本文设计了一套真空搅拌法流态冰制取装置,对冰浆的生成全过程进行了观测,通过实验研究了乙二醇添加剂、溶液体积、搅拌速度等因素对冰浆形成过程过冷状态的影响。结果表明:真空状态下冰浆的制取需经历溶液蒸发、沸腾、过冷及冰晶生成...本文设计了一套真空搅拌法流态冰制取装置,对冰浆的生成全过程进行了观测,通过实验研究了乙二醇添加剂、溶液体积、搅拌速度等因素对冰浆形成过程过冷状态的影响。结果表明:真空状态下冰浆的制取需经历溶液蒸发、沸腾、过冷及冰晶生成这四个阶段;冰晶生成瞬间系统的压力会发生突增,压力的升值即过冷结晶压差可用于表征过冷程度的高低;平均过冷结晶压差随乙二醇添加剂浓度的增大而减小,当乙二醇浓度从3%提高至6%时,过冷结晶压差从58.9 Pa降至49.4 Pa,降低了16.1%;溶液体积的增大会使平均过冷结晶压差减小,40 m L溶液的平均过冷结晶压差较20 m L溶液的平均过冷结晶压差下降了12.9%;搅拌速度对过冷程度几乎无影响。展开更多
An innovative approach was introduced for the development of a AA6063 recrystallization model.This method incorporated a regression-based technique for the determination of material constants and introduced novel equa...An innovative approach was introduced for the development of a AA6063 recrystallization model.This method incorporated a regression-based technique for the determination of material constants and introduced novel equations for assessing the grain size evolution.Calibration and validation of this methodology involved a combination of experimentally acquired microstructural data from the extrusion of three different AA6063 profiles and results from the simulation using the Qform Extrusion UK finite element code.The outcomes proved the agreement between experimental findings and numerical prediction of the microstructural evolution.The trend of the grain size variation based on different process parameters was accurately simulated,both after dynamic and static recrystallization,with an error of less than 25% in almost the whole sampling computations.展开更多
The macroscopic mechanical properties of rocks are significantly influenced by their microstructure.As a material bonded by mineral grains,the grain morphology of crystalline rock is the primary factor influencing the...The macroscopic mechanical properties of rocks are significantly influenced by their microstructure.As a material bonded by mineral grains,the grain morphology of crystalline rock is the primary factor influencing the strength.However,most strength criteria neglect the strength variations caused by different grain characteristics in rocks.Furthermore,the traditional linear criteria tend to overestimate tensile strength and exhibit apex singularity.To address these shortcomings,a piecewise strength criterion that considers the grain size effect has been proposed.A part of an ellipse was employed to construct the envelope of the tensive-shear region on the meridian plane,to accurately reproduce the low tensile-compressive strength ratio.Based on the analysis of experimental data,both linear and exponential modification functions that account for grain size effects were integrated into the proposed criterion.The corresponding finite element algorithm has been implemented.The accuracy and applicability of the proposed criterion were validated by comparing with the experimental data.展开更多
The multi-pass hot compression test of 7055 aluminum alloy was performed at different temperatures and then the samples were heat treated by T6 heat treatment.The compressed samples were analyzed by OM and TEM.The res...The multi-pass hot compression test of 7055 aluminum alloy was performed at different temperatures and then the samples were heat treated by T6 heat treatment.The compressed samples were analyzed by OM and TEM.The results reveal that the average aspect ratio of the grains in the specimens compressed first decreases and then increases,the dislocation density decreases and subgrain diameter increases with the increase of deformation temperature.The effects of deformation temperature on the microstructure and mechanical properties of 7055 aluminum alloy after heat treatment were investigated by means of OM and mechanical property test.The results indicate that the deformation temperature significantly influences microstructure and mechanical property of 7055 aluminum alloy.The volume fraction of recrystallization grains presents a ＂fall-rise＂ pattern with the deformation temperature rising.The mechanical properties get better when the volume fraction of recrystallization grains decreases.Moreover,the volume fraction of recrystallization grain has a minimum value,appropriately 45%,and the sample exhibits the highest strength and elongation at the deformation temperature of 400 ℃.展开更多
Standard mechanical test bars with a diameter of 6.4 mm and a gauge length of 50 mm were processed, and the microstructures of die cast AM60B alloy under different die casting process parameters were observed. The inf...Standard mechanical test bars with a diameter of 6.4 mm and a gauge length of 50 mm were processed, and the microstructures of die cast AM60B alloy under different die casting process parameters were observed. The influences of the slow shot speed, the fast shot speed and the biscuit thickness on the externally solidified crystals （ESCs） were investigated. With the increase of the biscuit thickness, the number of the ESCs in the cast samples decreases. Under a low slow shot speed, larg ESCs are found in the cast structure and a high fast shot speed results in more spherical ESCs. The relationships between ESCs and process parameters were also discussed.展开更多
