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气相色谱质谱法测定6种加香目标物质的含量及对烟丝加香均匀性的评价 被引量:12
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作者 夏启东 何邦华 +4 位作者 侯英 申晓锋 蒋举兴 杨蕾 邱昌桂 《分析测试学报》 CAS CSCD 北大核心 2012年第7期816-822,共7页
建立了一种运用气相色谱-质谱联用技术(GC-MS)同时测定卷烟烟丝中呋喃酮、异戊酸异戊酯、麦芽酚、薄荷醇、乙基麦芽酚和茴香脑6种烟用加香目标物的检测方法。试样用二氯甲烷溶液振荡提取,旋转蒸发仪浓缩,气相色谱-质谱联用仪检测分析。... 建立了一种运用气相色谱-质谱联用技术(GC-MS)同时测定卷烟烟丝中呋喃酮、异戊酸异戊酯、麦芽酚、薄荷醇、乙基麦芽酚和茴香脑6种烟用加香目标物的检测方法。试样用二氯甲烷溶液振荡提取,旋转蒸发仪浓缩,气相色谱-质谱联用仪检测分析。分别对样品量、萃取溶剂和萃取时间等前处理条件进行了优化。该方法的线性相关系数r均在0.998以上,采用SIM法定量分析,其平均加标回收率为86%~92%,相对标准偏差(RSD,n=6)为4.7%~7.1%,检出限(S/N=3)和定量下限(S/N=10)分别为0.014 7~0.0746μg/g和0.048 9~0.248 8μg/g。结果表明,该方法简便、灵敏度高、线性关系好,能满足同时测定烟丝中此6种加香目标物质的要求。方法还通过测定烟丝样品中加香目标物的含量及其含量的RSD值对卷烟制丝工艺加香的均匀性进行了评价。 展开更多
关键词 气相色谱-质谱(GC-MS) 卷烟 目标物质 加香均匀性 测定方法
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物质主义者自我概念的特点和相关理论 被引量:14
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作者 周静 谢天 《心理科学进展》 CSSCI CSCD 北大核心 2019年第5期914-925,共12页
物质主义的经典研究分别从人格、价值观、目标和需要的角度界定和理解物质主义的相关现象。自我概念一直是贯穿物质主义研究的线索,但直到最近研究者才试图以它为理论基点统摄与整合已有研究。相关研究表明,物质主义者对自我的评价较低... 物质主义的经典研究分别从人格、价值观、目标和需要的角度界定和理解物质主义的相关现象。自我概念一直是贯穿物质主义研究的线索,但直到最近研究者才试图以它为理论基点统摄与整合已有研究。相关研究表明,物质主义者对自我的评价较低,表现为低自尊、权变性自尊;对自我的认识具有不一致性,表现为自我概念不清晰、外显-内隐自尊分离、以及自我差距(理想自我与现实自我的差距)。最近出现的两个综合理论——物质主义的自我逃离理论与物质主义的认同目标追求理论提出,物质主义是个体将物质拥有作为逃避自我的方式或满足自我认同动机的手段。这两个理论弥补了现有物质主义研究缺乏整合性理论的不足。未来研究可以通过借鉴有关自我概念的理论,超越单纯的物质主义者自我匮乏的思路,从而做出更大的理论贡献。 展开更多
关键词 物质主义 自我概念 物质主义的自我逃离理论 物质主义的认同目标追求理论
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两种葡萄酒的核磁共振氢谱的信息分析
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作者 金英今 杨光 +2 位作者 方英玉 李熙峰 王思宏 《食品研究与开发》 CAS 北大核心 2023年第16期157-161,共5页
基于核磁共振(nuclear magnetic resonance,NMR)技术具有无损检测结构信息的特点,利用宽带探头(broadband observe,BBO)和标准压制水峰脉冲序列zgcpfqpr(zero go composite pulse frequency presaturation),获得两种葡萄酒非目标物质信... 基于核磁共振(nuclear magnetic resonance,NMR)技术具有无损检测结构信息的特点,利用宽带探头(broadband observe,BBO)和标准压制水峰脉冲序列zgcpfqpr(zero go composite pulse frequency presaturation),获得两种葡萄酒非目标物质信息,并用标准加入法检定葡萄酒中的甲醇含量,研究结果表明核磁共振可以判断两种葡萄酒中甲醇、糖度、乙酸、乳酸、柠檬酸、琥珀酸、葡萄汁液中脯氨酸等信息。 展开更多
关键词 葡萄酒 核磁共振氢谱 目标物质信息 无损检测 标准加入法
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Shape Optimization and Assessment of Wind Induced Stresses in Domes
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作者 K. S. Babu Narayan Subhash C. Yaragal Yukio Tamura 《Journal of Civil Engineering and Architecture》 2012年第7期925-927,共3页
Domes are popularly used for column free areas. They are employed as covers to reservoirs and treatment units and also as containment in nuclear reactors. Inverted domes are popular as foundations. Structures are buil... Domes are popularly used for column free areas. They are employed as covers to reservoirs and treatment units and also as containment in nuclear reactors. Inverted domes are popular as foundations. Structures are built with an intended end use for a specified utility period. The functional requirement is to serve the purpose and the structural requirement