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马钱子生品、炮制品中马钱子碱和士的宁的含量测定及毒性实验研究 被引量:13
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作者 卢军 刘兆龙 +1 位作者 赵翡翠 田红林 《新疆医科大学学报》 CAS 2020年第4期506-509,共4页
目的测定马钱子生品、砂烫炮制品和牛奶炮制品中马钱子碱和士的宁含量,及其毒性研究。方法采用HPLC法测定马钱子生品、砂烫炮制品和牛奶炮制品中马钱子碱和士的宁含量,通过小鼠急性毒性实验测定马钱子生品、马钱子砂烫炮制品及马钱子牛... 目的测定马钱子生品、砂烫炮制品和牛奶炮制品中马钱子碱和士的宁含量,及其毒性研究。方法采用HPLC法测定马钱子生品、砂烫炮制品和牛奶炮制品中马钱子碱和士的宁含量,通过小鼠急性毒性实验测定马钱子生品、马钱子砂烫炮制品及马钱子牛奶炮制品的半数致死量(LD50)。结果马钱子生品中马钱子碱和士的宁的含量分别为(0.037±0.014)mg/g和(0.934±0.254)mg/g,LD50为1.9737 mg/kg体质量。马钱子砂烫炮制品中马钱子碱和士的宁的含量分别为(0.016±0.005)mg/g和(0.237±0.098)mg/g。马钱子牛奶炮制品中马钱子碱和士的宁的含量分别为(0.011±0.006)mg/g和(0.191±0.048)mg/g。马钱子砂烫炮制品和牛奶炮制品按最大给药剂量(2.70 mg/kg体质量)给药后,小鼠均无出现死亡。结论砂烫、牛奶炮制能够降低马钱子生品中马钱子碱和士的宁的含量,提高用药的安全性。 展开更多
关键词 马钱子 制品 牛奶制品 马钱子碱 士的宁 急性毒性实验
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吴茱萸炮制历史与现状 被引量:10
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作者 杨磊 黄开颜 +3 位作者 陈兴 杨晖 李康 张志国 《中国药业》 CAS 2011年第8期65-66,共2页
目的了解历代对吴茱萸是否有砂烫炮炙法。方法查阅相关文献并进行归纳、整理。结果吴茱萸炮炙,除净制外,有洗、泡、清炒、炙、煮、九蒸九曝、熬、焙、火炮、烘、煨等。液体辅料有水、盐水、醋、酒、姜汁、黑豆汁、童便、米泔水、糯米与... 目的了解历代对吴茱萸是否有砂烫炮炙法。方法查阅相关文献并进行归纳、整理。结果吴茱萸炮炙,除净制外,有洗、泡、清炒、炙、煮、九蒸九曝、熬、焙、火炮、烘、煨等。液体辅料有水、盐水、醋、酒、姜汁、黑豆汁、童便、米泔水、糯米与萝卜共煎汁、木香汁、黄连汁、甘草汁等。固体辅料有黄黑大豆、盐、补骨脂、黄连、牵牛子、黑糯米等。结论历代对吴茱萸无砂烫炮炙法,此法为湖南习用。 展开更多
关键词 吴茱萸 固体辅料 制用具
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民族药铁棒锤砂炒炮制品的质量标准研究 被引量:3
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作者 廖琦 杨继家 +1 位作者 张艺 张静 《中国药房》 CAS CSCD 2013年第11期1007-1009,共3页
目的:制定民族药铁棒锤砂炒炮制品的质量标准。方法:采用薄层色谱(TLC)法对该炮制品进行定性鉴别,采用高效液相色谱法测定样品中苯甲酰乌头原碱的含量,并对样品进行水分、灰分与浸出物测定。结果:TLC中苯甲酰乌头原碱斑点明显,分离度好... 目的:制定民族药铁棒锤砂炒炮制品的质量标准。方法:采用薄层色谱(TLC)法对该炮制品进行定性鉴别,采用高效液相色谱法测定样品中苯甲酰乌头原碱的含量,并对样品进行水分、灰分与浸出物测定。结果:TLC中苯甲酰乌头原碱斑点明显,分离度好;样品中苯甲酰乌头原碱的质量分数在0.53%~1.73%之间,水分、总灰分、酸不溶性灰分、70%乙醇浸出物的平均质量分数分别为2.80%、2.89%、1.08%、21.38%。铁棒锤砂炒炮制品中不得检出乌头碱。结论:所建标准可用于铁棒锤砂炒炮制品的质量控制和评价。 展开更多
关键词 铁棒锤 制品 质量标准 薄层色谱法 高效液相色谱法 水分 灰分 浸出物
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《科技风》 2003年第17期48-65,共18页
关键词 吸水保水剂 砂炮 生产技术 口香糖 爆炸喷涂技术 复合增强材料 牙签肉 无土栽培营养液 液氧呼吸器
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Optimum Level of Replacement Slag in OPC-Slag Mortars 被引量:1
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作者 Fathollah Sajedi Payam Shafigh 《Journal of Civil Engineering and Architecture》 2010年第1期11-19,共9页
The present paper reports the testing of 14 OPC-slag mortars and 2 controls OPC and slag mortars. The main aim is to determine the optimum level of replacement slag for achievement to the highest early strength with r... The present paper reports the testing of 14 OPC-slag mortars and 2 controls OPC and slag mortars. The main aim is to determine the optimum level of replacement slag for achievement to the highest early strength with reasonable flow. Variable was the level of GGBFS in the binder. In this experimental work, two types of sands were used that are: silica and mining sands. It is determined that the optimum level of replacement slag is 40% and use of silica sand in OPC is preferable to mining sand and reversely, use of mining sand is preferred in GG100 to silica sand. All mortars had W/B and S/B 0.33 and 2.25, respectively. 展开更多
关键词 Ground granulated blast furnace slag (GGBFS) high early strength optimum level OPC-slag mortar flow
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Technological Evolution of Historic Structural Mortars
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作者 Vasiliki Pachta Maria Stefanidou Stavroula Konopisi Ioanna Papayianni 《Journal of Civil Engineering and Architecture》 2014年第7期846-854,共9页
