阿尔茨海默病(Alzheimer’s disease, AD)的中医认识历史悠久,历代医家对本病的病因病机有不同的认识,随着AD的病因病机研究不断深入,我国医学专家对AD的病因病机把握越来越明晰。对AD的探讨研究发现,AD的病因病机主要包括髓海不足说、...阿尔茨海默病(Alzheimer’s disease, AD)的中医认识历史悠久,历代医家对本病的病因病机有不同的认识,随着AD的病因病机研究不断深入,我国医学专家对AD的病因病机把握越来越明晰。对AD的探讨研究发现,AD的病因病机主要包括髓海不足说、脾肾互赞说、痰浊蒙窍说、毒损脑络说、肝肠脑相维说等,这些学说各有理论依据及临床意义,但仍有不足之处有待商榷和补充,本文结合先贤所执之见,对AD的病因和病机进行了全面的梳理和归纳总结,以期为后续临床的诊疗提供参考。The understanding of Alzheimer’s disease (AD) in traditional Chinese medicine has a long history. Doctors of all ages have different understandings of the etiology and pathogenesis of this disease. With the deepening of the research on the etiology and pathogenesis of AD, Chinese medical experts have become more and more clear about the etiology and pathogenesis of AD. The study of AD found that the etiology and pathogenesis of AD mainly include the theory of marrow sea deficiency, the theory of spleen and kidney mutual praise, the theory of phlegm turbidity, the theory of poison damage to brain collaterals, and the theory of liver, intestine and brain. These theories have their own theoretical basis and clinical significance, but there are still deficiencies to be discussed and supplemented. In this paper, combined with the views of the sages, the etiology and pathogenesis of AD are comprehensively sorted out and reviewed in depth. The purpose is to establish a set of unified efficacy evaluation indicators, so as to improve the clinical treatment effect, and provide a new idea for the clinical diagnosis and treatment of AD in traditional Chinese medicine.展开更多
Based on the Hirota bilinear method,this study derived N-soliton solutions,breather solutions,lump solutions and interaction solutions for the(2+1)-dimensional extended Boiti-Leon-Manna-Pempinelli equation.The dynamic...Based on the Hirota bilinear method,this study derived N-soliton solutions,breather solutions,lump solutions and interaction solutions for the(2+1)-dimensional extended Boiti-Leon-Manna-Pempinelli equation.The dynamical characteristics of these solutions were displayed through graphical,particularly revealing fusion and ssion phenomena in the interaction of lump and the one-stripe soliton.展开更多
The improvement of the heat transfer rate of phase change material(PCM)is studied by mixing with carbon fiber(CF)which is a good heat conductor.The composite PCM is prepared by blending CF and n-Docosane and its t...The improvement of the heat transfer rate of phase change material(PCM)is studied by mixing with carbon fiber(CF)which is a good heat conductor.The composite PCM is prepared by blending CF and n-Docosane and its thermal performance is tested using the method of differential scanning calorimetry(DSC)analysis and thermogravimetric/differential thermal analysis(TG/DTA).In addition,the influence of the mixing amount and the length of CF on the thermal conductivity of n-Docosane are investigated.The results show that CF can significantly improve the heat transfer rate of n-Docosane,and the mixing amount and the length of CF are two influence factors.The heat storage and release rates increase with the increase in the mixing amount of CF.Moreover,the melting point of n-Docosane is increased from 40.2 to 50.8 ℃ after being mixed with CF.The heating time is decreased from 720 to 660 s by mixing with 6% of CF,and is decreased to 600 s by mixing with 10% of CF.展开更多
Different from the previous qualitative analysis of linear systems in time and frequency domains, the method for describing nonlinear systems quantitatively is proposed based on correlated dimensions. Nonlinear dynami...Different from the previous qualitative analysis of linear systems in time and frequency domains, the method for describing nonlinear systems quantitatively is proposed based on correlated dimensions. Nonlinear dynamics theory is used to analyze the pressure data of a contrarotating axial flow fan. The delay time is 18 and the embedded dimension varies from 1 to 25 through phase-space reconstruction. In addition, the correlated dimensions are calculated before and after stalling. The results show that the correlated dimensions drop from 1. 428 before stalling to 1. 198 after stalling, so they are sensitive to the stalling signal of the fan and can be used as a characteristic quantity for the judging of the fan stalling.展开更多
