restoring the gas-phase relative permeability,especially for fracture core.The remaining gas distribution and the content are related to the core properties.Compared with pore cores,the water invasion rate strongly influences the residual gas distribution in fracture core.The results enhance the understanding of the water invasion mechanism,gas injection to resume production and the remaining gas distribution,so as to improve the recovery factors of carbonate gas reservoirs.
文摘[ Objective] The aim was to establish a method for the determination of Rhodamine B in food by HPLC-UV. [ Metkod] Rhodamine B was extracted with acetone/hexane from food samples. After concentrated and purified by alumina cartridge, the Rhodamine B content in the food was determined by using high performance liquid chromatography with ultraviolet visible detector. [ Result] Within tile concentration range of 0.005 - 2.000 mg/kg, the peak area of Rhodamine B presented good linear relation with the concentration, and the related coefficient was 0.999 98. With high average recovery rate, the detection limit of the method was 0.005 mg/kg[ Concision] It is a fast and accurate method with high sensitivity to detect Rhodamine B in food.
文摘Here we propose a method for determination of Avermectin residual content in milk and beef content. After extracting and processing the sample, use high performance liquid chromatography （HPLC） for determination. Mobile phase is： V（Methanol）： V（Water）=90： 10; determination wavelength is 245 nm; flow rate is 0.8 mL/min. Avermectin is completely separated in 17min, linear range is 5 - 0.3 g/L, correlation coefficient is 0.9997, average recovery rates of Avermectin in milk and beef are respectively 91.20 %- 100.32 % and 89.93 %-99.15 %, the relative standard deviations are respectively less than 7% and 4%. This method is simple, sensitive and accurate, so is suitable for determination of Avermectin residues in milk and beef, and it can meet domestic and foreign testing requirements.
