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载金炭分析方法 被引量:9
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作者 丁凤珍 黄福滨 《地质实验室》 1999年第4期232-234,共3页
研究了提出了载金炭分析的样品采集方法,水份分析和金的分析。试验表明所拟定的样品采集方法具有足够的代表性,水份分析值RSD〈0.5%,Au的分析值RSD〈0.7%。原子吸收分光光度法分析Au的结果与容量法、火法分析结果... 研究了提出了载金炭分析的样品采集方法,水份分析和金的分析。试验表明所拟定的样品采集方法具有足够的代表性,水份分析值RSD〈0.5%,Au的分析值RSD〈0.7%。原子吸收分光光度法分析Au的结果与容量法、火法分析结果上符。 展开更多
关键词 载金炭 采样 水份 火法分析
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火-湿法结合测定合质金品位 被引量:2
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作者 孙莹 《黄金》 CAS 北大核心 1995年第2期52-53,共2页
火-湿法结合测定合质金品位孙莹(沈阳黄金学院)合质金的品位分析方法有火法和湿法。湿法流程短、速度快,但只能用于较高品位合质金的分析。品位低于80%的合质金试样在王水中溶解时,生成致密的AgCl层复盖在表面,试样很难完... 火-湿法结合测定合质金品位孙莹(沈阳黄金学院)合质金的品位分析方法有火法和湿法。湿法流程短、速度快,但只能用于较高品位合质金的分析。品位低于80%的合质金试样在王水中溶解时,生成致密的AgCl层复盖在表面,试样很难完全溶解。火法即包铅灰吹一分银法,合... 展开更多
关键词 合质金 品位分析 火法分析 湿法分析 测定
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杂铜中金、银的测定方法研究 被引量:3
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作者 徐红喜 袁玉霞 李树森 《矿冶》 CAS 2003年第3期86-88,共3页
在参考粗铜中测定金银的国家标准分析方法基础上,对杂铜样品组成、取样代表性、样品分解及贵金属的快速有效分离富集等进行了研究,建立了杂铜中贵金属金银的分析方法。该方法不仅准确可靠、代表性好、适用含量范围宽,而且大大缩短了分... 在参考粗铜中测定金银的国家标准分析方法基础上,对杂铜样品组成、取样代表性、样品分解及贵金属的快速有效分离富集等进行了研究,建立了杂铜中贵金属金银的分析方法。该方法不仅准确可靠、代表性好、适用含量范围宽,而且大大缩短了分析周期。对于含量为Au2 83g/t、Ag956g/t的杂铜,测定的相对标准偏差(RSD)分别为6 47%和2 40%。 展开更多
关键词 杂铜 火法试金分析 测定方法 贵金属
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A New Method for Ride Quality Analysis of Vehicle
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作者 林建辉 张洁 +1 位作者 高燕 李天瑞 《Journal of Donghua University(English Edition)》 EI CAS 2006年第6期134-136,共3页
Current spectral analysis for evaluating the rail ride quality effectively is based on the sampling data at a uniform time interval, but the train is of fluctuation velocity in motion, which results in a non-uniform i... Current spectral analysis for evaluating the rail ride quality effectively is based on the sampling data at a uniform time interval, but the train is of fluctuation velocity in motion, which results in a non-uniform interval between consecutive sampling data. Therefore the accuracy of routine spectral analysis is in doubt when applying it in evaluating the rail ride quality. This paper presents a new way, namely, re-sampling with variable frequency to eliminate the influence of the train's uneven velocity. Its feature is that there is no need for precision measurement of the train's moving speed. Experiment results from the test-bed of rolling stock vibration show that it is valid. 展开更多
关键词 rail ride quality non-uniform sample resample and reconstitute signal processing.
