热压应变及相关因素对竹材表面粗糙度的影响

对用“热进热出”、“冷进冷出”热压工艺处理的竹材和自然状态下的竹材表面粗糙度用精密仪器进行检测,用数学方法对检测结果进行分析和处理,检测和分析结果表明,热压过程中竹材产生的应力和应变、竹材本身的微观构造和物理化学特性以及相关的热压工艺参数,对竹材的表面粗糙度均会产生不同程度的影响。

Effect of strain rate and deformation temperature on strain hardening and softening behavior of pure copper

The effects of the deformation temperature and the strain rate on the hot deformation behavior of pure copper were investigated based on compression tests. The expressions of strain hardening rate, dynamic recrystallization critical stress, saturated stress, dynamic recovery volume fraction and dynamic recrystallization volume fraction were determined. According to the processing map, the instability regions occur in regions of 400?450 °C, 0.001?0.05 s?1 and 450?750 °C, 0.05?1 s?1. The deformation mechanism in the stability region is dynamic recrystallization. The flow stress was predicted. The results also show that the true stress–true strain curves predicted by the extracted model are in good agreement with the experimental results.

改善LOM型快速成形中胶厚均匀性的研究

ＬＯＭ 制件中胶厚分布不均匀严重影响ＬＯＭ 技术的成形精度和应用效益。文章实测了ＺＩＰＰＹ快速成形系统使用的粘胶的流变学性能，建立了粘胶热压应变的力学模型，对模型进行求解和修正，并据此提出改善粘胶分布均匀性的措施。

Constitutive equation and processing map for hot compressed as-cast Ti-43Al-4Nb-1.4W-0.6B alloy

High temperature compressive deformation behaviors of as-cast Ti-43Al-4Nb-1.4W-0.6B alloy was investigated at temperatures ranging from 1323 K to 1473 K, and strain rates from 0.001 s-1 to 1 s-1. The results indicated that the true stress-true strain curves show a dynamic flow softening behavior. The flow curves after the friction and the temperature compensations were employed to develop constitutive equations. The effects of temperature and the strain rate on the deformation behavior were represented by Zener-Holloman exponential equation. The influence of strain was incorporated in the constitutive analysis by considering the effect of the strain on material constants by a five-order polynomial. A revised model was proposed to describe the relationships among the flow stress, strain rate and temperature and the predicted flow stress curves were in good agreement with experimental results. Appropriate deformation processing parameters were suggested based on the processing map which was constructed from friction and temperature corrected flow curves, determined as 1343 K, 0.02 s-1 and were successfully applied in the canned forging of billets to simulate industrial work condition.

Hot deformation behavior of Al-Zn-Mg-Cu-Zr aluminum alloys during compression at elevated temperature

The hot compression tests of Al-Zn-Mg-Cu-Zr aluminum alloys （7056 alloy and 7150 alloy） were performed in a temperature range from 300 to 450 °C and at strain rate range from 0.01 to 10 s-1. The results show that the true stress-true strain curves exhibit a peak stress at a critical strain, then the flow stresses decrease monotonically until high strains, showing a dynamic flow softening. The peak stresses depend on the temperature compensated strain rate, which can be represented by the Zener-Hollomon parameter Z in the hyperbolic-sine equation with hot deformation activation energy of 244.64 kJ/mol for 7056 alloy and 229.75 kJ/mol for 7150 alloy, respectively, while the peak stresses for the former are lower than those for the latter under the similar compression condition. The deformed microstructures consist of a great amount of precipitates within subgrains in the elongated grains at high Z value and exhibit well formed subgrains in the recrystallized grains at low Z value. The smaller subgrains and greater density of fine precipitates in 7150 alloy are responsible for the high peak stresses because of the substructural strengthening and precipitating hardening compared with 7056 alloy.

Effect of consolidation parameters on mechanical properties of Cu-based bulk amorphous alloy consolidated by hot pressing

Cu50Zr40Ti10 bulk amorphous alloys were fabricated by hot pressing gas-atomized Cu50Zr40Ti10 amorphous powder under different consolidation conditions without vacuum and inert gas protection. The consolidation conditions of the Cu50Zr40Ti10 amorphous powder were investigated based on an L9（34） orthogonal design. The compression strength and strain limit of the Cu50Zr40Ti10 bulk amorphous alloys can reach up to 1090.4 MPa and 11.9 %, respectively. The consolidation pressure significantly influences the strain limit and compression strength of the compact. But the mechanical properties are not significantly influenced by the consolidation temperature. In addition, the preforming pressure significantly influences not the compression strength but the strain limit. The optimum consolidation condition for the Cu50Zr40Ti10 amorphous powder is first precompacted under the pressure of 150 MPa, and then consolidated under the pressure of 450 MPa and the temperature of 380 °C.

