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空气隔断-连续流动分析法快速测定葡萄酒中总糖 被引量:9
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作者 涂小珂 林燕奎 +3 位作者 金晓蕾 林黎 罗洁 陈沛金 《食品科学》 EI CAS CSCD 北大核心 2015年第14期87-90,共4页
目的:建立空气隔断-连续流动分析仪快速测定葡萄酒中总糖含量的分析方法。方法:用样品校正葡萄糖标准溶液,同时在流路中增设透析器以减少样品溶液带来的基质效应及颜色干扰。经过条件优化,流路温度控制在88-92℃,水解反应时间、络合... 目的:建立空气隔断-连续流动分析仪快速测定葡萄酒中总糖含量的分析方法。方法:用样品校正葡萄糖标准溶液,同时在流路中增设透析器以减少样品溶液带来的基质效应及颜色干扰。经过条件优化,流路温度控制在88-92℃,水解反应时间、络合反应时间分别为5 min和12 min。结果:在0.05-3.0 g/L质量浓度范围内,体系吸光度与溶液质量浓度线性关系良好(r^2为0.999 7),方法检出限为0.01 g/L,加标回收率在88.1%-102.3%之间,方法相对标准偏差为2.8%-6.2%;测定结果与GB/T 15038—2006《葡萄酒、果酒通用分析方法》相比,相对标准偏差小于5%,测定快速(45样/h)。结论:方法适用于大批量葡萄酒中总糖含量的检测。 展开更多
关键词 葡萄酒 总糖 空气隔断-连续流动分析
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空气整段间隔流动注射分析中分散度影响因素及性能研究
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作者 支正良 田笠卿 《高等学校化学学报》 SCIE EI CAS CSCD 北大核心 1994年第5期669-671,共3页
空气整段间隔流动注射分析中分散度影响因素及性能研究支正良,田笠卿(中国药科大学分析计算中心,南京,210009)(南京大学现代分析中心,南京,210008)关键词空气整段间隔流动注射分析,分散度,铁空气整段间隔FIA... 空气整段间隔流动注射分析中分散度影响因素及性能研究支正良,田笠卿(中国药科大学分析计算中心,南京,210009)(南京大学现代分析中心,南京,210008)关键词空气整段间隔流动注射分析,分散度,铁空气整段间隔FIA[1,2]的特点是将注入的试样带首... 展开更多
关键词 空气整段间隔流动注射分析 分散度
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空气隔断连续流动分析法同时测定有机肥料中的氮磷钾
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作者 邵青松 叶蔓莉 +1 位作者 王鹏 刘秋霞 《山东化工》 CAS 2019年第5期92-94,共3页
建立了测定同时测定有机肥料中氮磷钾的空气隔断连续流动分析法,样品的氮相对标准偏差最高为2.54%,磷相对标准偏差最高为1.98%,钾相对标准偏差最高为3.73%,氮回收率在97.6%~102.4%之间,磷回收率在97.3%~103.1%之间,钾回收率在96.8%~1... 建立了测定同时测定有机肥料中氮磷钾的空气隔断连续流动分析法,样品的氮相对标准偏差最高为2.54%,磷相对标准偏差最高为1.98%,钾相对标准偏差最高为3.73%,氮回收率在97.6%~102.4%之间,磷回收率在97.3%~103.1%之间,钾回收率在96.8%~103.3%之间;本法相对NY525-2012《有机肥料》农业部标准测定方法而言操作简便、快速、准确度高,特别适合于大批量有机肥料样品中氮磷钾含量检测。 展开更多
关键词 空气隔断连续流动分析 有机肥料 氮磷钾
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一种新的连续流动注射分析法快速测定食品及葡萄酒中的总糖 被引量:3
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作者 王艳 林宏 +4 位作者 丁涛 刘芸 桂茜雯 吴斌 季美泉 《分析仪器》 CAS 2018年第3期82-85,共4页
采用空气气泡间隔-连续流动注射分析的新技术建立了一种快速测定食品总糖的方法。88℃条件下用HCl使样品水解成单糖,水解后的单糖经过透析器净化,除去颗粒物、蛋白质或者生成有色基团的大分子,然后在碱性条件下新亚铜复合物Ⅱ被还原性单... 采用空气气泡间隔-连续流动注射分析的新技术建立了一种快速测定食品总糖的方法。88℃条件下用HCl使样品水解成单糖,水解后的单糖经过透析器净化,除去颗粒物、蛋白质或者生成有色基团的大分子,然后在碱性条件下新亚铜复合物Ⅱ被还原性单糖(果糖、葡萄糖)在88℃热浴中还原形成新亚铜螯合物Ⅰ,在450nm波长处测定吸光度。分析速率可达40样/小时。方法以果糖、葡萄糖混合标准溶液做工作曲线,该法在0~5g/L范围内线性范围良好,相关系数r^2=0.999,方法相对标准偏差在0.008%~0.64%之间,食品基质总糖测定结果与GB 5009.8-2016相比结果相对标准偏差在1.24%~3.32%之间,葡萄酒基质测定结果与国标GB/T 15038-2006相比,相对标准偏差在0.8%~5%之间。本法测定结果与国标测定方法无显著性差异。因此该方法适合于食品中总糖的快速测定,大大缩短了分析时间,减少了手工滴定带来的人为操作误差。 展开更多
关键词 食品 葡萄酒 总糖 空气隔断-连续流动注射分析
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西门子上海中心双层幕墙的通风节能技术分析
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作者 张海 《建筑技术开发》 2016年第7期91-92,共2页
西门子上海中心双层幕墙系统设计整体整洁、透明大方、节能效果明显,该幕墙分格尺寸达到了2800mm×4000mm,设计过程中以计算机模拟为基础,技术论证计算为指导,过幕墙整体的通风构造设计、幕墙构件自身的断热设计及幕墙中间腔体的遮... 西门子上海中心双层幕墙系统设计整体整洁、透明大方、节能效果明显,该幕墙分格尺寸达到了2800mm×4000mm,设计过程中以计算机模拟为基础,技术论证计算为指导,过幕墙整体的通风构造设计、幕墙构件自身的断热设计及幕墙中间腔体的遮阳帘设计,幕墙整体的传热系数达到了1.8W/m^2·K,该双层幕墙节能性、舒适性均达到了设计初始要求。 展开更多
关键词 超大单元板块 通风构造设计 节能设计 空气流动分析
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Air flow patterns and noise analysis inside high speed angular contact ball bearings 被引量:3
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作者 翟强 闫柯 +2 位作者 张优云 朱永生 王亚泰 《Journal of Central South University》 SCIE EI CAS CSCD 2015年第9期3358-3366,共9页
The vortex formed around the rolling ball and the high pressure region formed around the ball-raceway contact zone are the principle factors that barricades the lubricant entering the bearing cavity, and further cause... The vortex formed around the rolling ball and the high pressure region formed around the ball-raceway contact zone are the principle factors that barricades the lubricant entering the bearing cavity, and further causes improper lubrication. The investigation of the air phase flow inside the bearing cavity is essential for the optimization of the oil-air two-phase lubrication method. With the revolutionary reference frame describing the bearing motion, a highly precise air phase flow model inside the angular contact ball bearing cavity was build up. Comprehensive factors such as bearing revolution, ball rotation, and cage structure were considered to investigate the influences on the air phase flow and heat transfer efficiency. The aerodynamic noise was also analyzed. The result shows that the ball spinning leads to the pressure rise and uneven pressure distribution. The air phase velocity, pressure and cage heat transfer efficiency increase as the revolving speed increases. The operating noise is largely due to the impact of the high speed external flow on the bearing. When the center of the oil-air outlet fixes near the inner ring, the aerodynamic noise is reduced. The position near the inner ring on the bigger axial side is the ideal position to fix the lubricating device for the angular contact ball bearing. 展开更多
