It was concluded that the described HPLC method could be used for the assayof salmon calcitonin in injection, as it offers qualified selectivity, accuracy and precision ofanalysis.
We measured the water content （0.01% 0.25% w/w） in crude oil emulsions using terahertz time-domain spectroscopy （THz-TDS）. To improve the precision and range of the measurements, we used 1 and 10 mm thick quartz c...We measured the water content （0.01% 0.25% w/w） in crude oil emulsions using terahertz time-domain spectroscopy （THz-TDS）. To improve the precision and range of the measurements, we used 1 and 10 mm thick quartz cells. The experiments were performed at 20 ℃ and the THz wave was transmitted vertically to the samples and detected on the other side. The experimental results suggest linear relation for the THz absorption coefficient and the water content of the crude oil emulsions in the observed range. The linear dependence facilitates high-precision measurements of the water content of crude oil. This suggests the potential of THz-TDS in determining the water concentration in crude oil and borehole fluid identification.展开更多
In order to measure the backhoe vibratory excavating resistance of a hydraulic excavator fast and precisely,the influences of vibratory excavating depth,angle,vibratory frequency,amplitude,bucket inserting velocity an...In order to measure the backhoe vibratory excavating resistance of a hydraulic excavator fast and precisely,the influences of vibratory excavating depth,angle,vibratory frequency,amplitude,bucket inserting velocity and soil type on the vibratory excavating resistance were analyzed.Simulation analysis was carded out to establish the bucket inserting velocity,amplitude and vibratory frequency considered as secondary variables and excavating resistance as primary variable.A fttzzy membership function was introduced to improve the anti-noise capacity of support vector machine,which is a soft-sensing model on the hydraulic excavator＇s backhoe vibratory excavating resistance based on fuzzy support vector machine.The simulation result reveals that its maximum relative training and testing error are nearly 0.68% and-0.47%,respectively.It is concluded that the model has quite high modeling precision and generalization capacity,and it can measure the vibratory excavating resistance accurately,reliably and fast in an indirect way.展开更多
Nuclear masses ranging from O to Ti isotopes are systematically investigated with relativistic continuum Hartree-Bogoliubov(RCHB)theory,which can provide a proper treatment of pairing correlations in the presence of t...Nuclear masses ranging from O to Ti isotopes are systematically investigated with relativistic continuum Hartree-Bogoliubov(RCHB)theory,which can provide a proper treatment of pairing correlations in the presence of the continuum.From O to Ti isotopes,there are 402 nuclei predicted to be bound by the density functional PC-PK1.For the 234 nuclei with mass measured,the root mean square(rms)deviation is 2.23 MeV.It is found that the proton drip-lines predicted with various mass models are roughly the same and basically agree with the observation.The neutron drip-lines predicted,however,are quite diferent.Due to the continuum couplings,the neutron drip-line nuclei predicted are extended further neutron-rich than other mass models.By comparison with finite-range droplet model(FRDM),the neutron drip-line nucleus predicted by RCHB theory has respectively2(O),10(Ne),10(Na),6(Mg),8(Al),6(Si),8(P),6(S),14(K),10(Ca),10(Sc),and 12(Ti)more neutrons.展开更多
The nanomechanical properties of single human immunoglobulin G and M antibodies were measured in a liquid environment using a fast force-volume technique with sub-10-nm spatial resolution. The ultrastructural details ...The nanomechanical properties of single human immunoglobulin G and M antibodies were measured in a liquid environment using a fast force-volume technique with sub-10-nm spatial resolution. The ultrastructural details of these molecules were resolved in the images. Simultaneously, important physical properties, including elasticity, adhesion, and deformation were measured. The dimensions and adsorption of the immunoglobulin M antibodies onto the substrate indicated that they are highly by a low elastic stiffness （34 ± 10 MPa） flexible. The antibodies were characterized and high deformability （1.5 ± 0.5 nm）.展开更多
Quantum chemical computations have been performed to evaluate the first and second hyperpolarizability quantities of the interference term, linear in the external static electric field, that appear in the electric fie...Quantum chemical computations have been performed to evaluate the first and second hyperpolarizability quantities of the interference term, linear in the external static electric field, that appear in the electric field-induced sum-frequency generation signal of chiral liquids. These are performed at the time-dependent Hartree-Fock level on the prototypical 1,1′-bi-2-naphtol chiral species.展开更多
文摘It was concluded that the described HPLC method could be used for the assayof salmon calcitonin in injection, as it offers qualified selectivity, accuracy and precision ofanalysis.
