The solubilities of isophthalic acid （1） in binary acetic acid （2） ＋ water （3） solvent mixtures were determined in a pressurized vessel. The temperature range was from 373.2 to 473.2K and the range of the mole ...The solubilities of isophthalic acid （1） in binary acetic acid （2） ＋ water （3） solvent mixtures were determined in a pressurized vessel. The temperature range was from 373.2 to 473.2K and the range of the mole fraction of acetic acid in the solvent mixtures was from x2 = 0 to 1. A new method to measure the solubility was developed, which solved the problem of sampling at high temperature. The experimental results indicated that within the temperature range studied, the solubilities of isophthalic acid in all mixtures showed an increasing trend with increasing tem- perature. The expe^mental solubilities were co .rrelated by the Buchowski equation, and the calculate results showed good agreement with the experimental solubilities. Furthermore, the mixed solvent systems were found to exhibit a maximum solubility effect on the solubility, which may be attributed to the intermolecular association between the solute and the solvent mixture： The maximum solubility effect was well modeled by the modified Wilson equation.展开更多
This paper presents a two-agent framework to build a natural langua g e query interface for IC information system, focusing more on scope queries in a single English sentence. The first agent, parsing agent, syntact...This paper presents a two-agent framework to build a natural langua g e query interface for IC information system, focusing more on scope queries in a single English sentence. The first agent, parsing agent, syntactically p rocesses and semantically interprets natural language sentence to construct a fu zzy structured query language (SQL) statement. The second agent, defuzzif ying agent, defuzzifies the imprecise part of the fuzzy SQL statement into its e quivalent executable precise SQL statement based on fuzzy rules. The first agent can also actively ask the user some necessary questions when it manages to disa mbiguate the vague retrieval requirements. The adaptive defuzzification approach employed in the defuzzifying agent is discussed in detail. A prototype interface has been implemented to demonstrate the effectiveness.展开更多
In order to analyze the composition and frequency distribution of acceleration signal in the process of projectile penetrating,this paper uses wavelet transform to decompose penetration acceleration signal to get the ...In order to analyze the composition and frequency distribution of acceleration signal in the process of projectile penetrating,this paper uses wavelet transform to decompose penetration acceleration signal to get the distribution of penetration acceleration signal in different frequency bands.Compared with the ideal acceleration signal curve and its characteristics,it can be concluded that the frequency range of the acceleration signal in the axis of the projectile and the vibration frequency range of the projectile are 31.25-62.5kHz and 62.5-125 kHz,respectively.Finally,the penetration acceleration signal curve is obtained by Simulink.展开更多
The hot deformation behaviors of solution treated Mg-1.8Mn-0.4Er-0.2Al alloys were investigated by means of compression tests on Gleeble-1500 in strain rate range of 0.01-10s-1,deformation temperature range of 250-450...The hot deformation behaviors of solution treated Mg-1.8Mn-0.4Er-0.2Al alloys were investigated by means of compression tests on Gleeble-1500 in strain rate range of 0.01-10s-1,deformation temperature range of 250-450℃ and a true strain of 0.6.The constitutive relationships among flow stress,strain rate and deformation temperature were described by Arrhenius-type equations,based on the fact that the material constants could be calculated under a wide range of strains.The results show that the flow stress of the experimental alloy decreases with temperature increasing and strain rate decreasing.Under the experimental conditions,the products of constant α and n in the constitutive equation are stable within certain strains,and the deformation activation energy ranges from 160 to 220 kJ/mol.It is proved that the values of calculated flow stress are close to the experimental results with average error of 2.01%.展开更多
Hot-compression of aluminum alloy 5182 was carried out on a Gleeble- 1500 thermo-simulator at deformation temperature ranging from 350 ℃ to 500 ℃ and at strain rate from 0.01 s^-1 to 10 s^-1 with strain range from 0...Hot-compression of aluminum alloy 5182 was carried out on a Gleeble- 1500 thermo-simulator at deformation temperature ranging from 350 ℃ to 500 ℃ and at strain rate from 0.01 s^-1 to 10 s^-1 with strain range from 0.7 to 1.9. The microstructures and macro-textures evolution under different conditions were investigated by polarized optical microscopy and X-ray diffraction analysis, respectively. The basic trend is that the hot-compression stress increases with the decrease of temperature and increase of strain rate, which is revealed and elucidated in terms of Zener-Hollomon parameter in the hyperbolic sine equation with the hot-deformation activation energy of 143.5 kJ/mol. An empirical constitutive equation is proposed to predict the hot-deformation behavior under different conditions. As deformation temperature increases up to 400 ℃, at strain rate over 1 s^-1, dynamic recrystallization （DRX） occurs. Cube orientation { 100} （001） is detected in the recrystallized sample after hot-compression.展开更多
