期刊文献+
共找到32篇文章
< 1 2 >
每页显示 20 50 100
聚结晶紫薄膜修饰电极对氧氟沙星的电催化作用 被引量:7
1
作者 周谷珍 蒋银燕 +1 位作者 孙元喜 郑清云 《药物分析杂志》 CAS CSCD 北大核心 2007年第2期201-203,共3页
目的:利用循环伏安法电聚合制备出对氧氟沙星(OFX)具有良好电催化作用的聚结晶紫薄膜修饰电极(PCVE),建立一种对 OFX 进行定量测定的新的电化学分析方法。方法:在0.050 mol·L^(-1)硫酸钠溶液+0.08 mol·L^(-1)。醋酸-醋酸钠缓... 目的:利用循环伏安法电聚合制备出对氧氟沙星(OFX)具有良好电催化作用的聚结晶紫薄膜修饰电极(PCVE),建立一种对 OFX 进行定量测定的新的电化学分析方法。方法:在0.050 mol·L^(-1)硫酸钠溶液+0.08 mol·L^(-1)。醋酸-醋酸钠缓冲液(pH=4.4)体系中,于0.4~1.2 V 范围内,以100 mV·s^(-1)的扫描速率进行循环伏安分析。结果:氧氟沙星的线性范围为1.6×10^(-7)~2.0×10^(-4)mol·L^(-1),r=0.9995,检测限可达8.0×10^(-9)mol·L^(-1)。样品分析的 RSD 均小于2%(n=8),回收率为95.7%~102.1%。结论:PCVE 制备简单、稳定性好。该方法是一种灵敏、准确测定样品中微量 OFX 的新的电化学分析方法。 展开更多
关键词 结晶薄膜修饰电极(PCVE) 氧氟沙星(OFX) 电催化
下载PDF
聚结晶紫薄膜修饰电极测定尿酸 被引量:17
2
作者 周谷珍 孙元喜 《分析测试学报》 CAS CSCD 北大核心 2004年第6期18-21,共4页
利用循环伏安法制备了聚结晶紫薄膜修饰电极(PCVE) ,详细研究了该修饰电极对生物分子尿酸 (UA)的电催化作用。结果表明 ,PCVE对UA具有较强的电催化作用 ,并且对抗坏血酸(AA)具有较强的抗干扰作用 ,允许高达1000倍以上AA存在而不干扰痕... 利用循环伏安法制备了聚结晶紫薄膜修饰电极(PCVE) ,详细研究了该修饰电极对生物分子尿酸 (UA)的电催化作用。结果表明 ,PCVE对UA具有较强的电催化作用 ,并且对抗坏血酸(AA)具有较强的抗干扰作用 ,允许高达1000倍以上AA存在而不干扰痕量UA的测定。将PCVE结合差分脉冲伏安(DPV)技术 ,对UA的检测线性范围为5.0×10 -7~5.0×10 -5mol/L,检出限达7.5×10 -8mol/L。将该法用于尿液中尿酸的测定 。 展开更多
关键词 结晶薄膜修饰电极 尿酸 循环伏安法 电催化 尿液 含量测定
下载PDF
聚结晶紫薄膜修饰电极的制备条件研究 被引量:6
3
作者 周谷珍 孙元喜 邓欢梅 《湖南文理学院学报(自然科学版)》 CAS 2003年第4期25-28,共4页
详细研究了结晶紫 (CV)在玻碳基体电极表面聚合成膜的条件 ,从而得到利用循环伏安法制备聚结晶紫薄膜修饰电极 (PCVE)的最佳条件 :在 0 .0 5mol/LKH2 PO4-Na2 HPO4(pH =6 .8) + 0 .2mol/LNaNO3 + 2 .0× 10 -4mol/LCV的最佳聚合体系... 详细研究了结晶紫 (CV)在玻碳基体电极表面聚合成膜的条件 ,从而得到利用循环伏安法制备聚结晶紫薄膜修饰电极 (PCVE)的最佳条件 :在 0 .0 5mol/LKH2 PO4-Na2 HPO4(pH =6 .8) + 0 .2mol/LNaNO3 + 2 .0× 10 -4mol/LCV的最佳聚合体系中 ,以 5 0mV/s的扫描速率 ,控制扫描电位范围为- 1.2~ 1.8V ,循环扫描 2 0圈即可制得聚结晶紫薄膜修饰电极 .该修饰电极具有良好的重现性和稳定性 ,并对邻苯二酚、多巴胺等具有良好的电催化作用 。 展开更多
关键词 结晶薄膜 修饰电极 制备条件 循环伏安法
下载PDF
采用固相晶化和准分子激光晶化制备结晶硅薄膜的对比
4
作者 王志雄 王欣 +2 位作者 李霞霞 黄飞武 张霞 《机械工程材料》 CAS CSCD 北大核心 2014年第11期46-49,108,共5页
为制备高质量的结晶硅薄膜,以工业玻璃为衬底,利用等离子体增强化学气相沉积工艺制备了非晶硅(α-Si)薄膜,然后分别通过固相晶化和准分子激光晶化两种工艺制备结晶硅(nc-Si)薄膜,采用激光显微拉曼光谱仪、X射线衍射仪和扫描电子显微镜... 为制备高质量的结晶硅薄膜,以工业玻璃为衬底,利用等离子体增强化学气相沉积工艺制备了非晶硅(α-Si)薄膜,然后分别通过固相晶化和准分子激光晶化两种工艺制备结晶硅(nc-Si)薄膜,采用激光显微拉曼光谱仪、X射线衍射仪和扫描电子显微镜等对两类结晶硅薄膜的结晶率、结晶质量和表面形貌等进行了对比分析。结果表明:采用固相晶化得到的结晶硅薄膜的结晶率约为70%,采用准分子激光晶化得到的结晶率则可达90%;当激光拉曼测试条件变化时,两种结晶硅薄膜的结晶率几乎不变,均处于稳定的晶态结构;采用准分子激光晶化制备的结晶硅薄膜显示出微弱的Si(111)结晶峰位,并具有较大的晶粒尺寸和规则的晶界分布。 展开更多
关键词 非晶硅薄膜 结晶薄膜 固相晶化 准分子激光晶化 结晶
下载PDF
非晶硅薄膜和结晶硅薄膜的拉曼光谱 被引量:2
5
作者 马希文 杨玉庆 +2 位作者 张坤 何佳 张霞 《实验室研究与探索》 CAS 北大核心 2016年第8期33-36,共4页