constitutes stability, strength, safety, serviceability and durability. Satisfaction of these requirements at affordable costs is the goal of structural optimization. This paper demonstrates the need and scope for optimization of domes by formulating and solving the problem by use of calculus (volume of material is the objective function being minimized using first principles of calculus). A simple but elegant method is suggested for determination of wind stresses by statics which compares very well with that obtained by rigorous method. 展开更多
关键词 DOME SHAPE wind stresses SEARCH optimization.
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Ranking Agricultural Sub-basins for Environmental Protection 被引量:1
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作者 Liu Wenbao Gu Fengxia 《Chinese Journal of Population,Resources and Environment》 2010年第1期32-37,共6页
Reconstructing long-term vegetation buffers along streams in agricultural landscapes has become a common environmental restoration strategy for improving water quality and wildlife habitat connectivity.This article de... Reconstructing long-term vegetation buffers along streams in agricultural landscapes has become a common environmental restoration strategy for improving water quality and wildlife habitat connectivity.This article developed a linear weighted model to rank the priority of agricultural sub-basins for the establishment of vegetative buffers.The method was applied to an agricultural watershed of 146 km2 in Ontario,Canada.The watershed was divided into 11 sub-basins as basic decision units.In each subbasin,four stream buffer schemes with widths of 5,10,15 and 20m were generated.For each buffer,three benefit-cost attributes of reconstructing vegetation cover were estimated,which include acreage per dollar,sediment abatement per dollar and habitat benefit per dollar.These attributes were first normalized using a linear normalization approach to eliminate the effects across different units.The normalized attributes were then integrated using a simple additive weighting method to rank the 11 sub-basins for prioritizing spatial restoration action.A sensitivity analysis was also conducted to observe the impact of a change in attribute weights on the management decisions.The results suggest that vegetation buffers reconstructed for achieving the water quality goal are not effective in improving habitat connectivity and vice versa. 展开更多
关键词 watershed management riparian buffer cost-benefit analysis landscape restoration
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金钱和快乐如何换算
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作者 林子 《财会月刊(合订本)》 北大核心 2003年第04C期59-60,共2页
谁说金钱买不到快乐?一项研究发现,仅1000英镑的横财,便足以令一个普通人的人生发生改变。
关键词 金钱 快乐 经济学理论 横财 薪酬 心理压力 婚姻 健康 物质目标 助人为乐
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Partial Characterization of Chitinolytic Extract from Endophytic Streptomyces sp. and Its Effects on the Boll Weevil