From the analysis and the contrast of band-limited ray tracing method based on Kirchhoff integral, it was found that the method performs many approximations in the derivation process and omits the derivative term of t...From the analysis and the contrast of band-limited ray tracing method based on Kirchhoff integral, it was found that the method performs many approximations in the derivation process and omits the derivative term of the phase factor in the Kirchhoff integral. Numerical calculations and analysis show that the omission of cor-relation terms in Kirchhoff integrals has a non-negligible effect on the calculation results, and the different terms in the Kirchhoff integral have different effects on different frequency ranges. The method can be applied to ve-locity models containing complex interfaces without changing waves and continuous media. the velocity model and can be extended to elastic waves and continuous media.展开更多
Deformation of ductile cuttings from sandstone in the mechanical compaction process was designed through the "experimental system of triaxial rock deformation",and the influence on porosity was studied by lo...Deformation of ductile cuttings from sandstone in the mechanical compaction process was designed through the "experimental system of triaxial rock deformation",and the influence on porosity was studied by looking into the deformation characteristics of ductile cuttings. The design indexes are as follows: simulated depth 0- 4 000 m,interval depth 500 m,and pressure range 0- 120 MPa at interval of 1. 5 MPa. The experimental results show that the porosity decreases as buried depth increases,indicating a negative relationship between them. The amount of compression was mainly obtained by porosity reduction and cutting deformation. Deformation of ductile cuttings is mainly ductile deformation; and deformation of crystal fragments is mainly expressed as brittle fracture,resulting in decrease of particle size. The research is of certain value for the exploration and development of oil and gas.展开更多
In our experiments,the PL spectra of several In x Ga 1 x N alloy samples with In contents x=0.1,0.15 and 0.25 were measured as a function of temperature ranging from 10 K to 300 K.S-shaped temperature dependencies wer...In our experiments,the PL spectra of several In x Ga 1 x N alloy samples with In contents x=0.1,0.15 and 0.25 were measured as a function of temperature ranging from 10 K to 300 K.S-shaped temperature dependencies were observed in all InGaN samples and a sharp decrease in the full width at half maximum occurred with decreasing temperature in the moderate temperature region.It was found that both phenomena are relative to localization effects.In addition,the degree of localization effects in three samples was investigated using the band-tail model.Our findings are presented in this paper.展开更多
High-purity straight and discrete multiwalled boron nitride nanotubes （BNNTs） were grown via a boron oxide vapor reaction with ammonia using LiNO3 as a promoter. Only a trace amount of boron oxide was detected as an...High-purity straight and discrete multiwalled boron nitride nanotubes （BNNTs） were grown via a boron oxide vapor reaction with ammonia using LiNO3 as a promoter. Only a trace amount of boron oxide was detected as an impurity in the BNNTs by energy-dispersive X-ray （EDX） and Raman spectroscopies. Boron oxide vapor was generated from a mixture of B, FeO, and MgO powders heated to 1,150 ℃, and it was transported to the reaction zone by flowing ammonia. Lithium nitrate was applied to the upper side of a BN bar from a water solution. The bar was placed along a temperature gradient zone in a horizontal tubular furnace. BNNTs with average diameters of 30-50 nm were mostly observed in a temperature range of 1,280-1,320 ℃. At higher temperatures, curled polycrystalline BN fibers appeared. Above 1,320 ℃, the number of BNNTs drastically decreased, whereas the quantity and diameter of the fibers increased. The mechanism of BNNT and fiber growth is proposed and discussed.展开更多
The aim of this study was to establish a quality-control method for calcineurin subunit B(CNB) biological activity determinations. CNB enhances the p-nitrophenylphosphate(p NPP) dephosphorylating activity of calcineur...The aim of this study was to establish a quality-control method for calcineurin subunit B(CNB) biological activity determinations. CNB enhances the p-nitrophenylphosphate(p NPP) dephosphorylating activity of calcineurin subunit A Δ316 mutant(CNAΔ316). A series of CNB concentrations were fitted to a four-parameter equation to calculate the corresponding p NPP maximum dephosphorylation rates. Values were calculated based on biological activity references using a parallel line method. The method was then validated for accuracy, precision, linearity, linear range, sensitivity, specificity, and robustness. The recovery results were greater than 98%. Intra-plate precision was 6.7%, with inter-plate precision of 10.8%. The coefficient of determination was greater than 0.98. The linear range was 0.05–50 μg m L?1, with sensitivity of 50 μg m L?1. Tested cytokines did not induce CNAΔ316 dephosphorylation of p NPP. The chosen CNAΔ316 concentration range did not affect activity determinations.展开更多
基金Supported by the Natural Science Foundation of Zhejiang Province, China （Z4100351） and the Fundamental Research Funds for the Central Universities （2013QNA4035）.
