The hot deformation characteristics of the Ti-5.7Al-2.1Sn-3.9Zr-2Mo-0.1Si(Ti-6242S)alloy with an acicular starting microstructure were analyzed using processing map.The uniaxial hot compression tests were performed at...The hot deformation characteristics of the Ti-5.7Al-2.1Sn-3.9Zr-2Mo-0.1Si(Ti-6242S)alloy with an acicular starting microstructure were analyzed using processing map.The uniaxial hot compression tests were performed at temperatures ranging from 850 to 1000℃and at strain rates of 0.001-1 s-1.The developed processing map was used to determine the safe and unsafe deformation conditions of the alloy in association with the microstructural evolution by SEM and OM.It was recognized that the flow stress revealed differences in flow softening behavior by deformation at 1000℃compared to the lower deformation temperatures,which was attributed to microstructural changes.The processing map developed for typical strain of 0.7 in two-phase field exhibited high efficiency value of power dissipation of about 55%at 950℃and 0.001 s-1,basically due to extensive globularization.An increase in strain rate and a decrease in temperature resulted in a decrease in globularization ofαlamellae,whileαlamellar kinking increased.Eventually,the instability domain of flow behavior was identified in the temperature range of 850-900℃and at the strain rate higher than 0.01 s-1 reflecting the flow localization and adiabatic shear banding.By considering the power efficiency domains and the microstructural observations,the deformation in the temperature range of 950-1000℃and strain rate range of 0.001-0.01 s-1 was desirable leading to high efficiencies.It was realized that(950℃,0.001 s-1)was the optimum deformation condition for the alloy.展开更多
Microstructural development in hot working of TA15titanium alloy with primary stripαstructure was investigated withthe aim to globularizeαstrips.Results show that the mechanisms of morphology transformation are the ...Microstructural development in hot working of TA15titanium alloy with primary stripαstructure was investigated withthe aim to globularizeαstrips.Results show that the mechanisms of morphology transformation are the same to the spheroidizationmechanisms of lamellar structure.Boundary splitting and termination migration are more important than coarsening due to the largesize of stripα.Theαstrips are stable in annealing due to the unfavorable geometrical orientation of intra-αboundaries,the largethickness of strip and the geometrical stability ofαparticles.Predeformation and low speed deformation accelerate globularization ofαstrips in the following ways:direct changing of particle shape,promotion of boundary splitting and termination migration byincreasing high angle grain boundaries and interfacial area,promotion of coarsening by forming dislocation structures.Largepredeformation combined with high temperature annealing is a feasible way to globularize stripα.展开更多
Hot compression was performed on a multilayered Au−20Sn eutectic alloy to investigate the deformation behavior and microstructure evolution.During hot compression,microstructural spheroidization was initiated from pla...Hot compression was performed on a multilayered Au−20Sn eutectic alloy to investigate the deformation behavior and microstructure evolution.During hot compression,microstructural spheroidization was initiated from plastic instability regions,and it was preferentially activated in vertical lamellae with a growth direction parallel to the compressive direction.Continuous dynamic recrystallization associated with lattice dislocations was the mechanism in both AuSn and Au5Sn multilayers.After spheroidization,strain accumulations were weakened in both of the equiaxed phases,and the deformation mechanism was substantially replaced by grain boundary sliding and migration.Based on these findings,hot rolling was conducted on an as-cast Au−20Sn alloy and a foil with a thickness of~50μm was successfully prepared.The present study can promote the development of Au−20Sn foils,and provide insights into the deformation behavior and microstructure evolution of multilayered eutectic alloys.展开更多
文摘The hot deformation characteristics of the Ti-5.7Al-2.1Sn-3.9Zr-2Mo-0.1Si(Ti-6242S)alloy with an acicular starting microstructure were analyzed using processing map.The uniaxial hot compression tests were performed at temperatures ranging from 850 to 1000℃and at strain rates of 0.001-1 s-1.The developed processing map was used to determine the safe and unsafe deformation conditions of the alloy in association with the microstructural evolution by SEM and OM.It was recognized that the flow stress revealed differences in flow softening behavior by deformation at 1000℃compared to the lower deformation temperatures,which was attributed to microstructural changes.The processing map developed for typical strain of 0.7 in two-phase field exhibited high efficiency value of power dissipation of about 55%at 950℃and 0.001 s-1,basically due to extensive globularization.An increase in strain rate and a decrease in temperature resulted in a decrease in globularization ofαlamellae,whileαlamellar kinking increased.Eventually,the instability domain of flow behavior was identified in the temperature range of 850-900℃and at the strain rate higher than 0.01 s-1 reflecting the flow localization and adiabatic shear banding.By considering the power efficiency domains and the microstructural observations,the deformation in the temperature range of 950-1000℃and strain rate range of 0.001-0.01 s-1 was desirable leading to high efficiencies.It was realized that(950℃,0.001 s-1)was the optimum deformation condition for the alloy.
基金Projects(51205317,51575449) supported by the National Natural Science Foundation of ChinaProject(3102015AX004) supported by the Fundamental Research Funds for the Central Universities,ChinaProject(104-QP-2014) supported by the Research Fund of the State Key Laboratory of Solidification Processing,China
文摘Microstructural development in hot working of TA15titanium alloy with primary stripαstructure was investigated withthe aim to globularizeαstrips.Results show that the mechanisms of morphology transformation are the same to the spheroidizationmechanisms of lamellar structure.Boundary splitting and termination migration are more important than coarsening due to the largesize of stripα.Theαstrips are stable in annealing due to the unfavorable geometrical orientation of intra-αboundaries,the largethickness of strip and the geometrical stability ofαparticles.Predeformation and low speed deformation accelerate globularization ofαstrips in the following ways:direct changing of particle shape,promotion of boundary splitting and termination migration byincreasing high angle grain boundaries and interfacial area,promotion of coarsening by forming dislocation structures.Largepredeformation combined with high temperature annealing is a feasible way to globularize stripα.
基金financial supports from the National Natural Science Foundation of China(Nos.U1502272,51901204)the Precious Metal Materials Genome Engineering in Yunnan Province,China(Nos.2019ZE001,202002AB080001)。
文摘Hot compression was performed on a multilayered Au−20Sn eutectic alloy to investigate the deformation behavior and microstructure evolution.During hot compression,microstructural spheroidization was initiated from plastic instability regions,and it was preferentially activated in vertical lamellae with a growth direction parallel to the compressive direction.Continuous dynamic recrystallization associated with lattice dislocations was the mechanism in both AuSn and Au5Sn multilayers.After spheroidization,strain accumulations were weakened in both of the equiaxed phases,and the deformation mechanism was substantially replaced by grain boundary sliding and migration.Based on these findings,hot rolling was conducted on an as-cast Au−20Sn alloy and a foil with a thickness of~50μm was successfully prepared.The present study can promote the development of Au−20Sn foils,and provide insights into the deformation behavior and microstructure evolution of multilayered eutectic alloys.
