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白及真空冻干法与烘干法工艺条件优化对比 被引量:3
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作者 饶文霞 张敏 +3 位作者 林菁 张开元 周康 尹鸿翔 《黑龙江农业科学》 2019年第4期81-85,共5页
为考察白及饮片最佳干燥工艺,并为其他中药饮片干燥工艺的现代研究提供借鉴。采用变温电阻检测法测定白及共晶点;通过测量白及饮片在蒸制切片和生切片、厚度0.1和0.2 cm、烘干和真空冻干等8种工艺条件组合下的白及多糖含量及特性黏数,... 为考察白及饮片最佳干燥工艺,并为其他中药饮片干燥工艺的现代研究提供借鉴。采用变温电阻检测法测定白及共晶点;通过测量白及饮片在蒸制切片和生切片、厚度0.1和0.2 cm、烘干和真空冻干等8种工艺条件组合下的白及多糖含量及特性黏数,进一步测定饮片折干率,绘制折干率曲线,优选最佳因素,同时进行感官品质对比,确定出白及饮片的最佳干燥工艺。结果表明:白及饮片共晶点为-11.6℃;真空冻干法优化条件为0.2 cm生切片,-25℃预冻2 h后采用真空冻干(-45℃0.28 MPa)4 h,该饮片色泽洁白,片形平整,断面特征完好,感官品质最佳,适用于处方饮片;烘干法优化条件为0.2 cm蒸制切片,60℃恒温烘干2 h,该饮片虽然感官品质较差,但是多糖含量和特性黏数最高,适用于药厂投料。本文首次报道了白及共晶点,并确定了白及饮片两种干燥模式的最佳工艺条件,为《中国药典》白及标准的进一步完善,提供了重要的参考数据。 展开更多
关键词 白及 真空冻干法 干法 共晶点 白及多糖 特性黏数
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真空冻干法精制精氨酸
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作者 张铁红 《黑龙江科技信息》 2004年第6期244-244,共1页
本文研究以真空冻干法精制精氨酸的新工艺,以提高产量降低成本。
关键词 真空冻干法 精制 精氨酸 助溶剂 注射用药
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Optimization of pectin extraction and antioxidant activities from Jerusalem artichoke 被引量:5
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作者 刘胜一 史雪洁 +1 位作者 徐兰兰 衣悦涛 《Chinese Journal of Oceanology and Limnology》 SCIE CAS CSCD 2016年第2期372-381,共10页
Jerusalem artichoke is an economic crop widely planted in saline-alkaline soil. The use of Jerusalem artichoke is of great significance. In this study, the response surface method was employed to optimize the effects ... Jerusalem artichoke is an economic crop widely planted in saline-alkaline soil. The use of Jerusalem artichoke is of great significance. In this study, the response surface method was employed to optimize the effects of processing variables (extraction temperature, pH, extraction time, and liquid-to- solid ratio) on the yield of Jerusalem artichoke pectin. Under the optimal extraction conditions: pHl .52, 63.62 min, 100℃ and a liquid-to-solid ratio of 44.4 mL/g, the maximum pectin yield was predicted to be 18.76%. Experiments were conducted under these optimal conditions and a pectin yield of 18.52+0.90% was obtained, which validated the model prediction. The effects of different drying methods (freeze drying, spray drying and vacuum drying) on the properties of Jerusalem artichoke pectin were evaluated and they were compared with apple pectin. FTIR spectral analysis showed no major structural differences in Jerusalem artichoke pectin samples produced by various drying treatments. The antioxidant activities of pectin dried by different methods were investigated using in vitro hydroxyl and DPPH radical scavenging systems. The results revealed that the activities of spray dried pectin (SDP) and apple pectin (AP) were stronger than those of vacuum oven dried pectin (ODP) and vacuum freeze dried pectin (FDP). Therefore compared with the other two drying methods, the spray drying method was the best. 展开更多
关键词 Jerusalem artichoke pectin response surface drying methods antioxidant activities
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