The quench sensitivity of 6063 alloy was investigated via constructing time-temperature-property(TTP) curves by interrupted quenching technique and transmission electron microscopy(TEM) analysis.The results show t...The quench sensitivity of 6063 alloy was investigated via constructing time-temperature-property(TTP) curves by interrupted quenching technique and transmission electron microscopy(TEM) analysis.The results show that the quench sensitivity of 6063 alloy is lower than that of 6061 or 6082 alloy,and the critical temperature ranges from 300 to 410℃ with the nose temperature of about 360℃.From TEM analysis,heterogeneous precipitate β-Mg2Si is prior to nucleate on the(AlxFeySiz) dispersoids in the critical temperature range,and grows up most rapidly at the nose temperature of 360℃.The heterogeneous precipitation leads to a low concentration of solute,which consequently reduces the amount of the strengthening phase β'' after aging.In the large-scale industrial production of 6063 alloy,the cooling rate during quenching should be enhanced as high as possible in the quenching sensitive temperature range(410-300℃) to suppress the heterogeneous precipitation to get optimal mechanical properties,and it should be slowed down properly from the solution temperature to 410℃ and below 300℃ to reduce the residual stress.展开更多
The quenching sensitivity of AA7136 alloy was investigated by time−temperature−property(TTP)diagrams,and the heterogeneous precipitation behavior during isothermal holding was investigated using scanning electron micr...The quenching sensitivity of AA7136 alloy was investigated by time−temperature−property(TTP)diagrams,and the heterogeneous precipitation behavior during isothermal holding was investigated using scanning electron microscopy,scanning transmission electron microscopy and high resolution transmission electron microscopy.Based on 99.5%TTP diagram,the nose temperature is determined to be about 346℃ with the transformation time of about 0.245 s.The precipitation ofη(MgZn_(2)),T(Al_(2)Zn_(3)Mg_(3)),S(Al_(2)CuMg)or Cu−Zn-rich Y phases can be found depending on isothermal holding temperature and time,and it is described in a time−temperature−precipitation diagram.The size and area fraction of isothermal holding induced phase particles increase,which results in the decrease of hardness of samples after aging.The quantitative contribution to loss of hardness by grain boundaries/subgrain boundaries and dispersoids in the matrix is discussed based on the amount of heterogeneous precipitation related to them.展开更多
A combined conduction and radiation heat transfer model was used to simulate the heat transfer within wafer and investigate the effect of thermal transport properties on temperature non-uniformity within wafer surface...A combined conduction and radiation heat transfer model was used to simulate the heat transfer within wafer and investigate the effect of thermal transport properties on temperature non-uniformity within wafer surface. It is found that the increased conductivities in both doped and undoped regions help reduce the temperature difference across the wafer surface. However, the doped layer conductivity has little effect on the overall temperature distribution and difference. The temperature level and difference on the top surface drop suddenly when absorption coefficient changes from 104 to 103 m-1. When the absorption coefficient is less or equal to 103 m-1, the temperature level and difference do not change much. The emissivity has the dominant effect on the top surface temperature level and difference. Higher surface emissivity can easily increase the temperature level of the wafer surface. After using the improved property data, the overall temperature level reduces by about 200 K from the basis case. The results will help improve the current understanding of the energy transport in the rapid thermal processing and the wafer temperature monitor and control level.展开更多
基金Project supported by the National Natural Science Foundation of China(No.50776076)the Specialized Research Fund for the Doctoral Program of Higher Education(No.20110101110022),China
文摘The quench sensitivity of 6063 alloy was investigated via constructing time-temperature-property(TTP) curves by interrupted quenching technique and transmission electron microscopy(TEM) analysis.The results show that the quench sensitivity of 6063 alloy is lower than that of 6061 or 6082 alloy,and the critical temperature ranges from 300 to 410℃ with the nose temperature of about 360℃.From TEM analysis,heterogeneous precipitate β-Mg2Si is prior to nucleate on the(AlxFeySiz) dispersoids in the critical temperature range,and grows up most rapidly at the nose temperature of 360℃.The heterogeneous precipitation leads to a low concentration of solute,which consequently reduces the amount of the strengthening phase β'' after aging.In the large-scale industrial production of 6063 alloy,the cooling rate during quenching should be enhanced as high as possible in the quenching sensitive temperature range(410-300℃) to suppress the heterogeneous precipitation to get optimal mechanical properties,and it should be slowed down properly from the solution temperature to 410℃ and below 300℃ to reduce the residual stress.
基金financial supports from the National Key Research and Development Program of China (No. 2016YFB0300901)the Scientific Research Project of Inner Mongolia Colleges and Universities, China (No. NJZY21092)。
文摘The quenching sensitivity of AA7136 alloy was investigated by time−temperature−property(TTP)diagrams,and the heterogeneous precipitation behavior during isothermal holding was investigated using scanning electron microscopy,scanning transmission electron microscopy and high resolution transmission electron microscopy.Based on 99.5%TTP diagram,the nose temperature is determined to be about 346℃ with the transformation time of about 0.245 s.The precipitation ofη(MgZn_(2)),T(Al_(2)Zn_(3)Mg_(3)),S(Al_(2)CuMg)or Cu−Zn-rich Y phases can be found depending on isothermal holding temperature and time,and it is described in a time−temperature−precipitation diagram.The size and area fraction of isothermal holding induced phase particles increase,which results in the decrease of hardness of samples after aging.The quantitative contribution to loss of hardness by grain boundaries/subgrain boundaries and dispersoids in the matrix is discussed based on the amount of heterogeneous precipitation related to them.
基金Project(N110204015)supported by the Fundamental Research Funds for the Central Universities,ChinaProject(2012M510075)supported by the China Postdoctoral Science Foundation
文摘A combined conduction and radiation heat transfer model was used to simulate the heat transfer within wafer and investigate the effect of thermal transport properties on temperature non-uniformity within wafer surface. It is found that the increased conductivities in both doped and undoped regions help reduce the temperature difference across the wafer surface. However, the doped layer conductivity has little effect on the overall temperature distribution and difference. The temperature level and difference on the top surface drop suddenly when absorption coefficient changes from 104 to 103 m-1. When the absorption coefficient is less or equal to 103 m-1, the temperature level and difference do not change much. The emissivity has the dominant effect on the top surface temperature level and difference. Higher surface emissivity can easily increase the temperature level of the wafer surface. After using the improved property data, the overall temperature level reduces by about 200 K from the basis case. The results will help improve the current understanding of the energy transport in the rapid thermal processing and the wafer temperature monitor and control level.