The flow behavior and dynamic recrystallization（DRX） behavior of an as-cast AZ91 D alloy were investigated systematically by applying the isothermal compression tests in temperature range of 220-380 ℃ and strain ra...The flow behavior and dynamic recrystallization（DRX） behavior of an as-cast AZ91 D alloy were investigated systematically by applying the isothermal compression tests in temperature range of 220-380 ℃ and strain rate range of 0.001-1 s^-1.The effect of temperature and strain rate on the DRX behavior was discussed.The results indicate that the nucleation and growth of dynamic recrystallized grains easily occur at higher temperatures and lower strain rates.To evaluate the evolution of dynamic recrystallization,the DRX kinetics model was proposed based on the experimental data of true stress-true strain curves.It was revealed that the volume fraction of dynamic recrystallized grains increased with increasing strain in terms of S-curves.A good agreement between the proposed DRX kinetics model and microstructure observation results validates the accuracy of DRX kinetics model for AZ91 D alloy.展开更多
In order to describe and predict the kinetic process of discontinuous dynamic recrystallization （DDRX） during hot workingfor metals with low to medium stacking fault energies quantitatively, a new physically-based m...In order to describe and predict the kinetic process of discontinuous dynamic recrystallization （DDRX） during hot workingfor metals with low to medium stacking fault energies quantitatively, a new physically-based model was proposed by considering thecharacteristics of grain size distribution, capillary effect of initial grain boundaries （GBs） and continuous consumption of GBs. UsingIncoloy 028 alloy as a model system, experiments aiming to provide kinetic data （e.g., the size and volume fraction of recrystallizedgrain） and the associated microstructure were performed. Good agreement is obtained between model predictions and experimentalresults, regarding flow stress, recrystallized fraction and grain size evolution. On this basis, a thermo-kinetic relationship upon thegrowth of recrystallized grain was elucidated, i.e., with increasing thermodynamic driving force, the activation energy barrierdecreases.展开更多
Based on the steady-state strain measured by single-pass hot compression tests,the method by a double-pass hot compression testing was developed to measure the metadynamic-recrystallization kinetics.The metadynamic re...Based on the steady-state strain measured by single-pass hot compression tests,the method by a double-pass hot compression testing was developed to measure the metadynamic-recrystallization kinetics.The metadynamic recrystallization behavior of low-alloy steel Q345B during hot compression deformation was investigated in the temperature range of 1 000-1 100℃,the strain rate range of 0.01-0.10 s -1 and the interpass time range of 0.5-50 s on a Gleeble-3500 thermo-simulation machine.The results show that metadynamic recrystallization during the interpass time can be observed.As the deformation temperature and strain rate increase,softening caused by metadynamic recrystallization is obvious.According to the data of thermo-simulation,the metadynamic recrystallization activation energy is obtained to be Qmd=100.674 kJ/mol and metadynamic recrystallization kinetics model is set up.Finally,the error analysis of metadynamic recrystallization kinetics model proves that the model has high accuracy(correlation coefficient R=0.988 6).展开更多
The batch cooling crystallization initiated from spontaneous nucleation for aqueous solution of potassium nitrate was studied. The concentration and transmittance data were acquired on line throughout the operation.Ba...The batch cooling crystallization initiated from spontaneous nucleation for aqueous solution of potassium nitrate was studied. The concentration and transmittance data were acquired on line throughout the operation.Based on solute mass transfer in both liquid and solid phases, a kinetic model was deduced by assuming that the late period of primary nucleation resembles the initial period of the secondary nucleation. Nucleation and crystal growth stages were identified. Kinetic parameters were estimated piecewise from online experimental data and compared with those in literature. The estimated kinetic parameters for stages without apparent primary nucleation agreed well with those in literature. Further, a simulated concentration curve was also drawn from the estimated kinetic parameters and it matched well with that in experiment.展开更多
基金Project (51075098) supported by the National Natural Science Foundation of ChinaProject (HIT.NSRIF.2014006) supported by the Fundamental Research Funds for the Central Universities,China
文摘The flow behavior and dynamic recrystallization（DRX） behavior of an as-cast AZ91 D alloy were investigated systematically by applying the isothermal compression tests in temperature range of 220-380 ℃ and strain rate range of 0.001-1 s^-1.The effect of temperature and strain rate on the DRX behavior was discussed.The results indicate that the nucleation and growth of dynamic recrystallized grains easily occur at higher temperatures and lower strain rates.To evaluate the evolution of dynamic recrystallization,the DRX kinetics model was proposed based on the experimental data of true stress-true strain curves.It was revealed that the volume fraction of dynamic recrystallized grains increased with increasing strain in terms of S-curves.A good agreement between the proposed DRX kinetics model and microstructure observation results validates the accuracy of DRX kinetics model for AZ91 D alloy.
基金Project(51431008)supported by the National Natural Science Foundation of ChinaProjects(2017YFB0703001,2017YFB0305100)supported by the National Key Research and Development Program of China
文摘In order to describe and predict the kinetic process of discontinuous dynamic recrystallization （DDRX） during hot workingfor metals with low to medium stacking fault energies quantitatively, a new physically-based model was proposed by considering thecharacteristics of grain size distribution, capillary effect of initial grain boundaries （GBs） and continuous consumption of GBs. UsingIncoloy 028 alloy as a model system, experiments aiming to provide kinetic data （e.g., the size and volume fraction of recrystallizedgrain） and the associated microstructure were performed. Good agreement is obtained between model predictions and experimentalresults, regarding flow stress, recrystallized fraction and grain size evolution. On this basis, a thermo-kinetic relationship upon thegrowth of recrystallized grain was elucidated, i.e., with increasing thermodynamic driving force, the activation energy barrierdecreases.
基金Project(101048) supported by Fok Ying Tung Education FoundationProject(E2008000835) supported by the Natural Science Foundation of Hebei Province,China
文摘Based on the steady-state strain measured by single-pass hot compression tests,the method by a double-pass hot compression testing was developed to measure the metadynamic-recrystallization kinetics.The metadynamic recrystallization behavior of low-alloy steel Q345B during hot compression deformation was investigated in the temperature range of 1 000-1 100℃,the strain rate range of 0.01-0.10 s -1 and the interpass time range of 0.5-50 s on a Gleeble-3500 thermo-simulation machine.The results show that metadynamic recrystallization during the interpass time can be observed.As the deformation temperature and strain rate increase,softening caused by metadynamic recrystallization is obvious.According to the data of thermo-simulation,the metadynamic recrystallization activation energy is obtained to be Qmd=100.674 kJ/mol and metadynamic recrystallization kinetics model is set up.Finally,the error analysis of metadynamic recrystallization kinetics model proves that the model has high accuracy(correlation coefficient R=0.988 6).
文摘The batch cooling crystallization initiated from spontaneous nucleation for aqueous solution of potassium nitrate was studied. The concentration and transmittance data were acquired on line throughout the operation.Based on solute mass transfer in both liquid and solid phases, a kinetic model was deduced by assuming that the late period of primary nucleation resembles the initial period of the secondary nucleation. Nucleation and crystal growth stages were identified. Kinetic parameters were estimated piecewise from online experimental data and compared with those in literature. The estimated kinetic parameters for stages without apparent primary nucleation agreed well with those in literature. Further, a simulated concentration curve was also drawn from the estimated kinetic parameters and it matched well with that in experiment.