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作者 M. C. Quecine P. T. Lacava +4 位作者 S. R. Magro J. R. P. Parra W. L. Araujo J. L. Azevedo A. A.Pizzirani-Kleiner 《Journal of Agricultural Science and Technology》 2011年第4期420-427,共8页
The present study achieves the biochemistry partial characterization of the chitinolytic extract produced by an endophytic Streptomyces sp. strain (A8). This extract was also tested against Anthonomus grandis, the c... The present study achieves the biochemistry partial characterization of the chitinolytic extract produced by an endophytic Streptomyces sp. strain (A8). This extract was also tested against Anthonomus grandis, the cotton boll weevil aiming its control. The chitinase crude extract from the A8 strain was cultured for five days in a minimum liquid media supplemented with chitin. The extract was partially characterized by standard methods. The chitinolytic extract had an optimum temperature of 66 "C and an optimum pH between 4 to 9 (around 80% of relative activity). We also characterized the temperature and pH stability and measured the effects of enzyme inhibitors. The filtered chitinolytic extract was added to an artificial boll weevil diet. Boll weevil development from the egg stage to the adult stage was prolonged, and the percentage of adults that emerged was approximately 66% less than on control diet. This study showed that the.larval development of A. grandis was inhibited by the presence of characterized chitinolytic extract in artificial diet. This work provides an experimental basis for using the chitinase from an endophytic bacterium Streptomyces sp. as a biocontrol alternativeto controlling the plant pest A. grandis. 展开更多
关键词 Anthonomus grandis CHITINASE ENDOPHYTE STREPTOMYCES biocontrol.
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高校校园体育文化生态化建设研究 被引量:4
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作者 吴小茂 《环境科学与管理》 CAS 2018年第2期182-185,共4页
针对高校校园体育文化生态化建设的探讨,文中介绍了生态体育运动的必要性,这是高校校园体育文化生态化建设的基础,同时介绍了大学生对生态体育的认识,这是高校校园体育文化生态化建设的动力,最后给出了高校体育课生态化建设的目标,主要... 针对高校校园体育文化生态化建设的探讨,文中介绍了生态体育运动的必要性,这是高校校园体育文化生态化建设的基础,同时介绍了大学生对生态体育的认识,这是高校校园体育文化生态化建设的动力,最后给出了高校体育课生态化建设的目标,主要包括生态体育物质硬件建设,生态体育锻炼环境建设和体育行为生态化建设,对于高校校园体育文化生态化建设,只有做到这些,才能够使高校大学生,通过在高校校园体育文化生态化建设,使他们在身体素质上得到提高。 展开更多
关键词 针对高校校园体育文化生态化建设的探讨 文中介绍了生态体育运动的必要性 这是高校校园体育文化生态化建设的基础 同时介绍了大学生对生态体育的认识 这是高校校园体育文化生态化建设的动力 最后给出了高校体育课生态化建设的目标 主要包括生态体育物质硬件建设 生态体育锻炼环境建设和体育行为生态化建设 对于高校校园体育文化生态化建设 只有做到这些 才能够使高校大学生 通过在高校校园体育文化生态化建设 使他们在身体素质上得到提高校校园 体育文化 生态化建设
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慢·停·等
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作者 范俊强 《心理与健康》 2013年第1期31-31,共1页
上周三,同事开着车,我和他一块去省局上报单位的材料,没想到回来的路上发生了一个小插曲,让我感慨良久。当时车正在经五路上走着,由于路不平坦,加上时不时有逆行的人和自行车,同事开车的速度慢了下来,我们也乘机谈论起时下的一... 上周三,同事开着车,我和他一块去省局上报单位的材料,没想到回来的路上发生了一个小插曲,让我感慨良久。当时车正在经五路上走着,由于路不平坦,加上时不时有逆行的人和自行车,同事开车的速度慢了下来,我们也乘机谈论起时下的一些焦点新闻和某个明星的八卦,甚为惬意。在行至黄河路时, 展开更多
关键词 赶路 生活节奏 物质目标 交通灯
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