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一种提高气相色谱仪柱效的方法
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作者 黄菊君 翁维正 万惠霖 《福建分析测试》 CAS 1996年第4期539-540,共2页
国产气相色谱仪气体定体积进样装置一般选择旋转式六通阀,进样口按常规的联接方式,由于死体积较大,使色谱峰产生扩展,影响色谱柱的柱效及混合试样的分离度。Nogare等认为,把色谱柱外的死体积降低到最小值是获得理论柱效的一种重要的因... 国产气相色谱仪气体定体积进样装置一般选择旋转式六通阀,进样口按常规的联接方式,由于死体积较大,使色谱峰产生扩展,影响色谱柱的柱效及混合试样的分离度。Nogare等认为,把色谱柱外的死体积降低到最小值是获得理论柱效的一种重要的因素。所以。 展开更多
关键词 气相色谱仪 联接方式 柱效 分离度 死体积 六通阀 色谱柱 进样装置 进样口 混合试样
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应用发射光谱法测定地球化学样品中微量银的方法改进 被引量:1
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作者 罗艳 《中国锰业》 2017年第4期153-155,共3页
应用发射光谱法测定地球化学样品中微量银的方法,由于基体差异,存在大量样品与合成硅酸盐光谱分析标准物质之间一致性较差,低含量段准确度和精密度均不理想的问题。通过减少取样量,增加试样与缓冲剂混合比例,改进电极形状的措施,可实现... 应用发射光谱法测定地球化学样品中微量银的方法,由于基体差异,存在大量样品与合成硅酸盐光谱分析标准物质之间一致性较差,低含量段准确度和精密度均不理想的问题。通过减少取样量,增加试样与缓冲剂混合比例,改进电极形状的措施,可实现国家一级标准物质测定值与合成硅酸盐光谱分析标准物质工作曲线吻合较好。银检出限:0.010μg/g,精密度:3.9%~9.1%。 展开更多
关键词 取样量 试样与缓冲剂混合比例 电极形状 发射光谱法
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Joint member angle limits of composite beams and CFT square columns 被引量:2
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作者 LEE Seung-Jo LEE Kang-Guk 《Journal of Central South University》 SCIE EI CAS 2013年第1期199-206,共8页
This work aims to understand the relationship between the member angle limit and the energy ratio for 24 test samples of composite beams and CFT square steel tube columns. This work also compares the formula applicabi... This work aims to understand the relationship between the member angle limit and the energy ratio for 24 test samples of composite beams and CFT square steel tube columns. This work also compares the formula applicability for member angle limit with the previous test result to provide the basic data for the design of composite beam-CFT column. The evaluation of the member angle limit was performed with concrete compressive strength (fC =22.16 MPa, 30.49 MPa), breadth-to-thickness ratio (B/t=25.0, 33.3, 43.5), and axial capacity ratio (N/N0=0, 0.3, 0.4, 0.5) as the main variables of the test samples. For the relationship between the member angle limit (Ru) and the energy ratio (ES/EC ), the test result shows that the energy ratio becomes lower as the axial capacity ratio and the breadth-to-thickness ratio increase. The energy ratio is lower for the Type B test sample compared with that of Types A and C. For the formula suggested by SATO, the test samples are distributed evenly for comparison between test values and the member angle limit; however, other formulas indicate a deviation. Specifically, for the comparison between R u,cal and R u (Test), Maeda's formula shows severe deviation. 展开更多
关键词 square steel tube axial capacity ratio member angle limit breadth-to-thickness ratio
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Performance of Square Lightweight Concrete Specimens Confined by CFRP and GFRP
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作者 A. Vatani Oskouei M. Pirgholi Kivi S. Taghipour Boroujeni 《Journal of Civil Engineering and Architecture》 2010年第5期22-28,共7页
Confinement is an effective method in order to increase concrete strength and its ductility capacity. To improve the structural properties of lightweight concrete, Fiber Reinforced Polymer (FRP) can be used to confi... Confinement is an effective method in order to increase concrete strength and its ductility capacity. To improve the structural properties of lightweight concrete, Fiber Reinforced Polymer (FRP) can be used to confine the concrete. Effect of Fiber Reinforced Polymer on confined lightweight concrete elements is one of the most important research fields. It is generally accepted that the strength and stiffness of confined concrete is higher than unconfined one. In this research, behavior of confined and unconfined concrete specimens under uniaxial loading has been studied. In order to decrease stress concentration corners of specimens were chamfered to a radius of 5 to 25 mm. The Carbon Fiber Reinforced Polymer (CFRP) and Glass Fiber Reinforced Polymer (GFRP) were used to confine lightweight concrete specimens. The stress-strain curve of specimens is compared. 展开更多
关键词 Axial loading CFRP CONFINEMENT GFRP lightweight concrete.
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