In the traditional pipeline magnetic flux leakage(MFL)detection technology,circumferential or axial excitation is mainly used to excite the magnetic field of defects.However,the domestic and foreign pipeline detection...In the traditional pipeline magnetic flux leakage(MFL)detection technology,circumferential or axial excitation is mainly used to excite the magnetic field of defects.However,the domestic and foreign pipeline detection devices currently in operation are mainly axial excitation MFL detection tools,in which circumferential cracks can be clearly identified,but the detection sensitivity of axial cracks is not high,thus forming a detection blind zone.Therefore,a composite excitation multi-extension direction defect MFL detection method is proposed,which can realize the simultaneous detection of axial and circumferential defects.On the basis of the electromagnetic theory Maxwell equation and Biot Savart law,a mathematical model of circumferential and axial magnetization is firstly established.Then finite element simulation software is used to establish a model of a new type of magnetic flux leakage detection device,and a simulation analysis of crack detection in multiple extension directions is carried out.Finally,under the conditions of the relationship model between the change rate of leakage magnetic field and external excitation intensity under unsaturated magnetization and the multi-stage coil magnetization model,the sample vehicle towing experiment is carried out.The paper aims to analyze the feasibility and effectiveness of the new magnetic flux leakage detection device for detecting defects in different extension directions.Based on the final experimental results,the new composite excitation multi extension direction leakage magnetic field detector has a good detection effect for defects in the axial and circumferential extension directions.展开更多
ZnO nanorods prepared by a solution-phase method are annealed at different temperatures in oxygen ambient.The luminescence properties of the samples are investigated.In the same excitation condition,the photoluminesce...ZnO nanorods prepared by a solution-phase method are annealed at different temperatures in oxygen ambient.The luminescence properties of the samples are investigated.In the same excitation condition,the photoluminescence(PL) spectra of all samples show an ultraviolet(UV) emission and a broad strong visible emission band.The asymmetric visible emis-sion band of annealed samples has a red-shift as the annealing temperature increasing from 200 ℃ to 600 ℃ and it can be deconvoluted into two subband emissions centered at 535 nm(green emission) and 611 nm(orange-red emission) by Gaussian-fitting analysis.Analyses of PL excitation(PLE) spectra and PL spectra at different excitation wavelengths reveal that the green emission and the orange-red emission have a uniform initial state,which can be attributed to the electron transition from Zn interstitial(Zni) to oxygen vacancy(Vo) and oxygen interstitial(Oi),respectively.展开更多
基金National Natural Science Foundation of China(No.51804267)State Key Laboratory of Petroleum Resources and Prospecting,China University of Petroleum,Beijing(No.PRP/open-1610)。
文摘In the traditional pipeline magnetic flux leakage(MFL)detection technology,circumferential or axial excitation is mainly used to excite the magnetic field of defects.However,the domestic and foreign pipeline detection devices currently in operation are mainly axial excitation MFL detection tools,in which circumferential cracks can be clearly identified,but the detection sensitivity of axial cracks is not high,thus forming a detection blind zone.Therefore,a composite excitation multi-extension direction defect MFL detection method is proposed,which can realize the simultaneous detection of axial and circumferential defects.On the basis of the electromagnetic theory Maxwell equation and Biot Savart law,a mathematical model of circumferential and axial magnetization is firstly established.Then finite element simulation software is used to establish a model of a new type of magnetic flux leakage detection device,and a simulation analysis of crack detection in multiple extension directions is carried out.Finally,under the conditions of the relationship model between the change rate of leakage magnetic field and external excitation intensity under unsaturated magnetization and the multi-stage coil magnetization model,the sample vehicle towing experiment is carried out.The paper aims to analyze the feasibility and effectiveness of the new magnetic flux leakage detection device for detecting defects in different extension directions.Based on the final experimental results,the new composite excitation multi extension direction leakage magnetic field detector has a good detection effect for defects in the axial and circumferential extension directions.
基金supported by the National Natural Science Foundation of China(Nos.60877029,10904109,60977035 and 60907021)the Natural Science Foundation of Tianjin(Nos.09JCYBJC01400 and 10SYSYJC28100)+1 种基金the Key Subject for Materials Physics and Chemistry of Tianjinthe Open Foundation of Key Laboratory of Luminescence and Optical Information of Ministry of Education(Nos.2010LOI02 and 2010LOI11)
文摘ZnO nanorods prepared by a solution-phase method are annealed at different temperatures in oxygen ambient.The luminescence properties of the samples are investigated.In the same excitation condition,the photoluminescence(PL) spectra of all samples show an ultraviolet(UV) emission and a broad strong visible emission band.The asymmetric visible emis-sion band of annealed samples has a red-shift as the annealing temperature increasing from 200 ℃ to 600 ℃ and it can be deconvoluted into two subband emissions centered at 535 nm(green emission) and 611 nm(orange-red emission) by Gaussian-fitting analysis.Analyses of PL excitation(PLE) spectra and PL spectra at different excitation wavelengths reveal that the green emission and the orange-red emission have a uniform initial state,which can be attributed to the electron transition from Zn interstitial(Zni) to oxygen vacancy(Vo) and oxygen interstitial(Oi),respectively.