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Estimation of Knock Wheel Noise of Rail Transport with an Acoustic Intensity Method
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作者 Kolykhalin Vitaly 《Journal of Mechanics Engineering and Automation》 2012年第8期465-469,共5页
The application of railway wheel noise compensation method is considered. The effect can be obtained by shift a pair of usual parallel rail joints on a pair of offset rail joints, for example, the right rail joint is ... The application of railway wheel noise compensation method is considered. The effect can be obtained by shift a pair of usual parallel rail joints on a pair of offset rail joints, for example, the right rail joint is shifted concerning the left rail joint on the certain distance. The distance is depend on the speed of train and promotes the correlation interconnection between excited acoustical pulses. The intensity wheel knock spectrograms corresponding of different distance between rail joints registered by the microphone are estimated. The spectrograms considerably differed from each other in low frequency band are analyzed. The result of practical using the acoustic noise compensation method is proved. 展开更多
关键词 Control noise ACOUSTIC RAILWAY MICROPHONE wheel knock.
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Criteria of limiting temperature and parametric analysis of the large deflection behavior for fully restrained steel beams in fire 被引量:2
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作者 XI Feng LUAN YanPing 《Science China(Technological Sciences)》 SCIE EI CAS 2012年第1期264-275,共12页
This paper mainly involve 3 parts:1) To apply the minimum principle of acceleration in dynamics of elastic-plastic continua at finite deformation to the statics problems,a computing model is presented for the restrain... This paper mainly involve 3 parts:1) To apply the minimum principle of acceleration in dynamics of elastic-plastic continua at finite deformation to the statics problems,a computing model is presented for the restrained steel beams exposed to the fire.In this model,both effects of large deflection and thermal expansion deformation are taken into account,and the constitutive equations with the temperature effects are used.Then a dynamic finite difference(DFD) method is presented by using the dis-crete technique,which can be used in simulating the response of the steel beams at elevated temperature,and the large deflec-tion behavior and catenary action effects of the beams can be adequately expressed.The primary numerical results show that the method is valid and credible.Compared with other methods,this technique is very simple,and it can also be further devel-oped to simulate the behavior of steel beams subjected to the coupling loading of explosion and fire when both effects of strain rate and inertia are considered.2) By using this DFD method,detailed parametric analysis are presented so as to check the consistency of response results for several different formulas of thermal expansion deformation and retention factors of steel at elevated temperature,the influence of these parameters on the critical temperature is examined.3) Based on the analysis for the curves of temperature-generalized yield function comprised by the axial force and bending moment,both criteria to determine the limiting temperature(or failure temperature) of large deflection steel beams are presented more explicitly,that is,both lim-iting temperatures can be determined by if the catenary force begins to appear or arrives at the maximum value,respectively.It is shown by numerical results that both limiting temperatures are close to the both critical temperatures which are correspond-ing to the maximum deflections equal to span/20 and span/10,respectively.This conclusion may be helpful to make rational fire resisting design for the steel beams. 展开更多
关键词 steel beam FIRE DFD method large deflection parametric analysis limiting temperature criteria yield function
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Implantation induced defects and electrical properties of Sb-implanted ZnO 被引量:1
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作者 XIE Hui LIU Tong +4 位作者 LIU JingMing CAO Ke Wei DONG ZhiYuan YANG Jun ZHAO YouWen 《Science China(Technological Sciences)》 SCIE EI CAS CSCD 2015年第8期1333-1338,共6页
Defects in Sb implanted Zn O single crystals have been studied by using photoluminescence(PL) spectroscopy,X-ray diffraction(XRD) and Raman scattering.Electrical properties of the samples were analyzed by Hall effect ... Defects in Sb implanted Zn O single crystals have been studied by using photoluminescence(PL) spectroscopy,X-ray diffraction(XRD) and Raman scattering.Electrical properties of the samples were analyzed by Hall effect measurement.The results indicate that the annealed Sb-implanted sample is n-type with a free electron concentration of the same amplitude as the calculated implantation concentration.The well-known oxygen vacancy related deep level green PL band is suppressed in the as-implanted sample and recovers to the level close to the as-grown Zn O single crystal after annealing.These phenomena suggest that a large portion of as-implanted Sb atoms occupy oxygen lattice site in an unstable state and move to the interstitial site,forming the complex donor defect upon high temperature annealing,resulting in n-type conduction even if the implantation dose is quite high. 展开更多
关键词 ZNO PHOTOLUMINESCENCE Ramam scattering Hall measurement ion implantation DEFECT
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