The microstructure and mechanical properties of the Mg-6Zn-xEr alloys in the as-cast, as-extruded and extruded-T5 states were investigated. It is found that the addition of Er has an obvious effect on improving mechan...The microstructure and mechanical properties of the Mg-6Zn-xEr alloys in the as-cast, as-extruded and extruded-T5 states were investigated. It is found that the addition of Er has an obvious effect on improving mechanical properties of Mg-6Zn based alloys. The results suggest that the Mg-6Zn-0.5Er alloy in the peak aged state shows the best tensile strength. The ultimate tensile strength and the yield tensile strength of the peak-aged Mg-6Zn-0.5Er alloy are about 329 MPa and 183 MPa, respectively, companying with a good elongation of 12%. The addition of 0.5% Er into the Mg-6Zn based alloys has a great effect on improving ageing hardening response. The highest tensile strength of the peak-aged Mg-6Zn-0.5Er alloy is mainly due to the refinement of microstructure and the precipitation of β1 phase.展开更多
The effects of vacuum assistance on the microstructure and mechanical properties of high-pressure die cast AZ91 D alloy at different slow shot speeds were evaluated. Plate-shaped castings of AZ91 D alloy were carried ...The effects of vacuum assistance on the microstructure and mechanical properties of high-pressure die cast AZ91 D alloy at different slow shot speeds were evaluated. Plate-shaped castings of AZ91 D alloy were carried out on a TOYO BD-350V5 cold chamber die casting machine incorporated with a self-improved TOYO vacuum system. It was found that the vacuum pressure in the die cavity at the beginning of mold filling increases with the increase of slow shot speed, following a cubic polynomial curve, resulting in a decline in the porosity-reduction ability of vacuum assistance with the increase of slow shot speed. The externally solidified crystal（ESC） contents in conventional and vacuum die castings behave similar against the slow shot speed. The tensile properties of vacuum die castings were strongly influenced by the ESC content at relative low slow shot speeds. With the increase of slow shot speed, the influence of the gas porosity level in vacuum die castings would get prominent.展开更多
文摘本文设计了一套真空搅拌法流态冰制取装置,对冰浆的生成全过程进行了观测,通过实验研究了乙二醇添加剂、溶液体积、搅拌速度等因素对冰浆形成过程过冷状态的影响。结果表明:真空状态下冰浆的制取需经历溶液蒸发、沸腾、过冷及冰晶生成这四个阶段;冰晶生成瞬间系统的压力会发生突增,压力的升值即过冷结晶压差可用于表征过冷程度的高低;平均过冷结晶压差随乙二醇添加剂浓度的增大而减小,当乙二醇浓度从3%提高至6%时,过冷结晶压差从58.9 Pa降至49.4 Pa,降低了16.1%;溶液体积的增大会使平均过冷结晶压差减小,40 m L溶液的平均过冷结晶压差较20 m L溶液的平均过冷结晶压差下降了12.9%;搅拌速度对过冷程度几乎无影响。
文摘An innovative approach was introduced for the development of a AA6063 recrystallization model.This method incorporated a regression-based technique for the determination of material constants and introduced novel equations for assessing the grain size evolution.Calibration and validation of this methodology involved a combination of experimentally acquired microstructural data from the extrusion of three different AA6063 profiles and results from the simulation using the Qform Extrusion UK finite element code.The outcomes proved the agreement between experimental findings and numerical prediction of the microstructural evolution.The trend of the grain size variation based on different process parameters was accurately simulated,both after dynamic and static recrystallization,with an error of less than 25% in almost the whole sampling computations.
基金Project(2023YFC2907403)supported by the National Key R&D Program of ChinaProject(52074021)supported by the National Natural Science Foundation of China+1 种基金Project(2242045)supported by Beijing Natural Science Foundation,ChinaProject(ZD202216)supported by the Beijing Association of Higher Education,China。
文摘The macroscopic mechanical properties of rocks are significantly influenced by their microstructure.As a material bonded by mineral grains,the grain morphology of crystalline rock is the primary factor influencing the strength.However,most strength criteria neglect the strength variations caused by different grain characteristics in rocks.Furthermore,the traditional linear criteria tend to overestimate tensile strength and exhibit apex singularity.To address these shortcomings,a piecewise strength criterion that considers the grain size effect has been proposed.A part of an ellipse was employed to construct the envelope of the tensive-shear region on the meridian plane,to accurately reproduce the low tensile-compressive strength ratio.Based on the analysis of experimental data,both linear and exponential modification functions that account for grain size effects were integrated into the proposed criterion.The corresponding finite element algorithm has been implemented.The accuracy and applicability of the proposed criterion were validated by comparing with the experimental data.
