The B4C/2024Al composites were successfully produced by pressureless infiltration method, and the effects of heat treatment on phase content and mechanical properties were investigated by X-ray diffraction （XRD）, sc...The B4C/2024Al composites were successfully produced by pressureless infiltration method, and the effects of heat treatment on phase content and mechanical properties were investigated by X-ray diffraction （XRD）, scanning electron microscopy （SEM） and mechanical properties testing. The results show that phases of BnC/2024Al composites include B4C, Al, Al3BC, AlB2 and Al2Cu. The phase species remain unchanged; however, the phase content of the composites changes significantly after heat treatment at the temperature of 660, 700, 800 or 900 ℃ for 12, 24 or 36 h. It is found that the heat treatment results in not only considerable enhancement in hardness, but also reduction in bending strength of the composites. Heat treatment at 800 ℃ for 36 h does best to hardness of the composites, while at 700 ℃ for 36 h it is the most beneficial to their comprehensive mechanical properties.展开更多
文摘碳纤维混杂增强复合材料由于具有重量轻、可设计性强等诸多优点,广泛用于汽车、海洋、航空航天等行业.根据固化剂与环氧树脂的配比化学原理,计算出石墨烯-碳纤维混杂增强树脂基(GO-CF/EP)复合材料的最佳配比为1∶5,并采用真空浸渗热压成型工艺(VIHPS)制备1∶2~1∶7共六个配比的试样,结合形状记忆性能测试及微观形貌的观察,得到固化剂与环氧树脂实际最佳配比.实验结果表明,GO-CF/EP复合材料性能主要取决于体系中交联度的大小,交联度越大,复合材料的形状记忆性能越好,微观组织形貌也较理想.当基体配比为1∶5时,GO-CF/EP复合材料体系中交联度最大,微观形貌呈现均匀致密的状态,形状固定率最大,为95.90%;形状回复率最大,为95.40%;形状回复时间最短,为80.30 s;形状回复力最大,为9.48 N.当基体配比为1∶2或1∶7时,固化剂过量或不足,交联度较小,微观组织形貌中有大量的基体聚集区,其形状记忆性能下降,形状固定率及回复率也相应减小,分别为82.99%,81.66%,81.91%,78.75%;形状回复力分别只有5.20 N和5.50 N.
基金Project(2011CB605805)supported by the National Basic Research Program of China
文摘The B4C/2024Al composites were successfully produced by pressureless infiltration method, and the effects of heat treatment on phase content and mechanical properties were investigated by X-ray diffraction （XRD）, scanning electron microscopy （SEM） and mechanical properties testing. The results show that phases of BnC/2024Al composites include B4C, Al, Al3BC, AlB2 and Al2Cu. The phase species remain unchanged; however, the phase content of the composites changes significantly after heat treatment at the temperature of 660, 700, 800 or 900 ℃ for 12, 24 or 36 h. It is found that the heat treatment results in not only considerable enhancement in hardness, but also reduction in bending strength of the composites. Heat treatment at 800 ℃ for 36 h does best to hardness of the composites, while at 700 ℃ for 36 h it is the most beneficial to their comprehensive mechanical properties.