关键词 high speed angular contact ball bearing air phase flow heat transfer efficiency cage structure
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Computational and experimental analysis of Mach 2 air flow over a blunt body with plasma aerodynamic actuation 被引量:10
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作者 SUN Quan CHENG BangQin +4 位作者 LI YingHong KONG WeiSong LI Jun ZHU YiFei JIN Di 《Science China(Technological Sciences)》 SCIE EI CAS 2013年第4期795-802,共8页
According to the mechanism of the arc plasma heating effect,and from a phenomenological perspective of view,the plasma actuation was simplified as heating energy injected into the supersonic flow field for the numeric... According to the mechanism of the arc plasma heating effect,and from a phenomenological perspective of view,the plasma actuation was simplified as heating energy injected into the supersonic flow field for the numerical research on controlling detached shock of the blunt body in non-center symmetrical positions.Besides,experimental research on the form and strength of detached shock wave control by plasma aerodynamic actuation in non-center symmetrical positions was conducted in a high-speed shock tunnel(M=2).The results showed that the detached distance of shock wave increased and the strength of normal shock wave ahead of the detached shock wave reduced when plasma actuation was applied.The control effect was greatly improved after the magnetic field was applied and the effect of upwind-direction flow was the best one.When the upwind-direction flow was applied with 1000 V voltage actuation,the distance of detached shock wave would increase from 3.4 to 7.6 mm and the time average strength of normal shock wave was weaken by 5.5%.At last,the mechanism of plasma actuation on controlling the detached shock wave was briefly analyzed. 展开更多
关键词 blunt body detached shock wave SUPERSONIC PLASMA shock tunnel
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Bifurcation analysis for vibrations of a turbine blade excited by air flows 被引量:7
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作者 WANG Dan CHEN YuShu +1 位作者 HAO ZhiFeng CAO QingJie 《Science China(Technological Sciences)》 SCIE EI CAS CSCD 2016年第8期1217-1231,共15页
A reduced three-degree-of-freedom model simulating the fluid-structure interactions (FSI) of the turbine blades and the on- coming air flows is proposed. The equations of motions consist of the coupling of bending a... A reduced three-degree-of-freedom model simulating the fluid-structure interactions (FSI) of the turbine blades and the on- coming air flows is proposed. The equations of motions consist of the coupling of bending and torsion of a blade as well as a van der Pol oscillation which represents the time-varying of the fluid. The 1:1 internal resonance of the system is analyzed with the multiple scale method, and the modulation equations are derived. The two-parameter bifurcation diagrams are computed. The effects of the system parameters, including the detuning parameter and the reduced frequency, on responses of the struc- ture and fluid are investigated. Bifurcation curves are computed and the stability is determined by examining the eigenvalues of the Jacobian matrix. The results indicate that rich dynamic phenomena of the steady-state solutions including the sad- dle-node and Hopf bifurcations can occur under certain parameter conditions. The parameter region where the unstable solu- tions occur should be avoided to keep the safe operation of the blades. The analytical solutions are verified by the direct nu- merical simulations. 展开更多
关键词 fluid-structure interaction (FSI) internal resonance two-parameter bifurcation diagram saddle-node bifurcation Hopf bifurcation direct numerical simulation
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