Vertically orientated TiO2 nanotube array with diameters ranging from 60 up to 80 nm and length of 4 μm was grown on titanium by anodization.Crack initiation,propagation and saturation were studied using the substrat...Vertically orientated TiO2 nanotube array with diameters ranging from 60 up to 80 nm and length of 4 μm was grown on titanium by anodization.Crack initiation,propagation and saturation were studied using the substrate straining test.The results show that annealing obviously modifies the interfaces.With the increase of tensile strain,cracks in TiO2 nanotube films propagate rapidly and reach the saturation within a narrow strain gap.Interfacial shear strengths of TiO2 nanotube films without annealing,with 250 ℃ annealing and with 400 ℃ annealing can be estimated as 163.3,370.2 and 684.5 MPa,respectively.The critical energy release rates of TiO2 nanotube films are calculated as 49.6,102.6 and 392.7 J/m2,respectively.The fracture toughnesses of TiO2 nanotube films are estimated as 0.996,1.433 and 2.803 MPa-m1/2,respectively.The interfacial bonding mechanism of TiO2 nanotube film is chemical bonding.展开更多
Shear-sliding mode(mode Ⅱ)fracture of rocks is a vital failure form in deep underground engineering.To gain deep insight into the anisotropic shear fracture behaviors of a typical shale under high normal stress condi...Shear-sliding mode(mode Ⅱ)fracture of rocks is a vital failure form in deep underground engineering.To gain deep insight into the anisotropic shear fracture behaviors of a typical shale under high normal stress conditions,a series of direct shear tests were conducted on double-notched specimens in three typical bedding orientations(i.e.,the arrester,divider,short-transverse orientations)and under five normal stresses.The modeⅡfracture toughness(K_(Ⅱc))is found to exhibit a significant 3D anisotropy.The maximum K_(Ⅱc)is obtained in the divider orientation,followed by those in the arrester and short-transverse orientations.In contrast,the 3D anisotropy in the critical modeⅡenergy release rate(G_(Ⅱc))is not as significant as that in K_(Ⅱc),and G_(Ⅱc)in the arrester orientation is quite close to that in the divider orientation.The anisotropy in the prepeak input energy accumulated during shearing is found to be exactly consistent with that in G_(Ⅱc),which has not been noted before.Furthermore,the anisotropies in the modeⅡfracture resistances will,unexpectedly,not be weakened by the high normal stress.Owing to the layered structures,tensile cracks are involved during the modeⅡfracture process,resulting in the formation of rough fracture surfaces.展开更多
In this work, a test method was developed to determine the interfacial fracture toughness of the air plasma sprayed （APS） thermal barrier coatings （TBCs） over a wide range of mode mixities. For this mixed-mode tes...In this work, a test method was developed to determine the interfacial fracture toughness of the air plasma sprayed （APS） thermal barrier coatings （TBCs） over a wide range of mode mixities. For this mixed-mode test method, the analytical expres- sions for the energy release rate and stress intensity factors were derived based on the energy theory and the concept of ＂equi- valence＂. The fidelity of these expressions was affirmed by selected finite element analysis. The experimental results showed that the critical energy release rate increased with the increase of the positive mode mixity, which was mainly due to the increase in contact/friction effect and plastic work dissipation with increasing shear mode loading. Furthermore, an elliptical interfacial failure criterion in terms of the stress intensity factors was proposed. The agreement between the experimental results in the literature and those in our work indicated that our test method and the corresponding analytical solutions can well determine the interfaeial fracture toughness of the TBCs over a wide range of mode mixities.展开更多
基金Project(50604017) supported by the National Natural Science Foundation of ChinaProject(20110946Z) supported by the State Key Laboratory of Powder Metallurgy,China
文摘Vertically orientated TiO2 nanotube array with diameters ranging from 60 up to 80 nm and length of 4 μm was grown on titanium by anodization.Crack initiation,propagation and saturation were studied using the substrate straining test.The results show that annealing obviously modifies the interfaces.With the increase of tensile strain,cracks in TiO2 nanotube films propagate rapidly and reach the saturation within a narrow strain gap.Interfacial shear strengths of TiO2 nanotube films without annealing,with 250 ℃ annealing and with 400 ℃ annealing can be estimated as 163.3,370.2 and 684.5 MPa,respectively.The critical energy release rates of TiO2 nanotube films are calculated as 49.6,102.6 and 392.7 J/m2,respectively.The fracture toughnesses of TiO2 nanotube films are estimated as 0.996,1.433 and 2.803 MPa-m1/2,respectively.The interfacial bonding mechanism of TiO2 nanotube film is chemical bonding.
基金Project(12172240)supported by the National Natural Science Foundation of ChinaProject(2021YFH0030)supported by the Science&Technology Department of Sichuan Province,China。
文摘Shear-sliding mode(mode Ⅱ)fracture of rocks is a vital failure form in deep underground engineering.To gain deep insight into the anisotropic shear fracture behaviors of a typical shale under high normal stress conditions,a series of direct shear tests were conducted on double-notched specimens in three typical bedding orientations(i.e.,the arrester,divider,short-transverse orientations)and under five normal stresses.The modeⅡfracture toughness(K_(Ⅱc))is found to exhibit a significant 3D anisotropy.The maximum K_(Ⅱc)is obtained in the divider orientation,followed by those in the arrester and short-transverse orientations.In contrast,the 3D anisotropy in the critical modeⅡenergy release rate(G_(Ⅱc))is not as significant as that in K_(Ⅱc),and G_(Ⅱc)in the arrester orientation is quite close to that in the divider orientation.The anisotropy in the prepeak input energy accumulated during shearing is found to be exactly consistent with that in G_(Ⅱc),which has not been noted before.Furthermore,the anisotropies in the modeⅡfracture resistances will,unexpectedly,not be weakened by the high normal stress.Owing to the layered structures,tensile cracks are involved during the modeⅡfracture process,resulting in the formation of rough fracture surfaces.
基金supports from the National Natural Science Foundation of China(No. 10872105 and No. 51071094)
文摘In this work, a test method was developed to determine the interfacial fracture toughness of the air plasma sprayed （APS） thermal barrier coatings （TBCs） over a wide range of mode mixities. For this mixed-mode test method, the analytical expres- sions for the energy release rate and stress intensity factors were derived based on the energy theory and the concept of ＂equi- valence＂. The fidelity of these expressions was affirmed by selected finite element analysis. The experimental results showed that the critical energy release rate increased with the increase of the positive mode mixity, which was mainly due to the increase in contact/friction effect and plastic work dissipation with increasing shear mode loading. Furthermore, an elliptical interfacial failure criterion in terms of the stress intensity factors was proposed. The agreement between the experimental results in the literature and those in our work indicated that our test method and the corresponding analytical solutions can well determine the interfaeial fracture toughness of the TBCs over a wide range of mode mixities.