Mortars are among the first building materials used in constructions, even from prehistoric times (8th millennium BC). Their study reveals a great source of information regarding the evolution of their technological... Mortars are among the first building materials used in constructions, even from prehistoric times (8th millennium BC). Their study reveals a great source of information regarding the evolution of their technological characteristics and application techniques, the availability and exploitation of raw materials, as well the wider socio-economic aspects of each era. The aim of this paper is to comparatively evaluate the analysis results from approximately 1,000 structural mortar samples taken from various monuments and historic buildings of Greece, dated from the Hellenistic period, until the beginning of the 20th century. The analysis focused in the determination of their physico-mechanical and chemical properties, such as porosity, apparent specific gravity, mechanical strength, aggregates type and granulometry and chemical composition. Through the results' evaluation, significant remarks can be made upon the evolution of the raw materials used (binding system, aggregates, additives), as well as regarding the final properties of historic structural mortars. It is concluded that hydrated lime was the main binding agent used for a long-lasting period of 2.5 millenniums, while mixed type binding systems based on lime and natural pozzolan were systematically used for producing durable mortars, resistant to humidity. In any case, it seems that ancient masons were fully aware of the significant role of mortars in constructions and were capable of exploiting the available raw materials and application techniques to the maximum. 展开更多
关键词 Structural mortars technological evolution physico-mechanical chemical properties.
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Strength Development of Cement-Slag Mortars
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作者 Fathollah Sajedi 《Journal of Civil Engineering and Architecture》 2012年第9期1169-1183,共15页
In this experimental work, three groups of cement-slag mortars namely OPC, OPC-slag, and slag mortars were made. All were cured in both water and air under room temperature. Strength development was studied up to 90 d... In this experimental work, three groups of cement-slag mortars namely OPC, OPC-slag, and slag mortars were made. All were cured in both water and air under room temperature. Strength development was studied up to 90 days. The mortars were prepared using 0%, 50%, and 100% replacement with slag. The sensitivity for all groups was obtained against the curing regime with the highest being attributed to the slag mortars. The highest and lowest strengths at early ages were attributed to OPC and slag mortars when both were cured in water. The highest and lowest strengths were attributed to OPC-slag and slag mortars at later ages, respectively. The highest strengths for OPC-slag, OPC, and slag mortars were as 72.0, 64.0, and 21.5 MPa at 90 days when the specimens cured in water, respectively. Strength loss was observed for all groups at later ages when cured in air under room temperature. The maximum and minimum, of about 8.0% and 1.3%, occurred at 56 and 90 days for slag and OPC-slag mortars, respectively. 展开更多
关键词 OPC-slag mortars slag mortars OPC mortars compressive strength strength development strength loss.
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