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配备光离子化检测器的微型气相色谱仪快速测定挥发性有机物 被引量:4
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作者 王海龙 付龙文 +2 位作者 陈令新 孙圣坤 鲍春 《环境化学》 CAS CSCD 北大核心 2016年第6期1189-1195,共7页
将自主研制的光离子化检测器(PID)配备在研发的微型气相色谱仪GC190A上,以空气为载气,用于苯系挥发性有机物(VOCs)的快速灵敏分析.无需样品前处理,将标准气体稀释,即可实现快速测定.实验表明,对挥发性有机物苯、甲苯、乙苯、对间二甲苯... 将自主研制的光离子化检测器(PID)配备在研发的微型气相色谱仪GC190A上,以空气为载气,用于苯系挥发性有机物(VOCs)的快速灵敏分析.无需样品前处理,将标准气体稀释,即可实现快速测定.实验表明,对挥发性有机物苯、甲苯、乙苯、对间二甲苯、邻二甲苯和苯乙烯六种成份的低浓度样品气分析,重现性良好,其中对浓度3.02 mg·m^(-3)的6次分析结果的相对标准偏差低于2.87%,对苯的检测限低至0.3 nmol·mol^(-1).该微型色谱仪具有灵敏度高、稳定性好、体积小、重量轻、经济环保、现场快速分析等特点,操作简单,作为产品方便客户使用,具有广阔的市场前景. 展开更多
关键词 光离子化检测器 微型相色谱 空气载气 电动自动进样 自动分析 挥发性有机物(VOCs)
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Superposability of unsteady aerodynamic loads on bridge deck sections 被引量:2
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作者 张志田 葛耀君 张伟峰 《Journal of Central South University》 SCIE EI CAS 2013年第11期3202-3215,共14页
The 2-dimensional unsteady aerodynamic forces,in the context of both a thin airfoil where theory of potential flow is always applicable and a bluff bridge-deck section where separated flow is typically induced,are inv... The 2-dimensional unsteady aerodynamic forces,in the context of both a thin airfoil where theory of potential flow is always applicable and a bluff bridge-deck section where separated flow is typically induced,are investigated from a point of view of whether or not they conform to the principle of linear superposition in situations of various structural motions and wind gusts.It is shown that some basic preconditions that lead to the linear superposability of the unsteady aerodynamic forces in cases of thin airfoil sections are no longer valid for a bluff section.Theoretical models of bridge aerodynamics such as the one related to flutter-buffeting analysis and those concerning aerodynamic admittance(AA)functions,however,necessitate implicitly this superposability.The contradiction revealed in this work may throw light on the perplexing problem of AA functions pertaining to the description of buffeting loads of bridge decks.Some existing theoretical AA models derived from flutter derivatives according to interrelations valid only for thin airfoil theories,which have been employed rather extensively in bridge aerodynamics,are demonstrated to be illogical.Finally,with full understanding of the preconditions of the applicability of linear superposability of the unsteady aerodynamic forces,suggestions in regard to experiment-based AA functions are presented. 展开更多
关键词 bridge unsteady load aerodynamic load SUPERPOSITION BUFFETING FLUTTER
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TBCs for Gas Turbines under Thermomechanical Loadings: Failure Behaviour and Life Prediction 被引量:8
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作者 Tilmann Beck Olena Trunova +1 位作者 Roland Herzog Lorenz Singheiser 《Journal of Energy and Power Engineering》 2013年第4期647-653,共7页
The present contribution gives an overview about recent research on a TBC (thermal barrier coating) system consisted of (I) an intermetallic MCrAIY-alloy BC (bond coat) applied by VPS (vacuum plasma spraying) ... The present contribution gives an overview about recent research on a TBC (thermal barrier coating) system consisted of (I) an intermetallic MCrAIY-alloy BC (bond coat) applied by VPS (vacuum plasma spraying) and (2) an YSZ (yttria stabilised zirconia) top coat APS (air plasma sprayed) at Forschungszentrum Juelich, Institute of Energy and Climate Research (IEK-2). The influence of high temperature dwell time, maximum and minimum temperature on crack growth kinetics during thermal cycling of such plasma sprayed TBCs is investigated using scanning electron microscopy and AE (acoustic emission) analysis. Thermocyclic life in terms of accumulated time at maximum temperature decreases with increasing high temperature dwell time and increases with increasing minimum temperature. AE analysis proves that crack growth mainly occurs during cooling at temperatures below the ductile-to-brittle transition temperature of the BC. Superimposed mechanical load cycles accelerate delamination crack growth and, in case of sufficiently high mechanical loadings, result in premature fatigue failure of the substrate. A life prediction model based on TGO growth kinetics and a fracture mechanics approach has been developed which accounts for the influence of maximum and minimum temperature as well as of high temperature dwell time with good accuracy in an extremely wide parameter range. 展开更多
关键词 Thermal barrier coating spallation failure crack propagation thermomechanical fatigue lifetime prediction.
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Experimental research on air film formation behavior of air cushion belt conveyor with stable load 被引量:6
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作者 GUO Sheng LIU Jian +2 位作者 LI ZhiRen ZHANG DongLi HUANG Wei 《Science China(Technological Sciences)》 SCIE EI CAS 2013年第6期1424-1434,共11页
In this paper, the air film formation behavior of air cushion belt conveyor with stable load is studied. The air cushion field is analyzed by means of theoretical derivation, numerical simulation and experimental rese... In this paper, the air film formation behavior of air cushion belt conveyor with stable load is studied. The air cushion field is analyzed by means of theoretical derivation, numerical simulation and experimental research. An intelligent experiment platform is developed. Three dimensional pressure distribution of air film and the air film thickness distribution along the conveyor belt in the width direction are obtained. The experimental result is analyzed by comparing with theoretical calculation and numerical simulation. The numerical and theoretical results are in good agreement with those obtained from experiments. The air film formation behavior pattern of air cushion belt conveyor with stable load is presented. The optimized film thickness and pore distribution are obtained based on the comprehensive energy consumption. This study provides a basis for the optimization design of air cushion belt conveyor. 展开更多
关键词 air cushion belt conveyor stable load air film formation behaviour energy consumption analysis
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