A novel micro-nano Ti−10Cu−10Ni−8Al−8Nb−4Zr−1.5Hf filler was used to vacuum braze Ti−47Al−2Nb−2Cr−0.15B alloy at 1160−1220℃ for 30 min.The interfacial microstructure and formation mechanism of TiAl joints and the rel...A novel micro-nano Ti−10Cu−10Ni−8Al−8Nb−4Zr−1.5Hf filler was used to vacuum braze Ti−47Al−2Nb−2Cr−0.15B alloy at 1160−1220℃ for 30 min.The interfacial microstructure and formation mechanism of TiAl joints and the relationships among brazing temperature,interfacial microstructure and joint strength were emphatically investigated.Results show that the TiAl joints brazed at 1160 and 1180℃ possess three interfacial layers and mainly consist of α_(2)-Ti_(3)Al,τ_(3)-Al_(3)NiTi_(2) and Ti_(2)Ni,but the brazing seams are no longer layered and Ti_(2)Ni is completely replaced by the uniformly distributed τ_(3)-Al_(3)NiTi_(2) at 1200 and 1220℃ due to the destruction of α_(2)-Ti_(3)Al barrier layer.This transformation at 1200℃ obviously improves the tensile strength of the joint and obtains a maximum of 343 MPa.Notably,the outward diffusion of Al atoms from the dissolution of TiAl substrate dominates the microstructure evolution and tensile strength of the TiAl joint at different brazing temperatures.展开更多
The visual observation of the mold filling and the standard analysis-of-variance （ANOVA） for the velocity of the filling metal are conducted to study foam-metal interface behaviors during the mold filling of the los...The visual observation of the mold filling and the standard analysis-of-variance （ANOVA） for the velocity of the filling metal are conducted to study foam-metal interface behaviors during the mold filling of the lost foam casting （LFC） process of the magnesium alloy. Results show that the foam primarily melts into liquid products instead of gasifying at the pouring temperature of the magnesium alloy. Without the vacuum, the metal fills smoothly with a slightly convex metal front, and the velocity of the filling metal is low and continually decreases as the foam is displaced. The mold filling is governed by the removal of foam decomposition products at the foam-metal interface. However, when the vacuum is applied, the mold filling is controlled by the foam decomposition rate at the foam-metal interface. A pronounced irregular and concave metal front is formed. The velocity of the metal front varies tremendously during the mold filling process and is ruleless. The metal velocity increases rapidly, and the vacuum shows a strong interaction effect with the pouring temperature on the metal velocity. As the vacuum continues to increase, the pouring temperature becomes the most significant factor for the mold filling, while both the vacuum effect and the interaction effect between the vacuum and the pouring temperature on the metal velocity are substantially reduced. Based on experimental results, a model for the foam thermal degradation and the removal of decomposition products occurred at the foam-metal interface is presented during the mold filling of the magnesium alloy LFC process under the vacuum.展开更多
Vacuum die casting can reduce the'air entrapment'phenomenon during casting process.Based on the temperature measurements at metal-die interface with different processing parameters,such as slow shot speed(VL),...Vacuum die casting can reduce the'air entrapment'phenomenon during casting process.Based on the temperature measurements at metal-die interface with different processing parameters,such as slow shot speed(VL),high shot speed(VH),pouring temperature(Tp)and initial die temperature(Tm),inverse method was developed to determine the interfacial heat transfer coefficient(IHTC).The results indicate that a closer contact between the casting and die could be achieved when the vacuum system is used.It is found that the vacuum could strongly increase the values of IHTC and decrease the grain size in castings.The IHTC could have a higher peak value with increasing the Tp from680to720℃or the VL from0.1to0.4m/s.In addition,the influence of the VH and Tm on IHTC could be negligible.展开更多
Diffusion bonding of as-cast Mg−6Gd−3Y magnesium alloy was carried out at temperatures of 400−480℃ with bonding pressure of 6 MPa for 90 min.Diffusion bonded joints were solution treated at 495℃ for 14 h and then ag...Diffusion bonding of as-cast Mg−6Gd−3Y magnesium alloy was carried out at temperatures of 400−480℃ with bonding pressure of 6 MPa for 90 min.Diffusion bonded joints were solution treated at 495℃ for 14 h and then aged at 200℃ for 30 h.Microstructures and mechanical properties of joints were analyzed.The results showed that rare earth elements and their compounds gathering at bonding interface hindered the grain boundary migration crossing bonding interface.Tensile strength of as-bonded and as-solution treated joints increased firstly and then decreased with the bonding temperature increasing due to the combined effects of grain coarsening and solid-solution strengthening.As-bonded and solution-treated joints fractured at matrix except the joint bonded at 400℃,while aged joints fractured at bonding interface.The highest ultimate tensile strength of 279 MPa with elongation of 2.8%was found in joint bonded at 440℃ with solution treatment followed by aging treatment.展开更多
基金the National Natural Science Foundation of China(No.51865012)the Natural Science Foundation of Jiangxi Province,China(No.20202BABL204040)+3 种基金the Open Foundation of National Engineering Research Center of Near-net-shape Forming for Metallic Materials,China(No.2016005)the Science Foundation of Educational Department of Jiangxi Province,China(No.GJJ170372)the GF Basic Scientific Research Project,China(No.JCKY2020205C002)the Civil Population Supporting Planning and Development Project,China(No.JPPT125GH038).