A new method for simultaneous determination of four phthalate esters ( PAEs) in commercial fat-containing foods was developed by the combination of a packed nanofibers column based on solid-phase extraction with gas...A new method for simultaneous determination of four phthalate esters ( PAEs) in commercial fat-containing foods was developed by the combination of a packed nanofibers column based on solid-phase extraction with gas chromatography-flame ionization detector ( GC-FID ). Conditions for obtaining optimum extraction efficiency such as extraction solvents, morphologies of adsorbent, ion strength and pH were investigated and optimized in detail. Under the optimized conditions, the limits of detection (LODs) found for dibutyl phthalate (DBP) , butyl benzyl phthalate (BBP), diethyl hexyl phthalate (DEHP) and di-n-octyl phthalate (DNOP) were 50, 25, 50 and 25 ng/g, respectively. Good linearity of four PAEs was achieved in the range of 50 to 4 000 ng/g. The proposed method was applied for analyzing different kinds of fat-containing samples. PAEs in commercial fat-containing samples can be highly extracted by a packed solid-phase extraction column of 5 mg polystyrene ( PS) nanofibers. The satisfactory average recoveries were obtained in the range of 96. 7% to 102. 3% , and the relative standard deviations (RSDs) below 5% were achieved. The proposed method reduces the organic solvent consumption, the complex and tedious procedures for sample pretreatment, and achieves high sensitivity and reproducibility for the investigated PAEs.展开更多
To consider the reliability and performance of electronic devices based on polyimide derivatives, dynamic water sorption and diffusion behavior in a polyimide derivative: poly(4'4 oxydiphenylene pyromellitimide) ...To consider the reliability and performance of electronic devices based on polyimide derivatives, dynamic water sorption and diffusion behavior in a polyimide derivative: poly(4'4 oxydiphenylene pyromellitimide) (PMDA-ODA)/silica nanocomposite was investigated by two-dimensional ATR-FTIR spectroscopy, by which three states of water molecules owning different H-bonding strength were distinguished. The amounts and strength of H-bonding also played a significant role in determining the diffusion rate of the different states of water molecules. The type of aggregated water molecules which also formed H-bonding with silicic acid (residues) or polyimide system was the last one diffusing to the polymer side in contact with the ATR crystal element because the polymeric matrix blocked their diffusion to a great extent. The diffusion coefficient was also estimated to gain the information of the dynamic diffusion behavior.展开更多
Ni-Mn-In-Co microwires with diameter of 30-100 μm are prepared by glass-coated metal filaments(Taylor–Ulitovsky) method. The effects of magnetic field on martensite transformation temperature in the as-prepared an...Ni-Mn-In-Co microwires with diameter of 30-100 μm are prepared by glass-coated metal filaments(Taylor–Ulitovsky) method. The effects of magnetic field on martensite transformation temperature in the as-prepared and annealed microwires are investigated using a physical property measurement system(PPMS). Magnetocaloric effect(MCE) attributed to field-induced austenite transformation in the as-prepared and annealed microwires is analyzed indirectly from the isothermal magnetization(M-B) curves. The as-prepared microwire has a 7-layer modulated martensite structure(7M) at room temperature. The changes of austenite starting temperature induced by an external magnetic field(ΔAs/ΔB) in the as-prepared and annealed microwires are-1.6 and-4 K/T, respectively. Inverse martensite to austenite transformation exists in annealed microwires when an external magnetic field is applied at temperatures near As. The entropy change(ΔS) obtained in the annealed microwires is 3.0 J/(kg·K), which is much larger than that in the as-prepared microwires 0.5 J/(kg·K). The large entropy change and low price make Ni-Mn-In-Co microwires a potential working material in magnetic refrigeration.展开更多
Viscose activated carbon fibers (ACFs) were characterized using specific surface area, scanning electron modified with chemical vapor deposition (CVD). The samples were microscopy (SEM), pore size distribution a...Viscose activated carbon fibers (ACFs) were characterized using specific surface area, scanning electron modified with chemical vapor deposition (CVD). The samples were microscopy (SEM), pore size distribution and Fourier transform infrared spectroscopy (FTIR). Batch adsorption experiments were carried out to investigate the adsorption behavior of modified ACFs for methyl orange(MO) from its aqueous solutions. The results show that the adsorption isotherms of MO onto modified ACFs well follows the Langmuir isotherm equation. The adsorption kinetics of MO can be well described by the pseudo second-order kinetic model. The adsorption process involves the intra-particle diffusion, but is not the only rate-controlling step. Thermodynamic parameters including AG, AH and AS were calculated, suggesting that the adsorption of MO onto modified ACFs is a spontaneous, exothermic and physisorption process. FTIR result indicates that the major adsorption mechanism of modified ACFs for MO is hydrogen bond.展开更多
