复方醋酸钠林格注射液中无水葡萄糖含量测定方法的建立及葡萄糖转化现象的探讨

目的建立复方醋酸钠林格注射液中无水葡萄糖含量测定方法,并针对方法建立中发现的葡萄糖转化问题开展研究。方法采用氨基硅烷键合硅胶为填充剂的色谱柱;以乙腈-水-氨水(体积比75∶25∶0.1)为流动相;示差折光检测器检测;流速为1.0 mL/min,柱温和检测池温度均为40℃。结果无水葡萄糖浓度在0.4125~8.249 mg/mL范围内线性关系良好(r=1.0000),定量限为101μg/L,平均回收率为100.5%,RSD为0.5%,采用该测定法发现样品中少量葡萄糖转化为果糖。结论建立的方法简单、准确、灵敏度高,不受葡萄糖转化现象的干扰,适用于复方醋酸钠林格注射液中无水葡萄糖的含量测定。

关于平坦地区大比例尺航测成图几个问题的探讨

一 立测综合法测图平坦地区进行航测大比例尺测图,由于内业所测高程难以满足成图精度要求,所以高程普遍采用野外实测办法;

利用“立杆测影”法开展课外活动

地理学的区域性特征要求地理教学必须培养学生区域位置判读的能力，这在近年来高考试题中已得到充分体现，但区域位置的判读，特别是利用经纬线来判读某地的区域位置，历来是高三学生复习的难点。为此，在学生对主要地理事物的相对位置已有一定掌握的基础上，采用建构经纬网格，以专题形式的复习方法，可以帮助学生理清头绪从宏观把握区域位置。

“干阑”建筑的历史演变——一种原建筑发生学的阐释

运用建筑人类学方法构建中国古代干阑建筑独特的文化模式和语言逻辑表达式。这种独特的干阑建筑文化模式和榫卯框架结构模式,为人类社会生产、生活实践提供了一种具有想象力和创造力的建筑语言逻辑。从"干阑"的语音、语义及其文字结构演变来看,"干"与"杆"、"阑"与"栏"语音相谐,语义相通,其字互为通假,这种语音、语义及其及文字的演变过程,充分证明了干阑建筑榫卯框架结构原发生学的过程。

Method of Growth in Finding the Test Cube of Industrial Robots

In order to find the test cube for industrial robots as specified by ISO 9283, a seed cube is grown up in an irregular working space of the robot, provided that the corners of the cube do not exceed the boundary of the working space. All possible cubes are searched, and the cube with the maximum volume is selected. The calculation examples show that the method of growth can be used for a variety of industrial robots. The method of growth can determine the test cube and test points of irregular working space according to ISO 9283, and can avoid blindness and randomness in the selection of test points.

MGB probe assay for rapid detection of mtDNA11778 mutation in the Chinese LHON patients by real-time PCR

Objective： Leber＇s hereditary optic neuropathy （LHON） is a maternally inherited degeneration of the optic nerve caused by point mutations of mitochondrial DNA （mtDNA）. Many unsolved questions regarding the penetrance and pathophysiological mechanism of LHON demand efficient and reliable mutation testing. This study aims to develop a minor groove binder （MGB） probe assay for rapid detection of mtDNA11778 mutation and heteroplasmy in Chinese LHON patients by real-time polymerase chain reaction （PCR）. Methods： Forty-eight patients suspected of having LHON and their maternal relatives underwent a molecular genetic evaluation, with 20 normal individuals as a control group at the same time. A real-time PCR involving two MGB probes was used to detect the mtDNA 1 1778 mutation and heteroplasmy. A linear standard curve was obtained by pUCmLHONG and pUCmLHONA clones. Results： All 48 LHON patients and their maternal relatives were positive for rntDNA11778 mutation in our assay, 27 heteroplasmic and 21 homoplasmic. Eighteen cases did not show an occurrence of the disease, while 9 developed the disease among the 27 heteroplasmic mutation cases. Eleven did not show an occurrence of the disease, while 10 cases developed the disease among 21 homoplasmic mutation cases. There was a significant difference in the incidence between the heteroplasmic and the homoplasmic mutation types. The time needed for running a real-time PCR assay was only 80 min. Conclusion： This real-time PCR assay is a rapid, reliable method for mtDNA mutation detection as well as heteroplasmy quantification. Detecting this ratio is very important for predicting phenotypic expression of unaffected carriers.

