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界面退火对外延BiFeO_3薄膜光伏特性的影响
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作者 彭增伟 刘保亭 《材料导报》 EI CAS CSCD 北大核心 2018年第A02期69-72,共4页
采用射频磁控溅射的方法在(001)取向的SrRuO_3(SRO)/SrTiO_3(STO)衬底上制备了外延BiFeO_3(BFO)薄膜,在室温条件下溅射一层金属Pt作为上电极,构建了Pt/BFO/SRO电容器。X射线衍射显示BFO薄膜呈现良好的外延生长,极化-电场滞后回线和净极... 采用射频磁控溅射的方法在(001)取向的SrRuO_3(SRO)/SrTiO_3(STO)衬底上制备了外延BiFeO_3(BFO)薄膜,在室温条件下溅射一层金属Pt作为上电极,构建了Pt/BFO/SRO电容器。X射线衍射显示BFO薄膜呈现良好的外延生长,极化-电场滞后回线和净极化强度测试结果说明Pt/BFO/SRO电容器具有良好的铁电性。为了检测界面对Pt/BFO/SRO电容器光伏特性的影响,将整个Pt/BFO/SRO电容器分别在180℃和500℃的条件下快速热处理2min,以改变Pt/BFO界面态。在室温、180℃和500℃的条件下,Pt/BFO/SRO电容器光伏效应的开路电压分别为0.22V、0.12V和0.05V,短路电流密度分别为9.2μA/cm^2,4.9μA/cm^2和0.12μA/cm^2。开路电压和短路电流密度都随着退火温度的升高而降低,这是高温退火恶化了界面态的结果。在室温条件下,Pt/BFO/SRO电容器光伏效应的光电转换效率为0.009 4%,大于部分前期报道的结果。 展开更多
关键词 界面退火 BIFEO3薄膜 光伏特性
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铝/钛/铝三层复合板热轧工艺及微观组织研究 被引量:11
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作者 陈泽军 陈全忠 +1 位作者 黄光杰 刘雪峰 《材料导报》 EI CAS CSCD 北大核心 2012年第6期106-109,共4页
钛/铝层状复合材料具有两种材料优异的特性,能够满足一些特殊工程需要。开发了热轧复合技术,成功制备了铝(1100)/钛(TA2)/铝(1100)三层复合板。研究了复合板轧制过程中的关键轧制技术参数(临界压下率和轧制复合工艺条件)。利用光学显微... 钛/铝层状复合材料具有两种材料优异的特性,能够满足一些特殊工程需要。开发了热轧复合技术,成功制备了铝(1100)/钛(TA2)/铝(1100)三层复合板。研究了复合板轧制过程中的关键轧制技术参数(临界压下率和轧制复合工艺条件)。利用光学显微镜和SEM观察了钛/铝复合板及结合界面形貌,分析了不同退火温度对复合板力学性能的影响。基于实验结果,描述了影响复合板质量和有助于提高复合板结合强度的关键工艺过程。 展开更多
关键词 复合板热轧微观结构结合界面退火
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离子束辅助淀积下Cu/Si系统相变研究
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作者 张楠 邱安平 《哈尔滨理工大学学报》 CAS 2001年第4期75-77,共3页
研究在离子束条件下硅基底上淀积金属薄膜及其界面结构在退火条件下金属硅化物的形成和变化特点,即15keV的Ar+在IBAD条件下直接生成Cu15Si4相.IBAD复合薄膜样品在退火前无新相生成,而退火后形成ε相,不同于... 研究在离子束条件下硅基底上淀积金属薄膜及其界面结构在退火条件下金属硅化物的形成和变化特点,即15keV的Ar+在IBAD条件下直接生成Cu15Si4相.IBAD复合薄膜样品在退火前无新相生成,而退火后形成ε相,不同于通常Cu-Si退火反应生成ε相的相序.研究证明在Cu-Si界面退火反应系统中,ε相的成核是得到稳定相结构的关键. 展开更多
关键词 金属硅化物 相变 金属薄膜 铜硅界面退火反应 离子束辅助沉积 真空镀膜
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Effect of heat treatment on microstructure and thermophysical properties of diamond/2024 Al composites 被引量:6
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作者 修子扬 王旭 +2 位作者 M.HUSSAIN 冯超 姜龙涛 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2013年第12期3584-3591,共8页
50%diamond particle (5μm) reinforced 2024 aluminum matrix (diamond/2024 Al) composites were prepared by pressure infiltration method. Diamond particles were distributed uniformly without any particle clustering, ... 50%diamond particle (5μm) reinforced 2024 aluminum matrix (diamond/2024 Al) composites were prepared by pressure infiltration method. Diamond particles were distributed uniformly without any particle clustering, and no apparent porosities or significant casting defects were observed in the composites. The diamond-Al interfaces of as-cast and annealed diamond/2024 Al composites were clean, smooth and free from interfacial reaction product. However, a large number of Al2Cu precipitates were found at diamond-Al interface after aging treatment. Moreover, needle-shaped Al2MgCu precipitates in Al matrix were observed after aging treatment. The coefficient of thermal expansion (CTE) of diamond/2024 Al composites was about 8.5×10-6 °C-1 between 20 and 100 °C, which was compatible with that with chip materials. Annealing treatment showed little effect on thermal expansion behavior, and aging treatment could further decrease the CTE of the composites. The thermal conductivity of obtained diamond/2024 Al composites was about 100 W/(m?K), and it was slightly increased after annealing while decreased after aging treatment. 展开更多
关键词 Al matrix composites DIAMOND INTERFACE ANNEALING AGING thermal properties
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Evolutions of texture and grain boundary plane distributions in a ferritic stainless steel
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作者 方晓英 王卫国 +2 位作者 郭红 秦聪祥 周邦新 《Journal of Central South University》 SCIE EI CAS 2012年第12期3363-3368,共6页
The grain size, textures and grain boundary plane distributions in a cold-rolled and annealed ferritic stainless steel were investigated by means of EBSD techniques. The results show that, following cold rolling with ... The grain size, textures and grain boundary plane distributions in a cold-rolled and annealed ferritic stainless steel were investigated by means of EBSD techniques. The results show that, following cold rolling with the thickness reduction of 85%, relatively low temperature (780℃) annealing brings an extremely sluggish grain growth and no grain texture develops when the annealing time varies from 5 min to 480 min. The free energy reduction of the system is mainly caused by the grain boundary plane re-orientation in addition to minor grain growth because the distributions of grain boundary planes are moderately preferred on { 100} according to the five parameter analyses (FPA) concerning the grain boundary plane characteristics. However, in the case of high-temperature (1 000 ℃) annealing, the average grain size does not increase until annealing time is prolonged to 90 min, after which extensive grain growth occurs and strong {100}(hkl) texture emerges whereas nearly random grain boundary plane distributions are observed. The free energy reduction of the system is most likely attributed to the selective growth. 展开更多
关键词 grain texture grain boundary plane EBSD ferritic stainless steel
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