[Objective] This study aimed to establish a determination method for iprobenfos residue in rice straw and husked rice. [Method] The rice straw and husked rice samples were extracted by acetone-ethyl acetate mixed solv...[Objective] This study aimed to establish a determination method for iprobenfos residue in rice straw and husked rice. [Method] The rice straw and husked rice samples were extracted by acetone-ethyl acetate mixed solvent. The extracts were purified using SPE C18 column and SPE NH2 column, and the iprobenfos residues were determined by GC-FTD. [Result] In the concentration range of 0.005-5.0 mg/kg, iprobenfos concentration showed a good linear relationship with peak area (r=0.999 8). When the iprobenfos concentrations were 0.01, 0.1 and 1.0 mg/kg respectively, the recoveries of added iprobenfos from rice straw ranged from 72.6% to 99.7% with relative standard deviation ranging from 5.65% to 8.48%; the recoveries of added iprobenfos from husked rice ranged from 81.6% to 97.6% with relative standard deviation ranging from 3.74% to 7.63%. The minimum detectable quantity of iprobenfos was 5×10^-12 g, and the minimum detectable concentrations of iprobenfos in rice straw and husked rice samples were 2.0 and 0.5 μg/kg, respec- tively. [Conclusion] The established determination method is characterized by low de- termination limit, high sensitivity, good reproducibility and high operability, which all meet the requirements by Guideline on Pesticide Residue Trials of the Ministry of Agriculture.展开更多
Locoweed is a poisonous plant wildly distributed in most areas of the world,which causes livestock poisoning or death with serious economic loss.The Astragalus strictus belongs to a species of Iocoweed.It is mainly di...Locoweed is a poisonous plant wildly distributed in most areas of the world,which causes livestock poisoning or death with serious economic loss.The Astragalus strictus belongs to a species of Iocoweed.It is mainly distributed in Tibet of China and is a serious hazard to the local livestock industry.The objective of this study is extracting and purifying condition of Swainsonine from Astragalus strictus with the cellulase extraction method.An optimum extracting technology of SW from Astragalus strictus was investigated through the orthogonal experiment under the cellulose assistance conditions,and then the content of swainsonine was analyzed with gas chromatography (GC) method.The optimized extraction conditions were as follow:The crushed mesh is 40; solid-liquid ratio is 1∶40 (g/ml); enzyme dosage is 3.5%; enzymatic time is 3 h.Under the above conditions,the extraction percentage of the swainsonine was 0.003 941%.The conditions for extracting swainsonine with cellulase extraction method are mild,it is easy to utilize industrial production.It is benefit for producing swainsonine from Astragalus strictus.展开更多
This paper presents a comprehensive treatment of the parametric sensitivity and runaway in fixed bed reactors with one dimensional pseudo homogeneous dispersion model (ODDM). In this case, we find the existence of m...This paper presents a comprehensive treatment of the parametric sensitivity and runaway in fixed bed reactors with one dimensional pseudo homogeneous dispersion model (ODDM). In this case, we find the existence of multiplicity and determine the runaway criterion through the critical isodisper sion curve. The calculated results indicate when the axial dispersion is relatively small, the impact of the axial dispersion on the parametric sensitivity may be neglected; but when the axial dispersion is large, this impact must be considered.展开更多
