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自催化还原制备微米和纳米级空心镍球的研究 被引量:3
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作者 邓意达 赵凌 +3 位作者 刘曦 沈彬 刘磊 胡文彬 《高等学校化学学报》 SCIE EI CAS CSCD 北大核心 2005年第7期1309-1312,M007,共5页
提出了一种新型的制备超细空心金属镍粉的方法.通过FESEM,TEM和XRD衍射对该制备方法进行了研究,并考察了有关工艺参数对产物粒径和粒度分布的影响.研究认为,通过在胶核表面发生自催化还原反应,形成金属镍壳,同时胶核发生自分解,最后可... 提出了一种新型的制备超细空心金属镍粉的方法.通过FESEM,TEM和XRD衍射对该制备方法进行了研究,并考察了有关工艺参数对产物粒径和粒度分布的影响.研究认为,通过在胶核表面发生自催化还原反应,形成金属镍壳,同时胶核发生自分解,最后可得到空心金属镍球.控制反应物浓度和NaOH的配比可得到粒径均匀的镍球;通过调整这两个参数可得到粒度在微米或纳米尺度的空心镍球. 展开更多
关键词 空心金属球 微米和纳米级粉末 自催化还原 胶体模板
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一种新型聚能爆破切割水下废弃油井方法的探索 被引量:7
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作者 江德安 李晓杰 闫鸿浩 《爆破器材》 CAS 2008年第3期7-10,共4页
从一个新的角度研究探索出一种新型聚能切割水下废弃油井的方法,用空心金属球与成型穿孔弹相结合以代替传统的线型聚能切割器。利用多个空心金属球之间接触的可移动性,能随时根据实际情况改变其外形;利用空心金属球的聚能效应和密封性,... 从一个新的角度研究探索出一种新型聚能切割水下废弃油井的方法,用空心金属球与成型穿孔弹相结合以代替传统的线型聚能切割器。利用多个空心金属球之间接触的可移动性,能随时根据实际情况改变其外形;利用空心金属球的聚能效应和密封性,可以达到很好的水下爆破切割效果。 展开更多
关键词 聚能切割器 空心金属球 油井
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A new electromagnetic functional material composed of metallic hollow micro-spheres 被引量:4
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作者 徐鸿飞 徐丽娜 +1 位作者 顾宁 孙忠良 《Journal of Southeast University(English Edition)》 EI CAS 2003年第1期8-11,共4页
This paper presents a new electromagnetic functional material developed byelectron-less nickel deposition technique, with a single hollow micro-sphere as the core templateand a thin nickel layer as the shell. The micr... This paper presents a new electromagnetic functional material developed byelectron-less nickel deposition technique, with a single hollow micro-sphere as the core templateand a thin nickel layer as the shell. The micrograph taken by a scanning electron microscope showsthe microstructures of the materials in detail. Scattering parameters of the waveguide sample holderfilled with the materials have been obtained over X band. The electromagnetic parameters computedfrom the measured S parameters show that the material with metallic hollow spheres has as highrelative permeability μ'_r as 19.0 with about 0.6 magnetic loss tangent over the whole bandwidth.Compared to the material with non-metallic spheres, the permeability μ'_r and the magnetic losstangent μ'_r increase greatly, while the permittivity remains lower than 1.8. 展开更多
关键词 electromagnetic functional material microwave absorbing electron-lessdeposition
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Hierarchical porous metal ferrite ball-in-ball hollow spheres: General synthesis, formation mechanism, and high performance as anode materials for Li-ion batteries 被引量:10
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作者 Shouli Li Aihua Li Ranran Zhang Yanyan He Yanjun Zhai Liqiang Xu 《Nano Research》 SCIE EI CAS CSCD 2014年第8期1116-1127,共12页
High yields of CoFe204, NiFe204 and CdFe204 hierarchical porous ball-in-ball hollow spheres have been achieved using hydrothermal synthesis followed by calcination. The mechanism of formation is shown to involve an in... High yields of CoFe204, NiFe204 and CdFe204 hierarchical porous ball-in-ball hollow spheres have been achieved using hydrothermal synthesis followed by calcination. The mechanism of formation is shown to involve an in situ carbonaceous-template process. Hierarchical porous CoFe2O4 hollow spheres with different numbers of shells can be obtained by altering the synthesis conditions. The electrochemical properties of the resulting CoFe2O4 electrodes have been compared, using different binders. The as-obtained CoFe2O4 and NiFe2O4 have relatively high reversible discharge capacity and good rate retention performance which make them promising materials for use as anode materials in lithium ion batteries. 展开更多
关键词 hierarchicalporous FERRITE lithium ion battery ball-in-ball
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