The mechanisms responsible for deformation behavior in Nb/NiTi composite during pre-straining were investigated systematically using in-situ synchrotron X-ray diffraction, transmission electron microscopy and tensile ...The mechanisms responsible for deformation behavior in Nb/NiTi composite during pre-straining were investigated systematically using in-situ synchrotron X-ray diffraction, transmission electron microscopy and tensile test. It is shown that upon loading, the composite experiences elastic elongation and slight plastic deformation of B19′,B2 and β-Nb phases, together with the forward stress-induced martensitic(SIM) transformation from B2 to B19′. Upon unloading, the deformation mechanisms of the composite mainly involve elastic recovery of B19′, B2 and β-Nb phases,compression deformation of β-Nb phase and incomplete B19′→B2 reverse SIM transformation. In the tensile loading-unloading procedure, besides the inherent elastic deformation and SIM transformation, the(001) compound twins in B19′ martensite can also be conducive to the elastic deformation occurring in B19′-phase of the composite.Therefore, this composite can exhibit a large recoverable strain after unloading owing to the elastic deformation, and the partially reversible and consecutive SIM transformation together with the(001) compound twins.展开更多
基金the National Natural Science Foundation of China (Nos.51771082,51971009,52175410,51801076)the Six Talent Peaks Project in Jiangsu Province,China (No.2019-XCL-113)+2 种基金Zhenjiang Science & Technology Program,China (No.GY2020001)Project of Faculty of Agricultural Equipment of Jiangsu University,China (No.NZXB20200101)the US Department of Energy,Office of Science and Office of Basic Energy Science (No.DE-AC02-06CH11357) for providing the Advanced Photon Source。
文摘The mechanisms responsible for deformation behavior in Nb/NiTi composite during pre-straining were investigated systematically using in-situ synchrotron X-ray diffraction, transmission electron microscopy and tensile test. It is shown that upon loading, the composite experiences elastic elongation and slight plastic deformation of B19′,B2 and β-Nb phases, together with the forward stress-induced martensitic(SIM) transformation from B2 to B19′. Upon unloading, the deformation mechanisms of the composite mainly involve elastic recovery of B19′, B2 and β-Nb phases,compression deformation of β-Nb phase and incomplete B19′→B2 reverse SIM transformation. In the tensile loading-unloading procedure, besides the inherent elastic deformation and SIM transformation, the(001) compound twins in B19′ martensite can also be conducive to the elastic deformation occurring in B19′-phase of the composite.Therefore, this composite can exhibit a large recoverable strain after unloading owing to the elastic deformation, and the partially reversible and consecutive SIM transformation together with the(001) compound twins.