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铌、铈、锰掺杂对钛酸钡基陶瓷性能的影响 被引量:3
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作者 张宏亮 李强 余爱梅 《科学技术与工程》 北大核心 2019年第12期182-187,共6页
在钛酸钡中以五氧化二铌、三氧化二铈形式引入铌、铈元素,采用了固相法反应制备Nb、Ce双施主掺杂的微米级钛酸钡基正温度系数(PTC)陶瓷粉;同时研究了加入受主元素Mn对PTC陶瓷材料性能的影响。利用XRD和SEM分析了样品的物相及微观相貌,... 在钛酸钡中以五氧化二铌、三氧化二铈形式引入铌、铈元素,采用了固相法反应制备Nb、Ce双施主掺杂的微米级钛酸钡基正温度系数(PTC)陶瓷粉;同时研究了加入受主元素Mn对PTC陶瓷材料性能的影响。利用XRD和SEM分析了样品的物相及微观相貌,发现样品结晶完整,颗粒均匀。实验表明,以Ce、Nb、Mn进行掺杂可有效改善材料在室温条件下的PTC性能;当掺入0.2 mol%Nb_2O_5、0.3 mol%Ce_2O_3、0.08 mol%Mn(NO_3)_2时,制出室温电阻率为616Ω·cm、升阻比大于10、居里温度为60℃的PTC热敏陶瓷;并利用制成的PTC材料作为加热源对受控器件进行加热实验。 展开更多
关键词 钛酸钡基PTC陶瓷 Ce、Nb、Mn 共掺杂 热控实验
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Experimental Study on Emission Control of Premixed Catalytic Combustion of Natural Gas Using Preheated Air 被引量:2
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作者 许考 刘中良 +2 位作者 何洪 程水源 马重芳 《Chinese Journal of Chemical Engineering》 SCIE EI CAS CSCD 2007年第1期68-74,共7页
In this paper the premixed catalytic combustion emissions such as CO, unburned hydrocarbon (UHC), NOx and the temperature distribution in the catalytic monolith with ultra low concentration of Pd were studied. Three t... In this paper the premixed catalytic combustion emissions such as CO, unburned hydrocarbon (UHC), NOx and the temperature distribution in the catalytic monolith with ultra low concentration of Pd were studied. Three types of monoliths were used for experiments and the temperature of preheated air was respectively 50℃ , 100℃ and 200℃ . The results showed that preheated air made radial temperature in the catalytic monolith uniform which helped to avoid local hot spots so as to decrease NOx emission. The experiment also proved that the shorter monolith showed much better catalytic combustion performance than longer one and the temperature at the exit of the shorter monolith was relatively lower. On the contrary, the temperature was higher in the longer monolith and the lethal NOx emission was slightly increased. 展开更多
关键词 catalytic combustion preheated air natural gas EMISSION
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Pyrolysis of Huadian oil shale by electrical heating on different heating rates 被引量:2
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作者 G.Roland Nguimbi 《Global Geology》 2012年第2期120-125,共6页
The electrical heating experiments on oil shale sample from Huadian of Jilin were carried out by the pyrolysis method at three different heating rate 2℃/min, 5 ℃/min and 10 ℃/min in the temperature range of 30℃ -... The electrical heating experiments on oil shale sample from Huadian of Jilin were carried out by the pyrolysis method at three different heating rate 2℃/min, 5 ℃/min and 10 ℃/min in the temperature range of 30℃ -750℃. Heating rate 2 ℃/rain is considered low, while intermediate one covers the range 5 ℃/min and high heating rate is 10℃/min. The controlling parameters studied were the final pyrolysis temperature and the influence of the heating rate as well as type. The heating rate has an important effect on the pyrolysis of oil shale and the amount of residual carbon obtained therefore. It is found that increasing the heating rate and py- rolysis temperature also increases the production of oil and the total weight loss. Higher heating rates resulted in higher rates of accumulation. The rate of oil and water collection passed through the maximum of different heat- ing rates at different pyrolysis temperatures. Heating rate affected density, oil conversion and oil yield. 展开更多
关键词 oil shale PYROLYSIS electrical heating Huadian Jilin
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Theoretical and Experimental Investigations of Solar Heating Systems at Specified Output Conditions of Hot Water
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作者 W. Tadros M. Saadeldin S.A. Hassan 《Journal of Energy and Power Engineering》 2011年第9期842-847,共6页
The theoretical analysis discussed in this work is a suitable mathematical tool by which the performance of the proposed collector can be predicted. The obtained experimental results coincide with the obtained theoret... The theoretical analysis discussed in this work is a suitable mathematical tool by which the performance of the proposed collector can be predicted. The obtained experimental results coincide with the obtained theoretical data obtained from the devised computer program. Controlled output temperature can be obtained from the proposed system. The performance of the tested collector under the proposed intermittent flow conditions overcomes that of the conventional thermosyphone flow collector. 展开更多
关键词 Solar collector thermal efficiency thermosyphone intermittent flow mass floW rate solar heating system
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Experimental Study of Perfectly Patterned Silica-Titania Optical Waveguide 被引量:1
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作者 Rimlee DEB ROY Devika SIL +2 位作者 Sunirmal JANA Prasanta Kumar BISWAS Shyamal Kumar BHADRA 《Photonic Sensors》 SCIE EI CAS 2012年第1期81-91,共11页
Inorganic silica-titania thin films with thicknesses 150 nm-200 nm are deposited on high purity and polished silicon wafer and silica glass substrates by sol-gel dipping process and are patterned by capillary force li... Inorganic silica-titania thin films with thicknesses 150 nm-200 nm are deposited on high purity and polished silicon wafer and silica glass substrates by sol-gel dipping process and are patterned by capillary force lithography technique. Subsequently grating structure is embossed in green stage. The patterned gel films are subjected to stepwise heat treatment to 500 ℃ and above in pure oxygen atmosphere in order to achieve major conversion of mixed-gel to oxide optical films which are characterized by Ellipsometry, Fourier transform infrared spectroscopy (FTIR) and atomic force microscopy (AFM) to optimize the fabrication parameters and to get perfectly matched film. Removal of organics and formation of perfectly inorganic silica-titania network at optimized heat treatment in controlled environment are ensured by FTIR spectral study. The difference in refractive indices between the substrate and coated film as developed waveguides for operating wavelength show the planar waveguide behavior of the films. calculated theoretically matches exactly with the (632.8 nm) and the measured optical properties 展开更多
关键词 Optical properties sol-gel technique thin films OXIDES
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