文摘The solubilities of isophthalic acid （1） in binary acetic acid （2） ＋ water （3） solvent mixtures were determined in a pressurized vessel. The temperature range was from 373.2 to 473.2K and the range of the mole fraction of acetic acid in the solvent mixtures was from x2 = 0 to 1. A new method to measure the solubility was developed, which solved the problem of sampling at high temperature. The experimental results indicated that within the temperature range studied, the solubilities of isophthalic acid in all mixtures showed an increasing trend with increasing tem- perature. The expe^mental solubilities were co .rrelated by the Buchowski equation, and the calculate results showed good agreement with the experimental solubilities. Furthermore, the mixed solvent systems were found to exhibit a maximum solubility effect on the solubility, which may be attributed to the intermolecular association between the solute and the solvent mixture： The maximum solubility effect was well modeled by the modified Wilson equation.
文摘This paper presents a two-agent framework to build a natural langua g e query interface for IC information system, focusing more on scope queries in a single English sentence. The first agent, parsing agent, syntactically p rocesses and semantically interprets natural language sentence to construct a fu zzy structured query language (SQL) statement. The second agent, defuzzif ying agent, defuzzifies the imprecise part of the fuzzy SQL statement into its e quivalent executable precise SQL statement based on fuzzy rules. The first agent can also actively ask the user some necessary questions when it manages to disa mbiguate the vague retrieval requirements. The adaptive defuzzification approach employed in the defuzzifying agent is discussed in detail. A prototype interface has been implemented to demonstrate the effectiveness.
文摘In order to analyze the composition and frequency distribution of acceleration signal in the process of projectile penetrating,this paper uses wavelet transform to decompose penetration acceleration signal to get the distribution of penetration acceleration signal in different frequency bands.Compared with the ideal acceleration signal curve and its characteristics,it can be concluded that the frequency range of the acceleration signal in the axis of the projectile and the vibration frequency range of the projectile are 31.25-62.5kHz and 62.5-125 kHz,respectively.Finally,the penetration acceleration signal curve is obtained by Simulink.
基金Project(2008BA4036) supported by the Natural Science Foundation of Chongqing Science and Technology Commission, ChinaProject(081061130) supported by the National University Students Research Training Program and Sharing Fund of Chongqing University’s Large-scale Equipment
文摘The hot deformation behaviors of solution treated Mg-1.8Mn-0.4Er-0.2Al alloys were investigated by means of compression tests on Gleeble-1500 in strain rate range of 0.01-10s-1,deformation temperature range of 250-450℃ and a true strain of 0.6.The constitutive relationships among flow stress,strain rate and deformation temperature were described by Arrhenius-type equations,based on the fact that the material constants could be calculated under a wide range of strains.The results show that the flow stress of the experimental alloy decreases with temperature increasing and strain rate decreasing.Under the experimental conditions,the products of constant α and n in the constitutive equation are stable within certain strains,and the deformation activation energy ranges from 160 to 220 kJ/mol.It is proved that the values of calculated flow stress are close to the experimental results with average error of 2.01%.
基金Project(50905188) supported by the National Natural Science FoundationProject(2012CB619500) supported by Key Basic Research Program of China
文摘Hot-compression of aluminum alloy 5182 was carried out on a Gleeble- 1500 thermo-simulator at deformation temperature ranging from 350 ℃ to 500 ℃ and at strain rate from 0.01 s^-1 to 10 s^-1 with strain range from 0.7 to 1.9. The microstructures and macro-textures evolution under different conditions were investigated by polarized optical microscopy and X-ray diffraction analysis, respectively. The basic trend is that the hot-compression stress increases with the decrease of temperature and increase of strain rate, which is revealed and elucidated in terms of Zener-Hollomon parameter in the hyperbolic sine equation with the hot-deformation activation energy of 143.5 kJ/mol. An empirical constitutive equation is proposed to predict the hot-deformation behavior under different conditions. As deformation temperature increases up to 400 ℃, at strain rate over 1 s^-1, dynamic recrystallization （DRX） occurs. Cube orientation { 100} （001） is detected in the recrystallized sample after hot-compression.