以玻璃为衬底,利用等离子体增强化学气相沉积工艺制备了非晶硅(α-Si)薄膜,然后通过准分子激光晶化方式获得结晶硅(nc-Si)薄膜,采用激光显微拉曼光谱仪对非晶硅薄膜、结晶硅薄膜这两类薄膜的拉曼光谱效应和结晶质量等进行了定量分析。... 以玻璃为衬底,利用等离子体增强化学气相沉积工艺制备了非晶硅(α-Si)薄膜,然后通过准分子激光晶化方式获得结晶硅(nc-Si)薄膜,采用激光显微拉曼光谱仪对非晶硅薄膜、结晶硅薄膜这两类薄膜的拉曼光谱效应和结晶质量等进行了定量分析。结果表明:当激光功率达到某一阈值时,非晶硅样品发生了晶化,即由非晶硅转化成了结晶硅,特征峰发生了46.8 cm-1的位移,薄膜的结晶性质发生根本变化。而结晶硅样品在激光功率变化过程中仅因能量积聚造成了薄膜内应力变化,激光能量消散后内应力恢复原来的状态,特征峰在±5.4 cm^(-1)位移内波动,薄膜的结晶性质并未发生明显变化,表明薄膜处于稳定的晶态结构。 展开更多
关键词 非晶硅薄膜 结晶薄膜 准分子激光晶化 拉曼光谱 拉曼位移
下载PDF
结晶氮化碳薄膜与金刚石争高低
6
《工业金刚石》 2003年第6期36-36,共1页
关键词 结晶氮化碳薄膜 金刚石 物理性能 武汉化工学院 脉冲电弧放电电离
下载PDF
纳米-Al_2O_3颗粒对镍电结晶初期阶段的影响(英文) 被引量:5
7
作者 谭澄宇 崔航 +2 位作者 胡炜 刘宇 郑子樵 《稀有金属材料与工程》 SCIE EI CAS CSCD 北大核心 2010年第1期10-16,共7页
利用循环伏安(CV)、计时安培(CA)和电化学阻抗(EIS)研究了纳米Al2O3颗粒在不同电位(vs.SCE)下对Ni自硫酸盐镀液在铜基体上电沉积的影响。结果表明,Ni-Al2O3体系共沉积的起始电位为:–740mV左右;在不同的电位下,纳米-Al2O3颗粒对镍沉积... 利用循环伏安(CV)、计时安培(CA)和电化学阻抗(EIS)研究了纳米Al2O3颗粒在不同电位(vs.SCE)下对Ni自硫酸盐镀液在铜基体上电沉积的影响。结果表明,Ni-Al2O3体系共沉积的起始电位为:–740mV左右;在不同的电位下,纳米-Al2O3颗粒对镍沉积过程的影响有所差别;在电位–740~–830mV范围,与纯Ni沉积相比较,Ni-Al2O3体系沉积的峰电流所对应的孕育期tm明显缩短,反映Al2O3颗粒在阴极表面有利于镍沉积成核,且促进了电结晶成核。Al2O3颗粒吸附在阴极表面可能会阻碍部分离子电荷放电和物质传输过程,尤其在电位–250~–650mV范围,致使Ni-Al2O3体系沉积阻抗增加。在较高的过电位下,Al2O3颗粒的促进作用有所减弱,许多颗粒堆积在电极表面上还可能减小Ni-Al2O3沉积的还原反应电流。在电位–890mV,Ni-Al2O3体系电沉积初期阶段的成核过程基本遵循三维的Scharifker-Hill瞬时成核模式。 展开更多
关键词 Ni-Al2O3 薄膜:电结晶成核 共沉积 1-t曲线
下载PDF
高能脉冲磁控溅射低温制备晶态薄膜的研究进展
8
作者 白雪冰 蔡群 张旭海 《中国表面工程》 EI CAS CSCD 北大核心 2022年第5期105-115,共11页
高能脉冲磁控溅射技术(HiPIMS)是一种新型的磁控溅射技术,以峰值功率密度高,金属离化率高为特点,与传统直流磁控溅射(DCMS)相比,表现出其独有的优势。晶态薄膜的制备以往通常采用高温沉积或者后续的热处理技术,不仅工艺复杂,而且容易造... 高能脉冲磁控溅射技术(HiPIMS)是一种新型的磁控溅射技术,以峰值功率密度高,金属离化率高为特点,与传统直流磁控溅射(DCMS)相比,表现出其独有的优势。晶态薄膜的制备以往通常采用高温沉积或者后续的热处理技术,不仅工艺复杂,而且容易造成能源损失。高度离化的脉冲等离子体使HiPIMS技术成功应用于晶态薄膜的沉积,极大地降低制备温度,简化制备工艺,扩展了基底材料的选择范围,提升了薄膜的应用空间。然而,针对HiPIMS低温制备晶态薄膜的系统研究较为缺乏,因此亟需对现有的研究结果进行整理、归纳、总结,对其进一步研究提供理论参考。基于晶态薄膜的低温制备,在详细介绍以Al_(2)O_(3)、VO_(2)、TiO_(2)为代表的晶态薄膜的HiPIMS低温沉积工艺及其结构性能的基础上,探讨薄膜低温结晶的机理,展望HiPIMS未来的研究方向和应用前景。 展开更多
关键词 HIPIMS 结晶薄膜 沉积温度 Al_(2)O_(3) VO_(2) TiO_(2)
下载PDF
氦等离子体前处理对多晶硅薄膜性能的影响
9
作者 汝丽丽 孟月东 陈龙威 《深圳大学学报(理工版)》 EI CAS 北大核心 2013年第4期398-403,共6页
采用微波电子回旋共振等离子体增强磁控溅射(microwave electron cyclotron resonance plasma-enhanced magnetron sputtering,ECR-PEMS)和电子回旋共振等离子体辅助化学气相沉积(microwave electroncyclotron resonance chemical vapor... 采用微波电子回旋共振等离子体增强磁控溅射(microwave electron cyclotron resonance plasma-enhanced magnetron sputtering,ECR-PEMS)和电子回旋共振等离子体辅助化学气相沉积(microwave electroncyclotron resonance chemical vapor deposition,ECR-CVD)技术,分别在单晶硅片(100)基底上低温制备了多晶硅薄膜.采用拉曼光谱仪、X射线衍射仪以及原子力显微镜对薄膜微观结构及表面形貌进行表征,研究纯氦等离子体基底前期处理对所沉积薄膜性能的影响.结果表明,氦等离子体前处理技术能大幅提高多晶硅薄膜结晶度和颗粒尺寸,明显改善ECR-CVD法所得多晶硅薄膜的微观结构特性和表面形貌. 展开更多
关键词 等离子体物理 多晶硅薄膜 电子回旋共振 等离子体增强 氦等离子体 磁控溅射 化学气相沉积 薄膜结晶 纳米材料
