热阴极离子规阴极灯丝断裂机理研究

介绍热阴极离子规的工作原理及组成结构,从热阴极灯丝变细、材料缺陷和工艺缺陷3方面分析离子规阴极灯丝断裂机理,根据断裂机理提出使用过程中的一些建议,以便延长使用寿命。

离子泵/离子规的工作原理与维护

１引言许多大型进口分析仪器（如ＰＨＩＬＩＰ公司生产的ＣＭ１２型透射电子显微镜）在工作时，为了在其真空室内产生和维持较高的真空氛围，一般采取的办法是设备开机后，机械真空泵和油扩散泵依次投入工作，吸收和排出真空室内的大部分气体。当真空室内的气压下降到０．...

Performance of Ionization Gauge and Quadrupole Mass Spectrometer with Bessel-Box Type Energy Analyzer:a Review of Progress

A novel energy analyzer with a simple structured Bessel box has been successfully developed and incorporated into ionization gauges and quadrupole mass spectrometers (QMS) to improve their measurement of the total and partial pressures,respectively.We found that the energy analyzer may not only effectively separate the gas phase ions and electron stimulated desorption (ESD) ions produced in the ionizer,but also screen the ion collector from irradiation of the soft X rays and VUVphotons generated in the ionizer.The screening effects considerably better the trace impurity detection limit of the QMS down to a few tens ppb in the pressure range of 10 -3 Pa.The modified ionization gauge is capable of measuring pressure ranging from 10 -11 to 10 -6 Pa in the pulse counting mode and its upper limit may extends to 10 -3 Pa in DC ion current mode with typical sensitivities factor of(6.7±0.2)×10 -3 Pa -1 for N 2 and (2.3±0.2)×10 -3 Pa -1 for H 2,respectively.No ESD ions was observed in the simple looking spectrum obtained with the modified QMS.We also found that the energy spectra of fragment ions depend strongly on species of parent ions.

D/MAX-RB X射线衍射仪维修一例

本文介绍日本理学公司生产D/MAX-RB X射线衍射仪维修一例。通过逐步分析检查,排除该仪器加高压不动作的故障,并介绍了有关电路故障的分析及排除方法。

In-situ growth of silver nanostructure on quartz glass substrates

Silver nanostructure compact aggregates on the surface of quartz glass substrates were synthesized by small gold seeds with the assistance of poly vinypyrrolidone (PVP) and irradiation of fluorescent lamp. The formation mechanism of silver nanostructure was proposed. The results show that both the PVP and the light irradiation are the keys to in-situ growth of silver nanostructure on quartz glass substrates. The silver nanostructure of the substrates which finally grow up to 150 nm after 20 h irradiation exhibits irregular shape, and some of nanoparticles stack to form bilayer. A new broad band appears in the absorption spectra of the substrates due to the interparticle dipole?dipole coupling of surface plasmon resonance response of the triangular silver nanoplate particles, which red shifts 600?800 nm as the particles grow up. The substrates have an emission band centered at 400 nm on their fluorescence spectra, and the fluorescence intensity shrinks as the average size of the silver nanostructure increases. The strongest SERS signal of SERS-active substrate is fabricated after 16 h.

1Assessing Soil Available Potassium by Cation Exchange Membrane and Conventional Chemical Extractions

Four testing methods using canon exchange membrane (CEM), ammonium acetate, ASI (0.25 mol L-1 NaHCO3+0.01 mol L-1 EDTA +0.01 mol L-1 NH4P) and 1.0 mol L-1 boiling nitric acid, respectively, were used to evaluate soil available K. The soil K tested by CEM was significantly correlated with that by the other (conventional) methods (r2=0.43**~0.95***). The soil K tested by CEM saturated with NH4HCO3 (15 min extraction) was most closely correlated with that by the other methods (2 =0. 60***~0.95***). Potassium availability, as predicted by soil test, was comparable to actual K uptake by canola and wheat grown on the soils in growth chamber. Regression analyses showed that plant K uptake was more closely correlated with K extracted by CEM (r2=0.56***~0.81***) than that by the conventional methods (r2=0.46***~;0.81***), most closely correlsted with that by NH4HCO3-saturated CEM for 15 min (r2=0.81***), and worst correlated with that by HNO3 (r2=0.45**~0.72***).

The Enrichment of Chloride Anion in the Occluded Cell and Its Effect on Stress Corrosion Crack of 304 Stainless Steel in Low Chloride Concentration Solution

The enrichment of chloride anion within the occluded cell （OC） for Type 304 austenitic stainless steel in low chloride concentration solution has been investigated by means of a simulated OC. The influence of the enrichment of chloride anion on stress corrosion crack （SCC） of Type 304 stainless steel has been studied. It was observed that the amount of chloride anion migration was proportional to the charge flowing through the anode. Owning to the effects of enrichment of chloride anion, low chloride concentration solution could induce SCC for Type 304 stainless steel.

