An X-ray diffraction and 57Fe MOssbauer effect study of mechanically alloyed Fe80Al20 is presented. X-ray measurements indicate that the disordered bcc α-Fe（A1） solid solution was formed after 2 h of milling, while...An X-ray diffraction and 57Fe MOssbauer effect study of mechanically alloyed Fe80Al20 is presented. X-ray measurements indicate that the disordered bcc α-Fe（A1） solid solution was formed after 2 h of milling, while the analysis of Mrssbauer spectra suggested that total dissolution of aluminium is achieved after 10 h of milling. These differences can be attributed to： （i） rapid nanocrystallization of aluminium and/or （ii） small particles with small amounts of aluminium cannot be detected by the X-ray diffraction technique.展开更多
文摘An X-ray diffraction and 57Fe MOssbauer effect study of mechanically alloyed Fe80Al20 is presented. X-ray measurements indicate that the disordered bcc α-Fe（A1） solid solution was formed after 2 h of milling, while the analysis of Mrssbauer spectra suggested that total dissolution of aluminium is achieved after 10 h of milling. These differences can be attributed to： （i） rapid nanocrystallization of aluminium and/or （ii） small particles with small amounts of aluminium cannot be detected by the X-ray diffraction technique.