下载PDF
玻璃表面的结晶装饰
10
《上海硅酸盐》 1989年第3期129-134,共6页
关键词 玻璃 表面 结晶 装饰 结晶薄膜
下载PDF
两种白钨矿碱分解溶液的蒸发与结晶过程研究 被引量:2
11
作者 徐志昌 张萍 《中国钼业》 2016年第2期32-39,共8页
本文采用旋转薄膜、玻璃真空蒸发器,对两种组成不同的白钨矿的苛性钠浸出溶液,选择了两种蒸发温度(90℃和80℃)下的蒸发-结晶试验。蒸发-结晶过程是按照流程设计的要求,所进行的承上启下的中间过程。目的是取得含有与不含有钼酸钠的... 本文采用旋转薄膜、玻璃真空蒸发器,对两种组成不同的白钨矿的苛性钠浸出溶液,选择了两种蒸发温度(90℃和80℃)下的蒸发-结晶试验。蒸发-结晶过程是按照流程设计的要求,所进行的承上启下的中间过程。目的是取得含有与不含有钼酸钠的钨酸钠结晶,以方便萃取分离钨/钼过程使用,并节省调整酸度过程的耗酸量;同时,取得高浓度氢氧化钠溶液,以便循环使用苛性钠试剂,并节省浸出试剂的消耗量。试验结果表明,对于含钼的钨酸钠-苛性碱浸出溶液而言,蒸发-结晶温度为90℃时(-0.098 MPa,56 r/min),尽管,氢氧化钠的回收率达到了尽善尽美,ηNa OH=100%,但是,美中不足的结晶率分别是:ηW=84.39%和ηM o=69.60%。即钨酸钠和钼酸钠的循环率分别为:ρw=16.17%和ρMo=31.29%。对于不含钼的钨酸钠-苛性碱溶液而言,蒸发-结晶温度为80℃,(-0.098 MPa,56 r/min),尽管,氢氧化钠的回收率接近完美,ηNa OH=100.0%,但是,美中不足是钨酸钠的循环率达到了,ηW=17.00%。两种结果表明,蒸发-结晶温度范围为80~90℃下,氢氧化钠的回收率,尽如人意,美中不足的是钨酸钠的循环率达到了16.1%~17.0%,钼酸钠的循环率达到31.29%。钨酸钠和钼酸钠之间的分离系数范围是1.21~1.56。 展开更多
关键词 旋转薄膜蒸发-结晶过程 含钼的与不含钼的白钨矿浸出溶液 钨酸钠和钼酸钠的结晶 氢氧化钠回收率 钨酸钠和钼酸钠的循环率 分离系数
下载PDF
Fabrication of Bottom-Gate and Top-Gate Transparent ZnO Thin Film Transistors 被引量:1
12
作者 张新安 张景文 +4 位作者 张伟风 王东 毕臻 边旭明 侯洵 《Journal of Semiconductors》 EI CAS CSCD 北大核心 2008年第5期859-862,共4页
Transparent zinc oxide thin film transistors (ZnO-TFTs) with bottom-gate and top-gate structures were constructed on 50mm silica glass substrates. The ZnO films were deposited by RF magnetron sputtering and SiO2 fil... Transparent zinc oxide thin film transistors (ZnO-TFTs) with bottom-gate and top-gate structures were constructed on 50mm silica glass substrates. The ZnO films were deposited by RF magnetron sputtering and SiO2 films served as the gate insulator layer. We found that the ZnO-TFTs with bottom-gate structure have better electrical performance than those with top-gate structure. The bottom-gate ZnO-TFTs operate as an n-channel enhancement mode, which have clear pinch off and saturation characteristics. The field effect mobility, threshold voltage, and the current on/off ratio were determined to be 18.4cm^2/(V ·s), - 0. 5V and 10^4 , respectively. Meanwhile, the top-gate ZnO-TFTs exhibit n-chan- nel depletion mode operation and no saturation characteristics were detected. The electrical difference of the devices may be due to the different character of the interface between the channel and insulator layers. The two transistors types have high transparency in the visible light region. 展开更多
关键词 zinc oxide thin film transistor structure interface
下载PDF
Poly-Si Thin Film Grown by Excimer Laser Crystallization and Its Ellipsometric Analysis