In order to study the correlations among quality indexes of tobacco leaf and contents of cellulose and lignin in upper leaves of flue-cured tobacco, 48 B2F flue-cured tobacco samples in seven counties of Wulin mountai...In order to study the correlations among quality indexes of tobacco leaf and contents of cellulose and lignin in upper leaves of flue-cured tobacco, 48 B2F flue-cured tobacco samples in seven counties of Wulin mountain area in 2011 and 2012 were used as test materials to measure the contents of cellulose and lignin in tobacco leaves and analyze the differences among varieties and between years. Meanwhile, correlations among contents of cellulose and lignin and appearance quality, physical characteristics, general chemical components and indexes of senso- ry quality were studied. The results showed that the contents of cellulose and lignin had no significant difference among years and varieties. Cellulose content was sig- nificantly correlated with some indexes of appearance qualities, physical indexes, general chemical compositions and sensory qualities. Lignin content was significantly correlated with grayness and oil content but not other quality indexes of tobacco leaf. It could be seen that the differences of cellulose and lignin contents between different years and among varieties were not significant. Cellulose content was closely correlated with quality indexes of tobacco leaf while lignin content had a small effect on tobacco leaf quality.展开更多
A procedure of low temperature solid-phase sintering(LTSS) was carried out to fabricate sintered metal fibrous media(SMFM) with high specific surface area.Stainless steel fibers which were produced by cutting proc...A procedure of low temperature solid-phase sintering(LTSS) was carried out to fabricate sintered metal fibrous media(SMFM) with high specific surface area.Stainless steel fibers which were produced by cutting process were first plated with a coarse copper coating layer by electroless plating process.A low-temperature sintering process was then completed at about 800 °C for 1 h under the protection of hydrogen atmosphere.The results show that a novel SMFM with complex surface morphology and high specific surface area(0.2 m2/g) can be obtained in this way.The effect of sintering temperature on the surface morphology and specific surface area of SMFM was studied by means of scanning electron microscopy and Brunauer-Emmett-Teller.The damage of micro-structure during the sintering process mainly contributed to the loss of specific surface area of SMFM and the optimal sintering temperature was 800 °C.展开更多
Beam focusing is one of the unique characteristics of ultrasonic phased array compared with conventional ultrasound.On the basis of two-dimensional radiated sound field of phased array,the three-dimensional radiated s...Beam focusing is one of the unique characteristics of ultrasonic phased array compared with conventional ultrasound.On the basis of two-dimensional radiated sound field of phased array,the three-dimensional radiated sound field was simulated in the paper,and then the effect of different frequencies,different number of array elements and different element spacings on focal spot,the depth of focus and the effect on horizontal and vertical resolution were analyzed.The optimal results of transducer parameters have certain reference value for the design of phased array probe.展开更多
For classifying unknown 3-D objects into a set of predetermined object classes, a part-level object classification method based on the improved interpretation tree is presented. The part-level representation is implem...For classifying unknown 3-D objects into a set of predetermined object classes, a part-level object classification method based on the improved interpretation tree is presented. The part-level representation is implemented, which enables a more compact shape description of 3-D objects. The proposed classification method consists of two key processing stages: the improved constrained search on an interpretation tree and the following shape similarity measure computation. By the classification method, both whole match and partial match with shape similarity ranks are achieved; especially, focus match can be accomplished, where different key parts may be labeled and all the matched models containing corresponding key parts may be obtained. A series of experiments show the effectiveness of the presented 3-D object classification method.展开更多
Surface electromyogram (EMG) signals were identified by fractal dimension.Two patterns of surface EMG signals were acquired from 30 healthy volunteers' right forearm flexor respectively in the process of forearm su...Surface electromyogram (EMG) signals were identified by fractal dimension.Two patterns of surface EMG signals were acquired from 30 healthy volunteers' right forearm flexor respectively in the process of forearm supination (FS) and forearm pronation (FP).After the raw action surface EMG (ASEMG) signal was decomposed into several sub-signals with wavelet packet transform (WPT),five fractal dimensions were respectively calculated from the raw signal and four sub-signals by the method based on fuzzy self-similarity.The results show that calculated from the sub-signal in the band 0 to 125 Hz,the fractal dimensions of FS ASEMG signals and FP ASEMG signals distributed in two different regions,and its error rate based on Bayes decision was no more than 2.26%.Therefore,the fractal dimension is an appropriate feature by which an FS ASEMG signal is distinguished from an FP ASEMG signal.展开更多