Hot compression behavior and deformation microstructure of Mg-6Zn-1Al-0.3Mn magnesium alloy

The hot compression behavior of a wrought Mg-6Zn-1Al-0.3Mn magnesium alloy was investigated using Gleeble test at 200-400 °C with strain rates ranging from 0.01 to 7 s-1. The true stress-strain curves show that the hot deformation behavior significantly depends on the deformation temperature and strain rate. The calculated hot deformation activation energy Q is 166 kJ/mol with a stress exponent n=5.99, and the constitutive equation is deduced to be ε＆ =3.16×1013[sinh（0.010σ）]5.99exp [-1.66×105/（RT）]· Deformation microstructure shows that the incompletely dynamically recrystallized grains can be found at grain boundaries and twins with the strain rates ranging from 0.01 to 1 s^-1 at 250 °C, and completely dynamic recrystallization occurs when the temperature is 350 °C or above during hot compression, the size of recrystallized grains decreases with the increment of the strain rate at the same temperature. The relatively suitable deformation condition is considered temperature 330-400 °C and strain rate of 0.01-0.03 s-1, and temperature of 350 °C and strain rate of 1 s-1.

Flow behavior and microstructure evolution of 6A82 aluminium alloy with high copper content during hot compression deformation at elevated temperatures

The flow behavior and microstructure evolution of 6A82 aluminum alloy (Al?Mg?Si?Cu) with high copper content were studied on a Gleeble?1500 system by isothermal hot compression test in the temperature range from 320 to 530 °C and the strain rate range from 0.001 to 10 s?1. The results reveal that the flow stress of the alloy exhibits a continuous flow softening behavior at low temperatures of 320?390 °C, whereas it reaches steady state at high temperatures (≥460°C), which are influenced greatly by the Zener?Hollomon parameter (Z) in the hyperbolic sine with the hot deformation activation energy of 325.12 kJ/mol. Microstructure characterizations show that prominent dynamic recrystallization and coarsening of dynamic precipitation may be responsible for the continuous flow softening behavior. Due to deformation heating at high strain rates (≥1 s?1), dynamic recrystallization is more prominent in the specimen deformed at 530 °C and 10 s?1 than in the specimen deformed at 460 °C and 0.1 s?1 even though they have very close lnZ values.

Flow stress behavior and processing map of extruded 7075Al/SiC particle reinforced composite prepared by spray deposition during hot compression

Hot compression tests of the extruded 7075Al/15%SiC (volume fraction) particle reinforced composite prepared by spray deposition were performed on Gleeble?1500 system in the temperature range of 300?450 °C and strain rate range of 0.001?1 s?1. The results indicate that the true stress?true strain curve almost exhibits rapid flow softening phenomenon without an obvious work hardening, and the stress decreases with increasing temperature and decreasing strain rate. Moreover, the stress levels are higher at temperature below 400 °C but lower at 450 °C compared with the spray deposited 7075Al alloy. Superplastic deformation characteristics are found at temperature of 450 °C and strain rate range of 0.001?0.1 s?1 with corresponding strain rate sensitivity of 0.72. The optimum parameters of hot working are determined to be temperature of 430?450 °C and strain rate of 0.001?0.05 s?1 based on processing map and optical microstructural observation.

Flow behavior of Al-6.2Zn-0.70Mg-0.30Mn-0.17Zr alloy during hot compressive deformation based on Arrhenius and ANN models

The hot deformation behavior of Al?6.2Zn?0.70Mg?0.30Mn?0.17Zr alloy was investigated by isothermal compressiontest on a Gleeble?3500machine in the deformation temperature range between623and773K and the strain rate range between0.01and20s?1.The results show that the flow stress decreases with decreasing strain rate and increasing deformation temperature.Basedon the experimental results,Arrhenius constitutive equations and artificial neural network(ANN)model were established toinvestigate the flow behavior of the alloy.The calculated results show that the influence of strain on material constants can berepresented by a6th-order polynomial function.The ANN model with16neurons in hidden layer possesses perfect performanceprediction of the flow stress.The predictabilities of the two established models are different.The errors of results calculated by ANNmodel were more centralized and the mean absolute error corresponding to Arrhenius constitutive equations and ANN model are3.49%and1.03%,respectively.In predicting the flow stress of experimental aluminum alloy,the ANN model has a betterpredictability and greater efficiency than Arrhenius constitutive equations.