13
作者 ZENGXiang-bin XUZhong-yang 《Semiconductor Photonics and Technology》 CAS 2000年第2期96-99,104,共5页
A novel approach of two-step laser crystallization for the growth of poly-Si thin film on glass substrate is investigated. Using this approach, we fabricated poly-Si thin film transistors with electron mobility of 103... A novel approach of two-step laser crystallization for the growth of poly-Si thin film on glass substrate is investigated. Using this approach, we fabricated poly-Si thin film transistors with electron mobility of 103 cm2/V·s and on/off current ratio of 1×10~7.They are better than those of the poly-Si TFTs fabricated by conventional single-step excimer laser crystallization. We also analyzed the structure of the laser crystallized poly-Si thin film by spectroscopic ellipsometry, and proposed the models to simulate the poly-Si thin film and calculated the ellipsometric spectra. The calculated results are in good agreement with the measured results. 展开更多
关键词 POLY-SI Thin film Laser crystallization Thin film transistors
下载PDF
Comparison of Poly-Si Thin Films Prepared by Conventional Furnace Annealing and Pulsed Rapid Thermal Annealing
14
作者 JIN Rui-min ZHENG Xiao-yan +3 位作者 CHEN Lan-li LUO Peng-hui GUO Xin-feng LU Jing-xiao 《Semiconductor Photonics and Technology》 CAS 2009年第2期117-119,共3页
Amorphous silicon films prepared by PECVD on glass substrate were crystallized by conventional furnace annealing(FA) and rapid thermal annealing(RTA),respectively. From the Raman spectra and scanning electronic micros... Amorphous silicon films prepared by PECVD on glass substrate were crystallized by conventional furnace annealing(FA) and rapid thermal annealing(RTA),respectively. From the Raman spectra and scanning electronic microscope(SEM),it found that the thin films made by RTA had smooth and perfect structure,while the thin films annealed by FA had a higher degree of structural disorder. 展开更多
关键词 PECVD conventional furnace annealing pulsed rapid thermal annealing
下载PDF
Nc-Si Thin Film Deposited at Low Temperature and Nc-Si Heterojunction Solar Cell
15
作者 赵占霞 崔容强 +2 位作者 孟凡英 于化丛 周之斌 《Journal of Shanghai Jiaotong university(Science)》 EI 2004年第4期81-84,共4页