文摘阿尔茨海默病(Alzheimer’s disease, AD)的中医认识历史悠久,历代医家对本病的病因病机有不同的认识,随着AD的病因病机研究不断深入,我国医学专家对AD的病因病机把握越来越明晰。对AD的探讨研究发现,AD的病因病机主要包括髓海不足说、脾肾互赞说、痰浊蒙窍说、毒损脑络说、肝肠脑相维说等,这些学说各有理论依据及临床意义,但仍有不足之处有待商榷和补充,本文结合先贤所执之见,对AD的病因和病机进行了全面的梳理和归纳总结,以期为后续临床的诊疗提供参考。The understanding of Alzheimer’s disease (AD) in traditional Chinese medicine has a long history. Doctors of all ages have different understandings of the etiology and pathogenesis of this disease. With the deepening of the research on the etiology and pathogenesis of AD, Chinese medical experts have become more and more clear about the etiology and pathogenesis of AD. The study of AD found that the etiology and pathogenesis of AD mainly include the theory of marrow sea deficiency, the theory of spleen and kidney mutual praise, the theory of phlegm turbidity, the theory of poison damage to brain collaterals, and the theory of liver, intestine and brain. These theories have their own theoretical basis and clinical significance, but there are still deficiencies to be discussed and supplemented. In this paper, combined with the views of the sages, the etiology and pathogenesis of AD are comprehensively sorted out and reviewed in depth. The purpose is to establish a set of unified efficacy evaluation indicators, so as to improve the clinical treatment effect, and provide a new idea for the clinical diagnosis and treatment of AD in traditional Chinese medicine.
基金Supported by the National Natural Science Foundation of China(12275172)。
文摘Based on the Hirota bilinear method,this study derived N-soliton solutions,breather solutions,lump solutions and interaction solutions for the(2+1)-dimensional extended Boiti-Leon-Manna-Pempinelli equation.The dynamical characteristics of these solutions were displayed through graphical,particularly revealing fusion and ssion phenomena in the interaction of lump and the one-stripe soliton.
基金The National Natural Science Foundation of China(No.50808042)the National Key Technology R&D Program of China during the 11th Five-Year Plan Period(No.2007BA000875-04)+2 种基金Six Projects Sponsoring Talent Summits of Jiangsu Province,Outstanding Young Teacher Funding Schemes of Southeast UniversityOpen Fund of Key Laboratory of Inorganic and Composite Materials of Jiangsu Province(No.wjjqfhxcl200703)the Scientific Research Foundation for the Returned Overseas Chinese Scholars,State Education Ministry
文摘The improvement of the heat transfer rate of phase change material(PCM)is studied by mixing with carbon fiber(CF)which is a good heat conductor.The composite PCM is prepared by blending CF and n-Docosane and its thermal performance is tested using the method of differential scanning calorimetry(DSC)analysis and thermogravimetric/differential thermal analysis(TG/DTA).In addition,the influence of the mixing amount and the length of CF on the thermal conductivity of n-Docosane are investigated.The results show that CF can significantly improve the heat transfer rate of n-Docosane,and the mixing amount and the length of CF are two influence factors.The heat storage and release rates increase with the increase in the mixing amount of CF.Moreover,the melting point of n-Docosane is increased from 40.2 to 50.8 ℃ after being mixed with CF.The heating time is decreased from 720 to 660 s by mixing with 6% of CF,and is decreased to 600 s by mixing with 10% of CF.
基金Supported by the Natural Science Foundation of Jiangsu Province(BK2005018)the Graduate Research and Innovation Plan of Jiangsu Province(CX07B-061Z)~~
文摘Different from the previous qualitative analysis of linear systems in time and frequency domains, the method for describing nonlinear systems quantitatively is proposed based on correlated dimensions. Nonlinear dynamics theory is used to analyze the pressure data of a contrarotating axial flow fan. The delay time is 18 and the embedded dimension varies from 1 to 25 through phase-space reconstruction. In addition, the correlated dimensions are calculated before and after stalling. The results show that the correlated dimensions drop from 1. 428 before stalling to 1. 198 after stalling, so they are sensitive to the stalling signal of the fan and can be used as a characteristic quantity for the judging of the fan stalling.