基金Supported by National Natural Science Foundation of China(No.41274120)
文摘From the analysis and the contrast of band-limited ray tracing method based on Kirchhoff integral, it was found that the method performs many approximations in the derivation process and omits the derivative term of the phase factor in the Kirchhoff integral. Numerical calculations and analysis show that the omission of cor-relation terms in Kirchhoff integrals has a non-negligible effect on the calculation results, and the different terms in the Kirchhoff integral have different effects on different frequency ranges. The method can be applied to ve-locity models containing complex interfaces without changing waves and continuous media. the velocity model and can be extended to elastic waves and continuous media.
基金Supported by joint project of CNOOC with Jilin University(No.CCL2012TJXSBS0282)
文摘Deformation of ductile cuttings from sandstone in the mechanical compaction process was designed through the "experimental system of triaxial rock deformation",and the influence on porosity was studied by looking into the deformation characteristics of ductile cuttings. The design indexes are as follows: simulated depth 0- 4 000 m,interval depth 500 m,and pressure range 0- 120 MPa at interval of 1. 5 MPa. The experimental results show that the porosity decreases as buried depth increases,indicating a negative relationship between them. The amount of compression was mainly obtained by porosity reduction and cutting deformation. Deformation of ductile cuttings is mainly ductile deformation; and deformation of crystal fragments is mainly expressed as brittle fracture,resulting in decrease of particle size. The research is of certain value for the exploration and development of oil and gas.
基金supported by the Special Funds for Major State Basic Research Project (Grant No. 2011CB301901)the National Natural Science Foundation of China (Grant Nos. 60820106003,60990311 and 60906025)+1 种基金the Natural Science Foundation of Jiangsu Province (Grant Nos.BK2008019 and BK2009255)the Research Funds from NJU-Yangzhou Institute of Opto-electronics
文摘In our experiments,the PL spectra of several In x Ga 1 x N alloy samples with In contents x=0.1,0.15 and 0.25 were measured as a function of temperature ranging from 10 K to 300 K.S-shaped temperature dependencies were observed in all InGaN samples and a sharp decrease in the full width at half maximum occurred with decreasing temperature in the moderate temperature region.It was found that both phenomena are relative to localization effects.In addition,the degree of localization effects in three samples was investigated using the band-tail model.Our findings are presented in this paper.
文摘High-purity straight and discrete multiwalled boron nitride nanotubes （BNNTs） were grown via a boron oxide vapor reaction with ammonia using LiNO3 as a promoter. Only a trace amount of boron oxide was detected as an impurity in the BNNTs by energy-dispersive X-ray （EDX） and Raman spectroscopies. Boron oxide vapor was generated from a mixture of B, FeO, and MgO powders heated to 1,150 ℃, and it was transported to the reaction zone by flowing ammonia. Lithium nitrate was applied to the upper side of a BN bar from a water solution. The bar was placed along a temperature gradient zone in a horizontal tubular furnace. BNNTs with average diameters of 30-50 nm were mostly observed in a temperature range of 1,280-1,320 ℃. At higher temperatures, curled polycrystalline BN fibers appeared. Above 1,320 ℃, the number of BNNTs drastically decreased, whereas the quantity and diameter of the fibers increased. The mechanism of BNNT and fiber growth is proposed and discussed.
基金supported by the National Important Novel Medicine Research Project (2012ZX09304010, 2013ZX09102062)the National Natural Science Foundation of China (31270849)
文摘The aim of this study was to establish a quality-control method for calcineurin subunit B(CNB) biological activity determinations. CNB enhances the p-nitrophenylphosphate(p NPP) dephosphorylating activity of calcineurin subunit A Δ316 mutant(CNAΔ316). A series of CNB concentrations were fitted to a four-parameter equation to calculate the corresponding p NPP maximum dephosphorylation rates. Values were calculated based on biological activity references using a parallel line method. The method was then validated for accuracy, precision, linearity, linear range, sensitivity, specificity, and robustness. The recovery results were greater than 98%. Intra-plate precision was 6.7%, with inter-plate precision of 10.8%. The coefficient of determination was greater than 0.98. The linear range was 0.05–50 μg m L?1, with sensitivity of 50 μg m L?1. Tested cytokines did not induce CNAΔ316 dephosphorylation of p NPP. The chosen CNAΔ316 concentration range did not affect activity determinations.