This paper reported some results about intrinsic nanocrystalline silicon thin films deposited by high frequency (HF) sputtering on p-type c-Si substrates at low temperature. Samples were examined by atomic force micro... This paper reported some results about intrinsic nanocrystalline silicon thin films deposited by high frequency (HF) sputtering on p-type c-Si substrates at low temperature. Samples were examined by atomic force microscopy (AFM), X-ray diffraction (XRD), infrared absorption, and ellipsometry. XRD measurements show that this film has a new microstructure, which is different from the films deposited by other methods. The ellipsometry result gives that the optical band gap of the film is about 2.63 eV. In addition, the n-type nc-Si∶H/p-type c-Si heterojunction solar cell, which has open circuit voltage (U oc ) of 558 mV and short circuit current intensity (I sc ) of 29 mA/cm2, was obtained based on the nanocrystalline silicon thin film. Irradiated under AM1.5, 100 mW/cm2 light intensity, the U oc , I sc , and FF can keep stable for 10 h. 展开更多
关键词 HF sputtering low temperature nanocrystalline silicon heterojunction solar cell
下载PDF
Topological Structure of Knotted Vortex Lines in Liquid Crystals
16
作者 DUAN Yi-Shi ZHAO Li ZHANG Xin-Hui 《Communications in Theoretical Physics》 SCIE CAS CSCD 2007年第6期1129-1134,共6页
In this paper, a novel decomposition expression for the U(1) gauge field in liquid crystals (LCs) is derived. Using this decomposition expression and the b-mapping topological current theory, we investigate the to... In this paper, a novel decomposition expression for the U(1) gauge field in liquid crystals (LCs) is derived. Using this decomposition expression and the b-mapping topological current theory, we investigate the topological structure of the vortex lines in LCs in detail. A topological invariant, i.e., the Chern-Simons (CS) action for the knotted vortex lines is presented, and the CS action is shown to be the total sum of all the self-linking and linking numbers of the knot family. Moreover, it is pointed out that the CS action is preserved in the branch processes of the knotted vortex lines. 展开更多
关键词 knotted vortex lines liquid crystals Chern-Simons action branch processes
下载PDF
An analytical model to explore open-circuit voltage of a-Si:H/c-Si heterojunction solar cells 被引量:1
17
作者 钟春良 耿魁伟 +1 位作者 罗兰娥 杨迪武 《Journal of Central South University》 SCIE EI CAS CSCD 2016年第3期598-603,共6页