基金The National Basic Research Program of China(973Program)(No.2012CB933302)the National Instrumental Research Program(No.2014YQ06077303)+1 种基金the National Natural Science Foundation of China(No.81172720,21307086)Suzhou Science and Technology Department Foundation(No.ZXG201441)
文摘A new method for simultaneous determination of four phthalate esters ( PAEs) in commercial fat-containing foods was developed by the combination of a packed nanofibers column based on solid-phase extraction with gas chromatography-flame ionization detector ( GC-FID ). Conditions for obtaining optimum extraction efficiency such as extraction solvents, morphologies of adsorbent, ion strength and pH were investigated and optimized in detail. Under the optimized conditions, the limits of detection (LODs) found for dibutyl phthalate (DBP) , butyl benzyl phthalate (BBP), diethyl hexyl phthalate (DEHP) and di-n-octyl phthalate (DNOP) were 50, 25, 50 and 25 ng/g, respectively. Good linearity of four PAEs was achieved in the range of 50 to 4 000 ng/g. The proposed method was applied for analyzing different kinds of fat-containing samples. PAEs in commercial fat-containing samples can be highly extracted by a packed solid-phase extraction column of 5 mg polystyrene ( PS) nanofibers. The satisfactory average recoveries were obtained in the range of 96. 7% to 102. 3% , and the relative standard deviations (RSDs) below 5% were achieved. The proposed method reduces the organic solvent consumption, the complex and tedious procedures for sample pretreatment, and achieves high sensitivity and reproducibility for the investigated PAEs.
基金supported by the National Natural Science Foundation of China(No.20573022,No.20425415)the National Basic Research Pro-gram of China(2005CB623800),the PHD Program of M0E(20050246010)the"Qimingxing"Project(No.04QM1402)of Shanghai Municipal Science and Technology Commission,and the"Shuguang"Project(No.01SG05)of the Shanghai Municipal Education Commission and Shanghai Education Development Foundation.
文摘To consider the reliability and performance of electronic devices based on polyimide derivatives, dynamic water sorption and diffusion behavior in a polyimide derivative: poly(4'4 oxydiphenylene pyromellitimide) (PMDA-ODA)/silica nanocomposite was investigated by two-dimensional ATR-FTIR spectroscopy, by which three states of water molecules owning different H-bonding strength were distinguished. The amounts and strength of H-bonding also played a significant role in determining the diffusion rate of the different states of water molecules. The type of aggregated water molecules which also formed H-bonding with silicic acid (residues) or polyimide system was the last one diffusing to the polymer side in contact with the ATR crystal element because the polymeric matrix blocked their diffusion to a great extent. The diffusion coefficient was also estimated to gain the information of the dynamic diffusion behavior.
基金Project(51001038)supported by the National Natural Science Foundation of China
文摘Ni-Mn-In-Co microwires with diameter of 30-100 μm are prepared by glass-coated metal filaments(Taylor–Ulitovsky) method. The effects of magnetic field on martensite transformation temperature in the as-prepared and annealed microwires are investigated using a physical property measurement system(PPMS). Magnetocaloric effect(MCE) attributed to field-induced austenite transformation in the as-prepared and annealed microwires is analyzed indirectly from the isothermal magnetization(M-B) curves. The as-prepared microwire has a 7-layer modulated martensite structure(7M) at room temperature. The changes of austenite starting temperature induced by an external magnetic field(ΔAs/ΔB) in the as-prepared and annealed microwires are-1.6 and-4 K/T, respectively. Inverse martensite to austenite transformation exists in annealed microwires when an external magnetic field is applied at temperatures near As. The entropy change(ΔS) obtained in the annealed microwires is 3.0 J/(kg·K), which is much larger than that in the as-prepared microwires 0.5 J/(kg·K). The large entropy change and low price make Ni-Mn-In-Co microwires a potential working material in magnetic refrigeration.