Flow stress behavior of Al-Cu-Li-Zr alloy containing Sc during hot compression deformation

The flow stress behavior of Al-3.5Cu-1.5Li-0.25(Sc+Zr) alloy during hot compression deformation was studied by isothermal compression test using Gleeble-1500 thermal-mechanical simulator. Compression tests were preformed in the temperature range of 653-773 K and in the strain rate range of 0.001-10 s-1 up to a true plastic strain of 0.7. The results indicate that the flow stress of the alloy increases with increasing strain rate at a given temperature,and decreases with increasing temperature at a given imposed strain rate. The relationship between the flow stress and the strain rate and the temperature was derived by analyzing the experimental data. The flow stress is in a hyperbolic sine relationship with the strain rate,and in an Arrhenius relationship with the temperature,which imply that the process of plastic deformation at an elevated temperature for this material is thermally activated. The flow stress of the alloy during the elevated temperature deformation can be represented by a Zener-Hollomon parameter with the inclusion of the Arrhenius term. The values of n,α and A in the analytical expressions of flow stress σ are fitted to be 5.62,0.019 MPa-1 and 1.51×1016 s-1,respectively. The hot deformation activation energy is 240.85 kJ/mol.

Reheating and thixoforging of ZK60+RE alloy deformed by ECAE

The two-pass equal channel angular extrusion (ECAE) process was introduced into strain-induced melt activation (SIMA) to predeform a ZK60 alloy with rare earth (RE) addition. Microstructure evolution of ECAE-formed ZK60+RE alloy during reheating was investigated. Furthermore, tensile properties of thixoforged components were determined. The results show that the SIMA process can produce ideal microstructures, and spheroidized solid particles with little entrapped liquid can be obtained. With prolonging holding time, the size of solid particles increases and the degree of spheroidization is improved. The tensile properties of the thixoforged ZK60+RE samples are close to those of two-pass ECAE-formed samples.

Thermal contact conductance at continuous roll-casting interface

The effects of surface roughness, strain rate, friction coefficient and pressure on real contact area were analyzed based on the research of Stupkiewicz. The real contact area model taking account of the effect of friction and deformation of material was obtained. The model of contact conductance at the rolling interface was obtained by integrating the specific feature of heat transfer through the interface of continuous roll-casting. The results indicate that the real contact area increases obviously when the material is under yield, and the real contact area varies inversely with surface roughness, whereas it varies exponentially with friction coefficient, strain rate and pressure, and the power factor depends on strain rate.

Hot compression deformation characteristics of Mg-Mn alloys

The hot deformation behaviors of solution treated Mg-1.8Mn-0.4Er-0.2Al alloys were investigated by means of compression tests on Gleeble-1500 in strain rate range of 0.01-10s-1,deformation temperature range of 250-450℃ and a true strain of 0.6.The constitutive relationships among flow stress,strain rate and deformation temperature were described by Arrhenius-type equations,based on the fact that the material constants could be calculated under a wide range of strains.The results show that the flow stress of the experimental alloy decreases with temperature increasing and strain rate decreasing.Under the experimental conditions,the products of constant α and n in the constitutive equation are stable within certain strains,and the deformation activation energy ranges from 160 to 220 kJ/mol.It is proved that the values of calculated flow stress are close to the experimental results with average error of 2.01%.

Hot deformation behavior of Ti-6.5Al-3.5Mo-1.5Zr-0.3Si alloy with acicular microstructure

The characteristics of hot deformation of an α＋β titanium alloy Ti-6.5Al-3.5Mo-1.5Zr-0.3Si with acicular microstructure were studied using isothermal hot compressive tests in a strain rate range of 0.01-10 s^-1 at 860-1 100 ℃. The true stress-tree strain curves of alloy hot-compressed in the α＋β region exhibit a peak stress followed by continuous flow softening; whereas in the β region, the flow stress attains a steady-state regime. At a strain rate of 10 s^-1 and in a wide temperature range, the alloy exhibits plastic flow instability. According to the kinetic rate equation, the apparent activation energies are estimated to be about 633 kJ/mol in the α＋β region and 281 kJ/mol in the β region, respectively. The processing maps show a domain of the globularization process of a colony structure and α dynamic recrystallization in the temperature range of 860-960 ℃ with a peak efficiency of about 60%, and a domain of β dynamic recrystallization in the β region with a peak efficiency of 80%.

Design and control of methyl acetate-methanol separation via heat-integrated pressure-swing distillation

Design and control of pressure-swing distillation(PSD) with different heat integration modes for the separation of methyl acetate/methanol azeotrope are explored using Aspen Plus and Aspen Dynamics. First, an optimum steady-state separation configuration conditions are obtained via taking the total annual cost(TAC) or total reboiler heat duty as the objective functions. The results show that about 27.68% and 25.40% saving in TAC can be achieved by the PSD with full and partial heat integration compared to PSD without heat integration. Second,temperature control tray locations are obtained according to the sensitivity criterion and singular value decomposition(SVD) analysis and the single-end control structure is effective based on the feed composition sensitivity analysis. Finally, the comparison of dynamic controllability is made among various control structures for PSD with partial and full heat integration. It is shown that both control structures of composition/temperature cascade and pressure-compensated temperature have a good dynamic response performance for PSD with heat integration facing feed flowrate and composition disturbances. However, PSD with full heat integration performs the poor controllability despite of a little bit of economy.