Determination of Ash Contents in Coal by Means of Ordinary Kriging Method

The ash contents in coal particles were examined in the paper dependably on particle size and its density. So, the two-dimensional regressive function Z = Z（P, D） was the searched object, where Z is random variable describing ash contents, P---density and D---particle diameter. This dependence was determined based on experimental data concerning the coal of type 31. For this coal, the method of ordinary kriging was applied to calculate the values of random variable Z. This method required the proper selection of so-called variogram function, in which four forms were considered in this paper in purpose to select the best solution. The given results were then evaluated by the mean standard error value and compared with empirical data.

OPTIMAL ANTENNA SUBSET SELECTION AND BLIND DETECTION APPROACH APPLIED TO ORTHOGONAL SPACE-TIME BLOCK CODING

An approach combining optimal antenna subset selection with blind detection scheme for Orthogonal Space-Time Block Coding (OSTBC) is proposed in this paper. The optimal antenna sub- set selection is taken into account at transmitter and/or receiver sides, which chooses the optimal an- tennas to increase the diversity order of OSTBC and improve further its performance. In order to en- hance the robustness of the detection used in the conventional OSTBC scheme, a blind detection scheme based on Independent Component Analysis (ICA) is exploited which can directly extract transmitted signals without channel estimation. Performance analysis shows that the proposed ap- proach can achieve the full diversity and the flexibility of system design by using the antenna selec-tion and the ICA based blind detection schemes.

Diverse Voices and Democratic Policymaking： What Causes Japan＇s Nuclear Phase-Out Plan to Fail？

The nuclear disaster at Fukushima has raised questions about the nature of democratic policymaking in Japan. Focusing on nuclear policymaking post-Fukushima, this paper considers ways in which the diversity of public opinion can be connected with legislative processes. The disaster forced the government to rethink existing nuclear policies. To infuse public voices into government policy, the Democratic Party of Japan （DPJ） government introduced a new method of public participation called ＂national debates＂, comprising a series of public hearings, mass public comments, and deliberative polling. The government also attached importance to anti-nuclear rallies and opinion polls conducted by the media. The national debates highlighted that the majority of Japanese people supported a nuclear-free society; as a result, the government drafted a new energy plan to phase out nuclear power by 2039. Owing to both domestic and international opposition, the plan failed to become law. Progress was also impeded by the public＇s contradictory demands. However, this paper posits that inefficient legislative deliberation was the main factor behind the policy failure. The Japanese case suggests that effective legislative deliberation is crucial to assessing and coordinating numerous divergent public voices.

A New Transient Impedance-Based Algorithm for Earth Fault Detection in Medium Voltage Networks

This paper presents a new earth-fault detection algorithm for unearthed （isolated） and compensated neutral medium voltage （MV） networks. The proposed algorithm is based on capacitance calculation from transient impedance and dominant transient frequency. The Discrete Fourier Transform （DFT） method is used to determine the dominant transient frequency. The values of voltage and current earth modes are calculated in the period of the dominant transient frequency, then the transient impedance can be determined, from which we can calculate the earth capacitance. The calculated capacitance gives an indication about if the feeder is faulted or not. The algorithm is less dependent on the fault resistance and the faulted feeder parameters; it mainly depends on the background network. The network is simulated by ATP/EMTP program. Several different fault conditions are covered in the simulation process, different fault inception angles, fault locations and fault resistances.