基金Project (50802115) supported by the National Natural Science Foundation of ChinaProject (2010FJ4075) supported by Science and Technology Planning Project of Hunan Province, China+1 种基金Project (CDJJ-10010205) supported by the Science Foundation of Changsha University, ChinaProject supported by the Construct Program of the Key Discipline in Hunan Province, China
文摘Viscose activated carbon fibers (ACFs) were characterized using specific surface area, scanning electron modified with chemical vapor deposition (CVD). The samples were microscopy (SEM), pore size distribution and Fourier transform infrared spectroscopy (FTIR). Batch adsorption experiments were carried out to investigate the adsorption behavior of modified ACFs for methyl orange(MO) from its aqueous solutions. The results show that the adsorption isotherms of MO onto modified ACFs well follows the Langmuir isotherm equation. The adsorption kinetics of MO can be well described by the pseudo second-order kinetic model. The adsorption process involves the intra-particle diffusion, but is not the only rate-controlling step. Thermodynamic parameters including AG, AH and AS were calculated, suggesting that the adsorption of MO onto modified ACFs is a spontaneous, exothermic and physisorption process. FTIR result indicates that the major adsorption mechanism of modified ACFs for MO is hydrogen bond.
基金Supported by Pesticide Registration Residual Test of Institute for the Control of Agrochemicals,Ministry of Agriculture(2013F216)~~
文摘[Objective] This study aimed to establish a determination method for iprobenfos residue in rice straw and husked rice. [Method] The rice straw and husked rice samples were extracted by acetone-ethyl acetate mixed solvent. The extracts were purified using SPE C18 column and SPE NH2 column, and the iprobenfos residues were determined by GC-FTD. [Result] In the concentration range of 0.005-5.0 mg/kg, iprobenfos concentration showed a good linear relationship with peak area (r=0.999 8). When the iprobenfos concentrations were 0.01, 0.1 and 1.0 mg/kg respectively, the recoveries of added iprobenfos from rice straw ranged from 72.6% to 99.7% with relative standard deviation ranging from 5.65% to 8.48%; the recoveries of added iprobenfos from husked rice ranged from 81.6% to 97.6% with relative standard deviation ranging from 3.74% to 7.63%. The minimum detectable quantity of iprobenfos was 5×10^-12 g, and the minimum detectable concentrations of iprobenfos in rice straw and husked rice samples were 2.0 and 0.5 μg/kg, respec- tively. [Conclusion] The established determination method is characterized by low de- termination limit, high sensitivity, good reproducibility and high operability, which all meet the requirements by Guideline on Pesticide Residue Trials of the Ministry of Agriculture.
文摘Locoweed is a poisonous plant wildly distributed in most areas of the world,which causes livestock poisoning or death with serious economic loss.The Astragalus strictus belongs to a species of Iocoweed.It is mainly distributed in Tibet of China and is a serious hazard to the local livestock industry.The objective of this study is extracting and purifying condition of Swainsonine from Astragalus strictus with the cellulase extraction method.An optimum extracting technology of SW from Astragalus strictus was investigated through the orthogonal experiment under the cellulose assistance conditions,and then the content of swainsonine was analyzed with gas chromatography (GC) method.The optimized extraction conditions were as follow:The crushed mesh is 40; solid-liquid ratio is 1∶40 (g/ml); enzyme dosage is 3.5%; enzymatic time is 3 h.Under the above conditions,the extraction percentage of the swainsonine was 0.003 941%.The conditions for extracting swainsonine with cellulase extraction method are mild,it is easy to utilize industrial production.It is benefit for producing swainsonine from Astragalus strictus.
文摘This paper presents a comprehensive treatment of the parametric sensitivity and runaway in fixed bed reactors with one dimensional pseudo homogeneous dispersion model (ODDM). In this case, we find the existence of multiplicity and determine the runaway criterion through the critical isodisper sion curve. The calculated results indicate when the axial dispersion is relatively small, the impact of the axial dispersion on the parametric sensitivity may be neglected; but when the axial dispersion is large, this impact must be considered.