Effect of twinning on flow stress during initial stage of hot compression of twin roll cast Mg-5.51Zn-0.49Zr alloy

A Thermecmastor-Z hot deformation simulator,optical microscopy,XRD and TEM were employed to characterize the flow stress behavior and microstructure of twin roll cast ZK60 magnesium alloy during initial stage of hot compression at elevated temperature of 300 ℃ and 400 ℃ and a given strain rate of 10-2s-1.The results suggest that flow stress drop during initial stage of hot compression at 300℃,generally led by dynamic recrystallization,is attributed to twinning,correspondingly to dynamic recrystallization as deformation temperature is raised to 400 ℃.

Effects of Heat Softening on Initiation of Landslides

Effects of heat softening on the initiation of slide surface(shear banding) in clayey slopes during fast deformation were discussed.Controlling equations considering heat,pore pressure and mechanical movement were presented.By perturbation method,the instability condition of localized zone(i.e.criterion for initiation of shear banding) for thermal related soils,such as clayey slope,was obtained.It is shown that slide surface initiates once the thermal-softening effects overcome the strain-hardening effects whether it is adiabatic or not.Without strain hardening effects,strain rate hardening obviously plays a role in initiation of shear band.During initiating process,heat is trapped inside the shear band,which leads rapidly to a pore pressure increase and fast loss of strength.The localized shear strain is concentrated in a narrow zone with a width of several centimeters at most and increases fast.This zone forms the sliding surface.Temperature can increase more than 2?C,pore pressure can increase 160% in about 0.1s inside this zone.These changes cause the fast decrease in friction-coefficient by about 36% over the initial value.That is how shear band initiated and developed in clayey slopes.

Hot compressive deformation behavior and constitutive relationship of Al-Zn-Mg-Zr alloy with trace amounts of Sc

Abstract： The hot deformation behaviors of AI-Zn-Mg-Sc-Zr alloy were investigated in a temperature range of 340-500℃ and a strain rate range of 0.001-10 s 1 using uniaxial compression test on Gleeble-1500 thermal simulation machine. The results show that the flow stress increases with increasing strain and tends to be constant after a peak value. The flow stress increases with increasing strain rate and decreases with increasing deformation temperature. The phenomenon of dynamic recovery and dynamic recrystallization can be observed by microstructural evolutions. Based on the hyperbolic Arrhenius-type equation, the true stress-true strain data from the tests were employed to establish the constitutive equation considering the effect of the true strain on material constants （α, β, Q, n and A）, which reveals the dependence of the flow stress on strain, strain rate and deformation temperature. The predicted stress-strain curves are in good agreement with experimental results, which confirms that the developed constitutive equations are suitable to research the hot deformation behaviors of Al-Zn-Mg-Sc-Zr alloy.

Flexible conductive Ag nanowire/cellulose nano?bril hybrid nanopaper for strain and temperature sensing applications

With the rapid development of smart wearable devices, flexible and biodegradable sensors are in urgent needs. In this study, ‘‘green" electrically conductive Ag nanowire (Ag NW)/cellulose nanofiber (CNF) hybrid nanopaper was fabricated to prepare flexible sensors using the facial solution blending and vacuum filtration technique. The amphiphilic property of cellulose is beneficial for the homogeneous dispersion of Ag NW to construct effective electrically conductive networks. Two different types of strain sensors were designed to study their applications in strain sensing. One was the tensile strain sensor where the hybrid nanopaper was sandwiched between two thermoplastic polyurethane (TPU) films through hot compression, and special micro-crack structure was constructed through the pre-strain process to enhance the sensitivity. Interestingly, typical pre-strain dependent strain sensing behavior was observed due to different crack densities constructed under different pre-strains. As a result, it exhibited an ultralow detection limit as low as 0.2%, good reproducibility under different strains and excellent stability and durability during 500 cycles (1% strain, 0.5 mm/min). The other was the bending strain sensor where the hybrid nanopaper was adhered onto TPU film, showing stable and recoverable linearly sensing behavior towards two different bending modes (tension and compression). Importantly, the bending sensor displayed great potential for human motion and physiological signal detection. Furthermore, the hybrid nanopaper also exhibited stable and reproducible negative temperature sensing behavior when it was served as a temperature sensor. This study provides a guideline for fabricating flexible and biodegradable sensors.