文摘A novel micro-nano Ti−10Cu−10Ni−8Al−8Nb−4Zr−1.5Hf filler was used to vacuum braze Ti−47Al−2Nb−2Cr−0.15B alloy at 1160−1220℃ for 30 min.The interfacial microstructure and formation mechanism of TiAl joints and the relationships among brazing temperature,interfacial microstructure and joint strength were emphatically investigated.Results show that the TiAl joints brazed at 1160 and 1180℃ possess three interfacial layers and mainly consist of α_(2)-Ti_(3)Al,τ_(3)-Al_(3)NiTi_(2) and Ti_(2)Ni,but the brazing seams are no longer layered and Ti_(2)Ni is completely replaced by the uniformly distributed τ_(3)-Al_(3)NiTi_(2) at 1200 and 1220℃ due to the destruction of α_(2)-Ti_(3)Al barrier layer.This transformation at 1200℃ obviously improves the tensile strength of the joint and obtains a maximum of 343 MPa.Notably,the outward diffusion of Al atoms from the dissolution of TiAl substrate dominates the microstructure evolution and tensile strength of the TiAl joint at different brazing temperatures.
文摘The visual observation of the mold filling and the standard analysis-of-variance （ANOVA） for the velocity of the filling metal are conducted to study foam-metal interface behaviors during the mold filling of the lost foam casting （LFC） process of the magnesium alloy. Results show that the foam primarily melts into liquid products instead of gasifying at the pouring temperature of the magnesium alloy. Without the vacuum, the metal fills smoothly with a slightly convex metal front, and the velocity of the filling metal is low and continually decreases as the foam is displaced. The mold filling is governed by the removal of foam decomposition products at the foam-metal interface. However, when the vacuum is applied, the mold filling is controlled by the foam decomposition rate at the foam-metal interface. A pronounced irregular and concave metal front is formed. The velocity of the metal front varies tremendously during the mold filling process and is ruleless. The metal velocity increases rapidly, and the vacuum shows a strong interaction effect with the pouring temperature on the metal velocity. As the vacuum continues to increase, the pouring temperature becomes the most significant factor for the mold filling, while both the vacuum effect and the interaction effect between the vacuum and the pouring temperature on the metal velocity are substantially reduced. Based on experimental results, a model for the foam thermal degradation and the removal of decomposition products occurred at the foam-metal interface is presented during the mold filling of the magnesium alloy LFC process under the vacuum.
基金Project (2016YFB0301001) supported by the National Key Research and Development Program of ChinaProject (2015M580093) supported by the General Financial Grant from the China Postdoctoral Science Foundation of China
文摘Vacuum die casting can reduce the'air entrapment'phenomenon during casting process.Based on the temperature measurements at metal-die interface with different processing parameters,such as slow shot speed(VL),high shot speed(VH),pouring temperature(Tp)and initial die temperature(Tm),inverse method was developed to determine the interfacial heat transfer coefficient(IHTC).The results indicate that a closer contact between the casting and die could be achieved when the vacuum system is used.It is found that the vacuum could strongly increase the values of IHTC and decrease the grain size in castings.The IHTC could have a higher peak value with increasing the Tp from680to720℃or the VL from0.1to0.4m/s.In addition,the influence of the VH and Tm on IHTC could be negligible.
基金financially supported by the Science Innovation Foundation of Shanghai Academy of Spaceflight Technology,China (No.SAST2020-117)。
文摘Diffusion bonding of as-cast Mg−6Gd−3Y magnesium alloy was carried out at temperatures of 400−480℃ with bonding pressure of 6 MPa for 90 min.Diffusion bonded joints were solution treated at 495℃ for 14 h and then aged at 200℃ for 30 h.Microstructures and mechanical properties of joints were analyzed.The results showed that rare earth elements and their compounds gathering at bonding interface hindered the grain boundary migration crossing bonding interface.Tensile strength of as-bonded and as-solution treated joints increased firstly and then decreased with the bonding temperature increasing due to the combined effects of grain coarsening and solid-solution strengthening.As-bonded and solution-treated joints fractured at matrix except the joint bonded at 400℃,while aged joints fractured at bonding interface.The highest ultimate tensile strength of 279 MPa with elongation of 2.8%was found in joint bonded at 440℃ with solution treatment followed by aging treatment.
