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离子束截面抛光-电子探针仪分析在SiC_p/Al复合材料相结构研究中的应用 被引量:5
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作者 胡莹 张澜庭 《理化检验(物理分册)》 CAS 2017年第2期101-104,共4页
SiC颗粒增强铝基复合材料(SiC_p/Al),由于其结构复杂且各组成单元之间的物理、化学性质存在明显的差异,因而在试样制备、微观结构表征等工作中存在一定困难。利用离子束截面抛光(CP)制样技术结合电子探针X射线分析仪(EPMA)分析,提出了... SiC颗粒增强铝基复合材料(SiC_p/Al),由于其结构复杂且各组成单元之间的物理、化学性质存在明显的差异,因而在试样制备、微观结构表征等工作中存在一定困难。利用离子束截面抛光(CP)制样技术结合电子探针X射线分析仪(EPMA)分析,提出了一种适宜解析这种复合材料微观相结构的方法。试验结果证实:该方法效果明显,结果直观、可靠;并可推广到类似材料的微观结构精细解析研究中。 展开更多
关键词 离子束截面抛光 电子探针仪分析 SICP/AL复合材料 相结构解析
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Process mineralogy and characteristic associations of iron and phosphorus-based minerals on oolitic hematite 被引量:10
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作者 罗立群 张汉泉 《Journal of Central South University》 SCIE EI CAS CSCD 2017年第9期1959-1967,共9页
The chemical compositions,mineralogical characteristics,as well as dissemination of iron-and phosphorus-based minerals were studied for the E’xi oolitic hematite from western Hubei Province in China by using chemical... The chemical compositions,mineralogical characteristics,as well as dissemination of iron-and phosphorus-based minerals were studied for the E’xi oolitic hematite from western Hubei Province in China by using chemical analysis,optical microscope,electron probe micro-analyzer(EPMA)and energy dispersive spectroscopy(EDS).It is found that this kind of oolitic hematite ore contains 47.71%TFe,10.96%SiO_2,as well as 0.874%P,with hematite as the dominant Fe-bearing minerals,and quartz,chamosite,illite and cellophane as main gangue minerals.The microscope examination showed that the ore has an oolitic structure,with some ooids principally formed by a series of concentric layers of hematite collophanite around nucleus that is hematite in the association with collophanite.Based on the EPMA and EDS analysis,it can be known that some ooids are primarily composed of hematite and collophanite.The separation can be achieved through fine grinding for those collophanite laminae with a higher P content.However,the dissemination of two minerals at the interface will result in the difficulty in effective separation.Besides,some ooids are made of chamosite with some nucleus formed of quartz,which is principally finely disseminated with hematite.In view of the close association and dissemination of iron-and phosphorus-based minerals in the ooids,it is found that the process of stage-grindings and stage-separations can be adopted to effectively increase the iron recovery and decrease the P content in the concentrate to some extent. 展开更多
关键词 oolitic hematite process mineralogy dissemination of iron- and phosphorus-based minerals electron probe micro-analyzer(EPMA) energy dispersive spectroscopy (EDS)
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