Projections of Wind Changes for 21st Century in China by Three Regional Climate Models

This paper examines the capability of three regional climate models (RCMs), i.e., RegCM3 (the International Centre for Theoretical Physics Regional Climate Model), PRECIS (Providing Regional Climates for Impacts Studies) and CMM5 (the fifth-generation Pennsylvania State University-the National Center for Atmospheric Research of USA, NCAR Mesoscale Model) to simulate the near-surface-layer winds (10 m above surface) all over China in the late 20th century. Results suggest that like global climate models (GCMs), these RCMs have the certain capability of imitating the distribution of mean wind speed and fail to simulate the greatly weakening wind trends for the past 50 years in the country. However, RCMs especially RegCM3 have the better capability than that of GCMs to simulate the distribution and change feature of mean wind speed. In view of their merits, these RCMs were used to project the variability of near-surface-layer winds over China for the 21st century. The results show that 1) summer mean wind speed for 2020-2029 will be lower compared to those in 1990-1999 in most area of China; 2) annual and winter mean wind speed for 2081-2100 will be lower than those of 1971-1990 in the whole China; and 3) the changes of summer mean wind speed for 2081-2100 are uncertain. As a result, although climate models are absolutely necessary for projecting climate change to come, there are great uncertainties in projections, especially for wind speed, and these issues need to be further explored.

Measurement and characteristics of ground vibration caused by blasting demolition of urban overpass

To analyze the characteristics of ground vibration caused by blasting demolition of urban overpass, in this paper we introduced the measurement method and then studied the characteristics of recorded ground vi- brations. Through the analysis of peak acceleration, peak frequency and duration, results indicated that the ver- tical component of vibration is the most important in the region close to the collapse point; the collapse of bridge segments will lead to superposition of ground vibration, and isolation measures can reduce the peak ac- celeration but increase the duration of vibration; blasting and collapse vibration cause no damage to the re- served structure which indicates that blastin~ demolition is a safe and effective method.

Micro-Displace Sensor Based on Self-Mixing Interference of the Fiber Laser With Phase Modulation

Micro-displacement measurement based on self-mixing interference using a fiber laser system was demonstrated. The sinusoidal phase modulation technique was introduced into the fiber laser self-mixing interference measurement system to improve the measurement resolution. The phase could be demodulated by the Fourier analysis method. Error sources were evaluated in detail, and the system was experimentally applied to reconstruct the motion of a high-precision commercial piezoelectric ceramic transducer （PZT）. The displacement measurement resolution was well beyond a half-wavelength. It provides a practical solution for displacement measurement based on all optical-fiber sensing applications with high precision.

Numerical and Experimental Study on Aerodynamic Performance of Small Axial Flow Fan with Splitter Blades

To improve the aerodynamic performance of small axial flow fan, in this paper the design of a small axial flow fan with splitter blades is studied. The RNG k-e turbulence model and SIMPLE algorithm were applied to the steady simulation calculation of the flow field, and its result was used as the initial field of the large eddy simulation to calculate the unsteady pressure field. The FW-H noise model was adopted to predict aerodynamic noise in the six monitoring points. Fast Fourier transform algorithm was applied to process the pressure signal. Experiment of noise testing was done to further investigate the aerodynamic noise of fans. And then the results obtained from the numerical simulation and experiment were described and analyzed. The results show that the static characteristics of small axial fan with splitter blades are similar with the prototype fan, and the static characteristics are improved within a certain range of flux. The power spectral density at the six monitoring points of small axial flow fan with splitter blades have decreased to some extent. The experimental results show sound pressure level of new fan has reduced in most frequency bands by comparing with prototype fan. The research results will provide a proof for parameter optimization and noise prediction of small axial flow fans with high performance.

GROUP CONTINGENCY TEST FOR TWO OR SEVERAL INDEPENDENT SAMPLES

This paper proposes a new and distribution-free test called ＂Group Contingency＂ test （GC, for short） for testing two or several independent samples. Compared with traditional nonparametric tests, GC test tends to explore more information based on samples, and it＇s location-, scale-, and shapesensitive. The authors conduct some simulation studies comparing GC test with Wilcoxon rank sum test （W）, Kolmogorov-Smirnov test （KS） and Wald-Wolfowitz runs test （WW） for two sample case, and with Kruskal-Wallis （KW） for testing several samples. Simulation results reveal that GC test usually outperforms other methods.