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用鞣酸作显色剂测定钛铁矿中的微量钒 被引量:1
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作者 王敬 杨谅孚 《云南冶金》 2001年第5期51-52,共2页
pH4 5的酸度条件下 ,钒与鞣酸生成蓝色络合物。该体系λmax=6 2 0nm ,ε =3 30× 10 4 ,0~ 12 μg钒 /2 5mL符合比尔定律。该体系可用于钛铁矿中钒的测定 ,钛、铁的干扰可用沉淀分离法除去。
关键词 鞣酸 分光光度法 钛铁矿 测定 湿色剂
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2-苯并噻唑偶氮-7-(4-硝基苯偶氮)-1,8-二羟基萘-3,6-二磺酸的合成及用于铁和钛同时分光光度测定 被引量:8
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作者 夏心泉 张学军 +2 位作者 夏钦 张春玲 李民 《冶金分析》 CAS CSCD 北大核心 2000年第3期4-7,共4页
合成了一种新的不对称双偶氮变色酸类试剂 2 苯并噻唑偶氮 7 ( 4 硝基苯偶氮 ) 1 ,8 二羟基萘 3,6-二磺酸。研究了试剂的结构和试剂的光度性质 ,并用偏最小二乘法 (PLS)不经分离同时分光光度测定了合成试样和铝合金试样中的微量Fe ... 合成了一种新的不对称双偶氮变色酸类试剂 2 苯并噻唑偶氮 7 ( 4 硝基苯偶氮 ) 1 ,8 二羟基萘 3,6-二磺酸。研究了试剂的结构和试剂的光度性质 ,并用偏最小二乘法 (PLS)不经分离同时分光光度测定了合成试样和铝合金试样中的微量Fe 和Ti 。 展开更多
关键词 分光光度法 测定 湿色剂 BTANPACA
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Wind-power estimating model based on the experimental data in laboratory
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作者 HUANG Chung-neng 《Journal of Energy and Power Engineering》 2009年第9期60-66,共7页
Wind-power (WP) estimation is necessary for power system in several operations, which are as the optimal power flow between conventional units and wind farms, generators scheduling, and electricity market bidding. E... Wind-power (WP) estimation is necessary for power system in several operations, which are as the optimal power flow between conventional units and wind farms, generators scheduling, and electricity market bidding. Estimating the output power of a wind energy conversion unit (WEC) mainly bases on the incident wind speed at the unit site by using the power characteristic curve. In addition, several time-series models have been using in wind speed forecasting. These models are characterized with requiring a large set of data. In order to prevent from the wind speed measurement and the need of a precise wind turbine model, an novel method basing on neural network and the grey predictor model GM (1,1) is proposed. Though the method, the estimating model can be built only by using the experimental data, which are obtained from the WP system in laboratory. The effectiveness of the estimating model is confirmed by the simulation results. 展开更多
关键词 wind-power estimating model neural network grey predictor model
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Experimentally investigating the effect of buccal acupuncture on analgesic time-effect characteristics and monoamine neurotransmitters 被引量:9
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作者 Pu Rui-sheng Fang Xiao-li +2 位作者 Jie Wang-j un Liu Ding-long Su Cheng-hong 《Journal of Acupuncture and Tuina Science》 CSCD 2018年第4期229-235,共7页
Objective: To investigate the analgesic time-effect characteristics and changes in concentrations of rabbit's hypothalamic 5-hydroxytryptamine (5-HT) and noradrenaline (NE) caused by buccal acupuncture in the rh... Objective: To investigate the analgesic time-effect characteristics and changes in concentrations of rabbit's hypothalamic 5-hydroxytryptamine (5-HT) and noradrenaline (NE) caused by buccal acupuncture in the rheumatoid arthritis (RA) rabbits, and to reveal the analgesic central mechanism of buccal acupuncture, thereby providing a theoretical basis for the treatment of pain by buccal acupuncture. Methods: Forty rabbits were randomly divided into a normal group, a model group, a body acupuncture group, and a buccal acupuncture group, with 10 rabbits in each group. No model was established in the normal group, while equal dose of normal saline was injected at the matched site and time point; rabbits in other groups were subjected to the establishment of RA models using egg protein. From the 27th day of the experiment, rabbits in each group received the designated intervention. Rabbits in the normal group and the model group were fixed for 30 min every day using the same method as those in the other groups. In the acupuncture group, Dubi (ST 35) and Zusanli (ST 36) on bilateral hind limbs were selected. Perpendicular needling (using the needles with 0.25 mm in diameter and 25 mm in length) was performed with twirling manipulation for 15 s at intervals of 5 min. The needles were retained for 30 min and acupuncture was performed once a day. In the buccal acupuncture group, the knee point in the buccal acupuncture and needles with a diameter of 0.25 mm and a length of 15 mm were selected. Oblique needling was performed with twirling manipulation for 15 s at intervals of 5 min. The needles were retained for 30 min and acupuncture was performed once a day. The thermal pain thresholds at the O, 5, 15, 30, 60, 120 and 240 rain after the 1st and 10th acupuncture therapy were measured with a PL-200 thermal-inducing pain meter. After the 10th acupuncture therapy, rabbit's hypothalamus was removed, and the 5-HT and NE concentrations in the hypothalamus at the peak point of the acupuncture pain threshold curve were determined by high performance liquid chromatography (HPLC). Results: The analgesic effect was obvious at 5 min after buccal acupuncture started, peaked at 30 min, and decreased to the lowest value at 240 rain. Rabbits in the body acupuncture group began to show significant analgesic effect at 15 min, which was peaked at 30 min, and began to decline at 60 min. The pain threshold at 240 min was still higher than that at 0 mino Compared with the model group, the concentrations of hypothalamic 5-HT in the buccal acupuncture group and the body acupuncture group was significantly increased, and the between-group differences were statistically significant (both P〈0.05). The NE/5-HT ratios in hypothalamus in the buccal acupuncture group and the body acupuncture group were significantly lower than the ratio in the model group, and the differences were statistically significant (both P〈0.05); difference in the decrease was statistically significant between the buccal acupuncture group and the body acupuncture group (P〈0.05). Conclusion: The analgesic effect of buccal acupuncture shows an obvious time-dependent curve. It is characterized by rapid onset of pain relief, rapid increase and decline in pain threshold. 5-HT and NE levels in rabbit's hypothalamus can be affected by buccal acupuncture, with increased 5-HT concentration and reduced NE/5-HT rati0. 展开更多
关键词 Acupuncture Therapy Buccal Acupuncture Acupuncture Analgesia ARTHRITIS RHEUMATOID 5-HYDROXYTRYPTAMINE Neuroregulators Rabbits
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