The simple approach to acquire the fltaxescenee spectra of vitamin bl, b2 and t6 is proposed by direct ilhanination on solid powder sample. The experimentally acquired fluorescence spectra are in accordance with the p...The simple approach to acquire the fltaxescenee spectra of vitamin bl, b2 and t6 is proposed by direct ilhanination on solid powder sample. The experimentally acquired fluorescence spectra are in accordance with the previous measurements on soluble samples. The fluorescence spectra for a mixture of vitamins bl, b2 and b6 with different concentrations have been investigated, and the fluorescence mechanism is explained on the basis of moleoalar struchture Possible reasons of the blue-shift of the fluorescence peak and enhancement of the peak power are explained as well. The advantages of solid powder method is analyzed and discussed.展开更多
An industrialized technique of preparation for oxidized com starch using oxygen as oxidant was investigated in this paper. The industrialized preparation parameters were optimized as follows： reaction temperature 85-...An industrialized technique of preparation for oxidized com starch using oxygen as oxidant was investigated in this paper. The industrialized preparation parameters were optimized as follows： reaction temperature 85-95 ℃, oxygen flow rate 8-12 L/min, reaction time 210 min, the ratio of starch to water 1：5, 3.5 wt% of NaOH and 0.1 wt% of catalyst. The experimental results show that the concentration of hydrolysate-oxidaton product is 16-18 wt%. The powdered products were gained through dehydrated and powdered process using quadruple-effect evaporator, spray drying tower and guide shell mixer. The composting test indicates that the degradability of the oxidized corn starch can reach 76.4%. The complexation capacity of calcium ions reaches 108.5 mg per gram oxidized starch, and the detergency ratio （P） reaches 1.30 as builder.展开更多
基金supported by the Tianjin Natural Science Foundation(No.06YFJZJC00300)the Natural Science Foundation of China(Nos.10674075,10774077,10674074,50802044 and 60736039)
文摘The simple approach to acquire the fltaxescenee spectra of vitamin bl, b2 and t6 is proposed by direct ilhanination on solid powder sample. The experimentally acquired fluorescence spectra are in accordance with the previous measurements on soluble samples. The fluorescence spectra for a mixture of vitamins bl, b2 and b6 with different concentrations have been investigated, and the fluorescence mechanism is explained on the basis of moleoalar struchture Possible reasons of the blue-shift of the fluorescence peak and enhancement of the peak power are explained as well. The advantages of solid powder method is analyzed and discussed.
文摘An industrialized technique of preparation for oxidized com starch using oxygen as oxidant was investigated in this paper. The industrialized preparation parameters were optimized as follows： reaction temperature 85-95 ℃, oxygen flow rate 8-12 L/min, reaction time 210 min, the ratio of starch to water 1：5, 3.5 wt% of NaOH and 0.1 wt% of catalyst. The experimental results show that the concentration of hydrolysate-oxidaton product is 16-18 wt%. The powdered products were gained through dehydrated and powdered process using quadruple-effect evaporator, spray drying tower and guide shell mixer. The composting test indicates that the degradability of the oxidized corn starch can reach 76.4%. The complexation capacity of calcium ions reaches 108.5 mg per gram oxidized starch, and the detergency ratio （P） reaches 1.30 as builder.
