等离子体填充能够明显提高真空电子器件的效率和功率,研究等离子体填充器件具有重要的科学价值.本文基于对等离子体填充金属光子晶体慢波结构色散特性的分析,利用粒子模拟方法展示了等离子体填充慢波结构中的注波互作用过程.重点研究了...等离子体填充能够明显提高真空电子器件的效率和功率,研究等离子体填充器件具有重要的科学价值.本文基于对等离子体填充金属光子晶体慢波结构色散特性的分析,利用粒子模拟方法展示了等离子体填充慢波结构中的注波互作用过程.重点研究了慢波结构中场分布特性、等离子体密度和外部工作条件对频率及输出功率的影响.研究发现,填充一定密度等离子体后,慢波结构内纵向和横向电场强度明显增大,注波互作用增强,输出频率受等离子体影响不大.金属光子晶体结构具有的频率选择特性使器件工作于TM01模态.阴极电压增加使输出功率增大,频率略有增加.引导磁场增加使输出功率先增大后减小,而频率基本不受影响.等离子体填充后器件的输出功率上升,当增加压强至100 m Torr(1 m Torr=0.133 Pa)时,输出功率提高约20%,但只有适当密度下才有较好的角向场分布.通过理论与模拟相结合,发现填充一定密度的等离子体能够提高器件输出功率和效率,为发展新型高功率毫米波振荡辐射源奠定了理论和仿真基础.展开更多
建立离子色谱法同时测定高纯试剂和有机溶剂中甲胺、二甲胺、三甲胺和6种阳离子的方法。对样品处理、色谱柱类型、淋洗液梯度等条件进行优化,实现了过氧化氢、乙醇、丙酮和异丙醇样品的直接进样分析。选用Metrosep C Supp 1阳离子交换...建立离子色谱法同时测定高纯试剂和有机溶剂中甲胺、二甲胺、三甲胺和6种阳离子的方法。对样品处理、色谱柱类型、淋洗液梯度等条件进行优化,实现了过氧化氢、乙醇、丙酮和异丙醇样品的直接进样分析。选用Metrosep C Supp 1阳离子交换柱进行梯度分离,采用微填充床阳离子抑制电导检测器检测。9种待测物质的质量浓度在5~200μg/L范围内与色谱峰面积具有良好的线性关系,相关系数均大于0.999,方法检出限为0.007~0.082μg/L。样品加标回收率为80.0%~110.5%,测定结果的相对标准偏差为0.58%~3.86%(n=5)。该方法满足高纯试剂中痕量有机胺杂质和阳离子的测定要求。展开更多
Chloride ion transport in reclaimed soil solutions filled with fly ash （FA） was investigated by measuring the hydraulic parameters （i,e. water retention curves and hydraulic conductivity） of three substrates, name...Chloride ion transport in reclaimed soil solutions filled with fly ash （FA） was investigated by measuring the hydraulic parameters （i,e. water retention curves and hydraulic conductivity） of three substrates, namely GSL, GFA, and CFA. Similar simulations were carried out under certain weather conditions. The different boundary conditions of chloride transport were also discussed from FA texture, cover soil thickness, groundwater table level, and initial chloride concentration. Furthermore, the sensitivities of chloride ions to these effect factors were analyzed. The results show that the different top soil thickness and initial chloride concentration have no effect on salinity of topsoil solution in the monitoring points, but they can clearly change the chloride concentration of FA layers. The sensibilities from top soil thickness and initial chloride content are exceedingly weak to the salinity balance based on two dimensions of the time and concentration. While the different FA texture and groundwater table not only affect the salinity equilibrium process of the whole reclaimed soil profile, but also change its balance state. Generally, coarse FA particles and high groundwater table can defer the salinity balance process of the reclaimed soil solution, and they also increase the chloride concentration of FA layer solutions, and even topsoil ones.展开更多
文摘等离子体填充能够明显提高真空电子器件的效率和功率,研究等离子体填充器件具有重要的科学价值.本文基于对等离子体填充金属光子晶体慢波结构色散特性的分析,利用粒子模拟方法展示了等离子体填充慢波结构中的注波互作用过程.重点研究了慢波结构中场分布特性、等离子体密度和外部工作条件对频率及输出功率的影响.研究发现,填充一定密度等离子体后,慢波结构内纵向和横向电场强度明显增大,注波互作用增强,输出频率受等离子体影响不大.金属光子晶体结构具有的频率选择特性使器件工作于TM01模态.阴极电压增加使输出功率增大,频率略有增加.引导磁场增加使输出功率先增大后减小,而频率基本不受影响.等离子体填充后器件的输出功率上升,当增加压强至100 m Torr(1 m Torr=0.133 Pa)时,输出功率提高约20%,但只有适当密度下才有较好的角向场分布.通过理论与模拟相结合,发现填充一定密度的等离子体能够提高器件输出功率和效率,为发展新型高功率毫米波振荡辐射源奠定了理论和仿真基础.
文摘建立离子色谱法同时测定高纯试剂和有机溶剂中甲胺、二甲胺、三甲胺和6种阳离子的方法。对样品处理、色谱柱类型、淋洗液梯度等条件进行优化,实现了过氧化氢、乙醇、丙酮和异丙醇样品的直接进样分析。选用Metrosep C Supp 1阳离子交换柱进行梯度分离,采用微填充床阳离子抑制电导检测器检测。9种待测物质的质量浓度在5~200μg/L范围内与色谱峰面积具有良好的线性关系,相关系数均大于0.999,方法检出限为0.007~0.082μg/L。样品加标回收率为80.0%~110.5%,测定结果的相对标准偏差为0.58%~3.86%(n=5)。该方法满足高纯试剂中痕量有机胺杂质和阳离子的测定要求。
基金Supported by the National Natural Science Foundation of China （51274013） the International Cooperation Projects of Anhui, China （10080703026） Acknowledgements We thank the work group of soil information systems and solute transport models from Osnabrueck University of Applied Sciences, Germany for providing us their experimental work.
文摘Chloride ion transport in reclaimed soil solutions filled with fly ash （FA） was investigated by measuring the hydraulic parameters （i,e. water retention curves and hydraulic conductivity） of three substrates, namely GSL, GFA, and CFA. Similar simulations were carried out under certain weather conditions. The different boundary conditions of chloride transport were also discussed from FA texture, cover soil thickness, groundwater table level, and initial chloride concentration. Furthermore, the sensitivities of chloride ions to these effect factors were analyzed. The results show that the different top soil thickness and initial chloride concentration have no effect on salinity of topsoil solution in the monitoring points, but they can clearly change the chloride concentration of FA layers. The sensibilities from top soil thickness and initial chloride content are exceedingly weak to the salinity balance based on two dimensions of the time and concentration. While the different FA texture and groundwater table not only affect the salinity equilibrium process of the whole reclaimed soil profile, but also change its balance state. Generally, coarse FA particles and high groundwater table can defer the salinity balance process of the reclaimed soil solution, and they also increase the chloride concentration of FA layer solutions, and even topsoil ones.