基金Supported by"Ecological Basic Research of Good Quality Tobacco Leaf with Middle Odor Type"of Major Special Project of China Tobacco Corporation for Tobacco Leaf with Good Quality(TS-02-20110012)~~
文摘In order to study the correlations among quality indexes of tobacco leaf and contents of cellulose and lignin in upper leaves of flue-cured tobacco, 48 B2F flue-cured tobacco samples in seven counties of Wulin mountain area in 2011 and 2012 were used as test materials to measure the contents of cellulose and lignin in tobacco leaves and analyze the differences among varieties and between years. Meanwhile, correlations among contents of cellulose and lignin and appearance quality, physical characteristics, general chemical components and indexes of senso- ry quality were studied. The results showed that the contents of cellulose and lignin had no significant difference among years and varieties. Cellulose content was sig- nificantly correlated with some indexes of appearance qualities, physical indexes, general chemical compositions and sensory qualities. Lignin content was significantly correlated with grayness and oil content but not other quality indexes of tobacco leaf. It could be seen that the differences of cellulose and lignin contents between different years and among varieties were not significant. Cellulose content was closely correlated with quality indexes of tobacco leaf while lignin content had a small effect on tobacco leaf quality.
基金Project (50930005) supported by the National Natural Science Foundation of ChinaProject (U0834002) supported by the Key Programof NSFC-Guangdong Joint Funds of China+1 种基金Project (LYM09024) supported by Training Program for Excellent Young Teachers withInnovation of Guangdong University, ChinaProject (2009ZM0121) supported by the Fundamental Research Funds for the CentralUniversities of South China University of Technology,China
文摘A procedure of low temperature solid-phase sintering(LTSS) was carried out to fabricate sintered metal fibrous media(SMFM) with high specific surface area.Stainless steel fibers which were produced by cutting process were first plated with a coarse copper coating layer by electroless plating process.A low-temperature sintering process was then completed at about 800 °C for 1 h under the protection of hydrogen atmosphere.The results show that a novel SMFM with complex surface morphology and high specific surface area(0.2 m2/g) can be obtained in this way.The effect of sintering temperature on the surface morphology and specific surface area of SMFM was studied by means of scanning electron microscopy and Brunauer-Emmett-Teller.The damage of micro-structure during the sintering process mainly contributed to the loss of specific surface area of SMFM and the optimal sintering temperature was 800 °C.
基金National Natural Science Foundation of China(No.61201412)Shanxi Province Fundation for Science and Technology Research(No.2012021011-5)Program for Top Young Academic Leaders of Higher Learning Institution in Shanxi Province
文摘Beam focusing is one of the unique characteristics of ultrasonic phased array compared with conventional ultrasound.On the basis of two-dimensional radiated sound field of phased array,the three-dimensional radiated sound field was simulated in the paper,and then the effect of different frequencies,different number of array elements and different element spacings on focal spot,the depth of focus and the effect on horizontal and vertical resolution were analyzed.The optimal results of transducer parameters have certain reference value for the design of phased array probe.
基金The National Basic Research Program of China(973Program)(No2006CB303105)the Research Foundation of Bei-jing Jiaotong University (NoK06J0170)
文摘For classifying unknown 3-D objects into a set of predetermined object classes, a part-level object classification method based on the improved interpretation tree is presented. The part-level representation is implemented, which enables a more compact shape description of 3-D objects. The proposed classification method consists of two key processing stages: the improved constrained search on an interpretation tree and the following shape similarity measure computation. By the classification method, both whole match and partial match with shape similarity ranks are achieved; especially, focus match can be accomplished, where different key parts may be labeled and all the matched models containing corresponding key parts may be obtained. A series of experiments show the effectiveness of the presented 3-D object classification method.
基金The National Natural Science Foundation of China(No.60171006)the National Basic Research Programof China (973 Pro-gram) (No.2005CB724303).
文摘Surface electromyogram (EMG) signals were identified by fractal dimension.Two patterns of surface EMG signals were acquired from 30 healthy volunteers' right forearm flexor respectively in the process of forearm supination (FS) and forearm pronation (FP).After the raw action surface EMG (ASEMG) signal was decomposed into several sub-signals with wavelet packet transform (WPT),five fractal dimensions were respectively calculated from the raw signal and four sub-signals by the method based on fuzzy self-similarity.The results show that calculated from the sub-signal in the band 0 to 125 Hz,the fractal dimensions of FS ASEMG signals and FP ASEMG signals distributed in two different regions,and its error rate based on Bayes decision was no more than 2.26%.Therefore,the fractal dimension is an appropriate feature by which an FS ASEMG signal is distinguished from an FP ASEMG signal.