Tribological properties of aqueous solutions with lauric acid random copolyether (LPE) added

This work presents the results of tribological investigations of lubricating substances composed of water and a nonionic surfactant:lauric acid random copolyether(LPE),as additive.At the current stage of investigation,aqueous solutions with LPE additives are prepared and subsequently the lowering friction and reducing wear behaviors are tested by means of friction/wear tester,in conjunction with that the film forming properties experiments are carried out with a nanoscale film thickness measure apparatus.The contact is under condition of steel-steel tribo-pair.The results show that the coefficient of friction measured decreases considerably to about over 60%relative to water.The film thickness data of friction process lubricated by aqueous solutions with LPE added show that the lubrication is in boundary lubrication regime.The results indicate that aqueous solutions with LPE added can be used to improve the lubricity and they may be applied to real tribological systems.

The first time observations of low-latitude ionospheric irregularities by VHF radar in Hainan

Sanya VHF radar （18.4°N, 109.6°E, dip latitude 12.8°N） at Hainan Island is the first coherent backscatter radar for sounding low-latitude ionospheric irregularities in the mainland of China. In this paper, we present the first results of low-latitude iono- spheric E and F region irregularities using the radar data during the period from February 2009 to March 2010. The Doppler velocity of radar echoes from E region field aligned irregularities （FAIs） was about several tens of meters per second, while the Doppler spectral width was appreciably larger than the velocity, and could reach one hundred meters per second, indicating that the observed E region FAls belonged to type 2 irregularities. The observations of range time intensity （RTI） maps of FAIs showed that E region irregularities most often occurred at night within the altitude range 85-115 kin, and were rarely observed at afternoon hours. The percentage occurrence of E region FAIs maximized during spring months （Feb.-May） with a peak value over 80%. The heights at which the strongest echo related FAIs occurred were mainly around 100 kin, lower than h＇Es and the difference is mostly 10-20 km. December solstice seemed to be the minimum period of occurrence when the FA! ech- oes were commonly detected at a narrow altitude range 90-100 km. Moreover, simultaneous radar and GPS observations dur- ing spread F events in the pre-midnight hours of solar minimum revealed that significant GPS L band scintillations coincided with the appearance of F region plasma plume structures, which extended up to 450 km in altitude.

Case study of small scale polytropic index in the central plasma sheet

This paper studies the effective polytropic index in the central plasma sheet （CPS） by using the method of Kartalev et al. （2006）, which adopts the denoising technique of Haar wavelet to identify the homogeneous MHD Bernoulli integral （MBI） and has been frequently used to study the polytropic relation in the solar wind. We chose the quiet CPS crossing by Cluster C1 during the interval 08：51：00-09：19：00 UT on 03 August 2001. In the central plasma sheet, thermal pressure energy per unit mass is the most important part in MBI, and kinetic energy of fluid motion and electromagnetic energy per unit mass are less important. In the MBI, there are many peaks, which correspond to isothermal or near isothermal processes. The interval lengths of homogenous MBI regions are generally less than 1 min. The polytropic indexes are calculated by linearly fitting the data of lnp and Inn within a 16 s window, which is shifted forward by 8 s step length. Those polytropic indexes with IRI ≥0.8 （R is the correlation coefficient between lnp and inn） and p-value≤0.1 in the homogeneous regions are almost all in the range of [0, 1]. The mean and median effective polytropic indexes with high R and low p-value in homogeneous regions are 0.34 and 0.32 respectively, which are much different from the polytropic index obtained by traditional method （αtrad=-0.15）. This result indicates that the CPS is not uniform even during quiet time and the blanket applications of polytropic law to plasma sheet may return misleading value of polytropic index. The polytropic indexes in homogeneous regions with a high correlation coefficient basically have good regression significance and are thus credible. These results are very important to understand the energy transport in magnetotail in the MHD frame.

Design rules of pseudocapacitive electrode materials:ion adsorption,diffusion,and electron transmission over prototype TiO_(2)

The development of a high-performing pseudocapacitor requires a comprehensive understanding of electrode materials from the aspects of electron transfer and electrolyte ion adsorption and diffusion.Herein,these factors are considered over the prototype TiO_(2),and a high pseudocapacitance is achieved via the introduction of various defects,i.e.,oxygen defect(V_(O))and co-doped defect(V_(O)+N_(O)).The study is based on joint explorations of first-principle calculations and the transfer matrix method.Relative to pristine TiO_(2)(300 F g^(-1)),defective TiO_(2) produces pseudocapacitance as high as 1700 F g^(-1).Moreover,defects induce small barriers for electron transmission caused by surface band bending.The climbing image nudged elastic band diffusion of H ions displays a much higher barrier in TiO_(2)-V_(O) than in TiO_(2)-V_(O)+N_(O).Such a result indicates easy H diffusion in the co-doped system.This work provides insights into the adsorption and diffusion of electrolyte ions and the influence of defects on electron transfer.The results are also significant for the design and optimization of electrode materials for the next generation of supercapacitors.