基金sponsored jointly by the National Key Basic Research Program of China(No.2013CB328706)the Special-funded Program on National Key Scientific Instruments and Equipment Development(No.2012YQ140005)+1 种基金the Beijing National Science Foundation(No.4122064)the Science Foundation of China University of Petroleum(Beijing)(No.QZDX-2010-01 and KYJJ2012-06-27)
文摘We measured the water content （0.01% 0.25% w/w） in crude oil emulsions using terahertz time-domain spectroscopy （THz-TDS）. To improve the precision and range of the measurements, we used 1 and 10 mm thick quartz cells. The experiments were performed at 20 ℃ and the THz wave was transmitted vertically to the samples and detected on the other side. The experimental results suggest linear relation for the THz absorption coefficient and the water content of the crude oil emulsions in the observed range. The linear dependence facilitates high-precision measurements of the water content of crude oil. This suggests the potential of THz-TDS in determining the water concentration in crude oil and borehole fluid identification.
基金Project(2003AA430200)supported by the National High Technology Research and Development Program of China
文摘In order to measure the backhoe vibratory excavating resistance of a hydraulic excavator fast and precisely,the influences of vibratory excavating depth,angle,vibratory frequency,amplitude,bucket inserting velocity and soil type on the vibratory excavating resistance were analyzed.Simulation analysis was carded out to establish the bucket inserting velocity,amplitude and vibratory frequency considered as secondary variables and excavating resistance as primary variable.A fttzzy membership function was introduced to improve the anti-noise capacity of support vector machine,which is a soft-sensing model on the hydraulic excavator＇s backhoe vibratory excavating resistance based on fuzzy support vector machine.The simulation result reveals that its maximum relative training and testing error are nearly 0.68% and-0.47%,respectively.It is concluded that the model has quite high modeling precision and generalization capacity,and it can measure the vibratory excavating resistance accurately,reliably and fast in an indirect way.
基金partially supported by the Major State Basic Research Development Program of China (Grant No. 2013CB834400)National Natural Science Foundation of China (Grant Nos. 11335002, 11345004, 11375015, 11105005, 11105006 and 11175002)+4 种基金China Postdoctoral Science Foundation (Grant Nos. 2012M520101 and 2013T60022)the Research Fund for the Doctoral Program of Higher Education (Grant No. 20110001110087)the support of the Young Core Instructor and Domestic Visitor Foundation from the Wuhan Center of Teacher Education Exchangesupported by the Rare Isotope Science Project funded by the Ministry of Science, ICT and Future Planning (MSIP) and National Research Foundation of Koreasupported by the Basic Science Research Program through the National Research Foundation of Korea (NRF) funded by the Ministry of Education, Science and Technology (Grant No. 2010-0023661)
文摘Nuclear masses ranging from O to Ti isotopes are systematically investigated with relativistic continuum Hartree-Bogoliubov(RCHB)theory,which can provide a proper treatment of pairing correlations in the presence of the continuum.From O to Ti isotopes,there are 402 nuclei predicted to be bound by the density functional PC-PK1.For the 234 nuclei with mass measured,the root mean square(rms)deviation is 2.23 MeV.It is found that the proton drip-lines predicted with various mass models are roughly the same and basically agree with the observation.The neutron drip-lines predicted,however,are quite diferent.Due to the continuum couplings,the neutron drip-line nuclei predicted are extended further neutron-rich than other mass models.By comparison with finite-range droplet model(FRDM),the neutron drip-line nucleus predicted by RCHB theory has respectively2(O),10(Ne),10(Na),6(Mg),8(Al),6(Si),8(P),6(S),14(K),10(Ca),10(Sc),and 12(Ti)more neutrons.
文摘The nanomechanical properties of single human immunoglobulin G and M antibodies were measured in a liquid environment using a fast force-volume technique with sub-10-nm spatial resolution. The ultrastructural details of these molecules were resolved in the images. Simultaneously, important physical properties, including elasticity, adhesion, and deformation were measured. The dimensions and adsorption of the immunoglobulin M antibodies onto the substrate indicated that they are highly by a low elastic stiffness （34 ± 10 MPa） flexible. The antibodies were characterized and high deformability （1.5 ± 0.5 nm）.
基金The calculations were performed on the computing facilities of the Consortium deséquipements de Calcul Intensif(CéCI),in particular those of the Plateforme Technologique de Calcul Intensif(PTCI)installed in the University of Namur,for which we gratefully acknowledge financial support of the FNRS-FRFC(2.4.617.07.F,2.5020.11)
文摘Quantum chemical computations have been performed to evaluate the first and second hyperpolarizability quantities of the interference term, linear in the external static electric field, that appear in the electric field-induced sum-frequency generation signal of chiral liquids. These are performed at the time-dependent Hartree-Fock level on the prototypical 1,1′-bi-2-naphtol chiral species.
