相射线Maslov求和法：一个完全的有限频率射线法

现有的有限频率射线方法,包括Maslov射线求和法和相射线法,只能部分地模拟菲涅耳干涉和介质非均匀性散射这两个影响有限频率波在非均匀介质传播的基本物理过程。为克服这些局限性,提出了一种新的有限频率射线方法。该方法融合了Maslov射线求和法和相射线法两者的长处,可以同时精确地模拟由菲涅耳干涉及介质非均匀性散射产生的有限频率波动现象,因此是一个完全的有限频率方法。此外,由于精确地描述了波场在焦散区附近由散射引起的波场平滑过程,也从根本上解决了渐近射线理论的奇异性问题。

X射线相定量法测单层分散阈值

本文简要介绍了自发单层分散现象及单层分散阈值效应 ,重点介绍了XRD(X光衍射 )

同轴法射线相衬成像的数值模拟计算与分析

对同轴法射线相衬成像进行数值模拟计算,可用于特定对象检测方法的可行性分析或检测参数优化。为此,分析了同轴法射线相衬成像系统数值模拟计算的原理及其实现方法,并针对圆形物体、长条形物体进行了相衬成像实验的数值模拟计算。对照计算结果进行分析可知:对物体平面进行离散化的尺寸很大程度上影响到数值模拟计算结果的准确程度,究其原因在于对物体平面进行离散化时决定了成像系统光学传递函数离散化的准确程度;为保证数值模拟结果的准确性,应使数值计算中光学传递函数取值点连续、不存在明显的失真;保证数值模拟结果准确所需的光学传递函数的离散化尺寸不是固定的,而是应与检测对象的大小相匹配。

粉末X射线衍射法测定氢气还原的气相醛加氢催化剂

采用粉末X射线衍射鉴定氢气还原的气相醛加氢催化剂中晶体物相并应用Scherrer法定量测定铜的晶粒尺寸。其晶体物相鉴定结果为:石墨、氧化锌、铜。采用化学计量学峰形拟合的方法计算铜(111)晶面晶粒尺寸约为10.3 nm,测定数据能够满足气相醛加氢催化剂研发的要求。

Carbothermic reduction of alumina with carbon in vacuum

Carbothermic reduction alumina in vacuum was conducted, and the products were analysed by means of XRD and gas chromatography. Thermodynamic analysis shows that in vacuum the initial carbothermic reduction reaction temperature reduces compared with that under normal pressure, and the preferential order of products is Al404C, Al4C3, Al2OC, Al20 and A1. Experiment results show that the carbothermic reduction products of alumina are A1404C and A14C3, and neither A12OC, Al20 or Al was found. During the carbothermic reduction process, the reaction rate of Al203 and carbon decreases gradually with increasing time. Meanwhile, lower system pressure or higher temperature is beneficial to the carbothermic reduction of alumina process. A1404C is firstly formed in the carbothermic reaction, and then A14C3 is formed in lower system pressure or at higher temperature.

Chinese Fuzzy Ontology Mapping Based on Support Vector Machine

Taking into account that fuzzy ontology mapping has wide application and cannot be dealt with in many fields at present,a Chinese fuzzy ontology model and a method for Chinese fuzzy ontology mapping are proposed.The mapping discovery between two ontologies is achieved by computing the similarity between the concepts of two ontologies.Every concept consists of four features of concept name,property,instance and structure.First,the algorithms of calculating four individual similarities corresponding to the four features are given.Secondly,the similarity vectors consisting of four weighted individual similarities are built,and the weights are the linear function of harmony and reliability.The similarity vector is used to represent the similarity relation between two concepts which belong to different fuzzy ontolgoies.Lastly,Support Vector Machine(SVM) is used to get the mapping concept pairs by the similarity vectors.Experiment results are satisfactory.

Cobalt-free gadolinium-doped perovskite Gd_xBa_(1-x)FeO_(3-δ) as high-performance materials for oxygen separation

Cobalt-free oxides GdxBal-xFeO3-σas（0.01 _〈 x _〈 0.1 ） were achieved by a solid state reaction method. It is found that GdxBal-xFeO3-σas（0.025 _〈 x _〈 0.1） exhibits the cubic perovskite structure. Among GdxBal-xFeO3-σas （0.025 -〈 x -〈 0.1 ）, the GdxBal-xFeO3-σas （GBF2.5） membrane shows the outstanding phase structure stability and the highest oxygen permeation, which can reach 1.44 ml. cm- 2. rain- 1 at 950 ℃ under air/He oxygen partial pressure gradient. The GBF2.5 membrane was successfully operated for more than 100 h at 800 ℃ and the oxygen permeation flux through the membrane is 0.62 ml. cm- 2. rain- 1. After 100 h oxygen permeation experiment at 800℃, X-ray diffraction （XRD） and energy dispersive X-ray spectrometer （EDXS） demonstrate that the GBF2.5 exhibits phase structure stability even at intermediate temoerature.

Anti-interference method for HF radars by transmitting phase-modulated chirps

Radio frequency interference （RFI） is a major problem in high-frequency （HF） radars. Conventional filtering-involved RFI suppression methods may introduce distortions to the target signals of interest and often demand extra hardware costs. In this paper, a novel method for RFI suppression by using linearly or randomly phase-modulated （PM） chirps is proposed, which enables independent analyses of the target signal and the RFI. Furthermore, the directions of arrival （DOA） of the interference are used as constraints to ensure a better DOA estimation of the target. The effectiveness of the method is demonstrated by numerical simulation results. The method can greatly improve the anti-interference capabilities of HF radars and is extremely applicable in the portable and low-cost radar systems.

X-ray pulsar-based navigation using pulse phase and Doppler frequency measurements

In order to eliminate the impact of the Doppler effects caused by the motion of the spacecraft on the X-ray pulsar-based navigation, an innovative navigation method using the pulse phase and Doppler frequency measurements of the X-ray pulsars is proposed. Given the initial estimate of the spacecraft's state,the real-time photon arrival model is established at the spacecraft with respect to the spacecraft's position and velocity predicted by the orbit dynamic model and their estimation errors. On this basis, a maximum likelihood estimation algorithm directly using the observed photon event timestamps is developed to extract a single pair of pulse phase and Doppler frequency measurements caused by the spacecraft's state estimation error. Since the phase estimation error increases as the observation time increases, we propose a new measurement updating scheme of referring the measurements to the middle time of an observation interval. By using the ground-based simulation system of X-ray pulsar signals, a series of photon-level simulations are performed. The results testify to the feasibility and real-timeliness of the proposed navigation method, and show that the incorporation of the Doppler measurement as well as the pulse phase into the navigation filter can improve the navigation accuracy.