基金Project(CHALCO-2007-KJ-02) supported by the Technology Development Program of Aluminum Corporation of ChinaProject (2011BS0802) supported by the Natural Science Foundation of Inner Mongolia,ChinaProject(NJZY11075) supported by the Research Fund for the Higher Education of Inner Mongolia,China
文摘The multi-pass hot compression test of 7055 aluminum alloy was performed at different temperatures and then the samples were heat treated by T6 heat treatment.The compressed samples were analyzed by OM and TEM.The results reveal that the average aspect ratio of the grains in the specimens compressed first decreases and then increases,the dislocation density decreases and subgrain diameter increases with the increase of deformation temperature.The effects of deformation temperature on the microstructure and mechanical properties of 7055 aluminum alloy after heat treatment were investigated by means of OM and mechanical property test.The results indicate that the deformation temperature significantly influences microstructure and mechanical property of 7055 aluminum alloy.The volume fraction of recrystallization grains presents a ＂fall-rise＂ pattern with the deformation temperature rising.The mechanical properties get better when the volume fraction of recrystallization grains decreases.Moreover,the volume fraction of recrystallization grain has a minimum value,appropriately 45%,and the sample exhibits the highest strength and elongation at the deformation temperature of 400 ℃.
基金Project(2009AA03Z114)supported by the National High-tech Research and Development Program of ChinaProject supported by Tsinghua-Toyo R&D Center of Magnesium and Aluminum Alloys Processing Technology
文摘Standard mechanical test bars with a diameter of 6.4 mm and a gauge length of 50 mm were processed, and the microstructures of die cast AM60B alloy under different die casting process parameters were observed. The influences of the slow shot speed, the fast shot speed and the biscuit thickness on the externally solidified crystals （ESCs） were investigated. With the increase of the biscuit thickness, the number of the ESCs in the cast samples decreases. Under a low slow shot speed, larg ESCs are found in the cast structure and a high fast shot speed results in more spherical ESCs. The relationships between ESCs and process parameters were also discussed.
基金Project(51071004)supported by the National Natural Science Foundation of ChinaProject(2011BAE22B01-3)supported by the National Key Technology R&D Program during the 12th Five-Year Period,China
文摘The microstructure and mechanical properties of the Mg-6Zn-xEr alloys in the as-cast, as-extruded and extruded-T5 states were investigated. It is found that the addition of Er has an obvious effect on improving mechanical properties of Mg-6Zn based alloys. The results suggest that the Mg-6Zn-0.5Er alloy in the peak aged state shows the best tensile strength. The ultimate tensile strength and the yield tensile strength of the peak-aged Mg-6Zn-0.5Er alloy are about 329 MPa and 183 MPa, respectively, companying with a good elongation of 12%. The addition of 0.5% Er into the Mg-6Zn based alloys has a great effect on improving ageing hardening response. The highest tensile strength of the peak-aged Mg-6Zn-0.5Er alloy is mainly due to the refinement of microstructure and the precipitation of β1 phase.
基金Project(2012ZX04012011)supported by the National Science and Technology Major Project of the Ministry of Science and Technology of ChinaProject(2011BAE22B02)supported by the National Key Technologies R&D Program of ChinaProject(51275269)supported by the National Natural Science Foundation of China
文摘The effects of vacuum assistance on the microstructure and mechanical properties of high-pressure die cast AZ91 D alloy at different slow shot speeds were evaluated. Plate-shaped castings of AZ91 D alloy were carried out on a TOYO BD-350V5 cold chamber die casting machine incorporated with a self-improved TOYO vacuum system. It was found that the vacuum pressure in the die cavity at the beginning of mold filling increases with the increase of slow shot speed, following a cubic polynomial curve, resulting in a decline in the porosity-reduction ability of vacuum assistance with the increase of slow shot speed. The externally solidified crystal（ESC） contents in conventional and vacuum die castings behave similar against the slow shot speed. The tensile properties of vacuum die castings were strongly influenced by the ESC content at relative low slow shot speeds. With the increase of slow shot speed, the influence of the gas porosity level in vacuum die castings would get prominent.