The effect of the parameters on the open-circuit voltage, V_(OC) of a-Si:H/c-Si heterojunction solar cells was explored by an analytical model. The analytical results show that V_(OC) increases linearly with the logar... The effect of the parameters on the open-circuit voltage, V_(OC) of a-Si:H/c-Si heterojunction solar cells was explored by an analytical model. The analytical results show that V_(OC) increases linearly with the logarithm of illumination intensity under usual illumination. There are two critical values of the interface state density(D_(it)) for the open-circuit voltage(V_(OC)), D_(it)^(crit,1) and D_(it)crit,2(a few 1010 cm^(-2)·e V^(-1)). V_(OC) decreases remarkably when D_(it) is higher than D_(it)^(crit,1). To achieve high V_(OC), the interface states should reduce down to a few 1010 cm^(-2)·e V^(-1). Due to the difference between the effective density of states in the conduction and valence band edges of c-Si, the open-circuit voltage of a-Si:H/c-Si heterojunction cells fabricated on n-type c-Si wafers is about 22 mV higher than that fabricated on p-type c-Si wafers at the same case. V_(OC) decreases with decreasing the a-Si:H doping concentration at low doping level since the electric field over the c-Si depletion region is reduced at low doping level. Therefore, the a-Si:H layer should be doped higher than a critical value of 5×10^(18) cm^(-3) to achieve high V_(OC). 展开更多
关键词 solar cells a-Si:H/c-Si heterojunctions open-circuit voltage
下载PDF
Theoretical Calculation on Optimum Si-doping Content in Boron Carbide Thin Film
18
作者 FAN Zhi-xin (Dept. of Appl. Phys., Hebei University of Technology, Tianjin 300130, CHN) 《Semiconductor Photonics and Technology》 CAS 2002年第2期92-95,共4页
The theoretical expression of the relationship between optimumdoping content and crystal structure is presented as well as thepreparation methods. By using this expression, the optimum dopingcontent of silicon-coped b... The theoretical expression of the relationship between optimumdoping content and crystal structure is presented as well as thepreparation methods. By using this expression, the optimum dopingcontent of silicon-coped boron carbide thin film is calculated. Thequantitative calculation value is consistent with the experimentalresults. This theoretical expression is also appropriate to resolvethe optimum doping content for Other electric materials. 展开更多
关键词 Thermoelectric material boron carbide thin film crystal structure optimum doping
下载PDF
Influence of substrate temperature on the deposition and structural properties of μc-Si:H thin films fabricated with VHF-PECVD
19
作者 YANG Hui-dongt 《Optoelectronics Letters》 EI 2005年第1期21-23,共3页
With in situ optical emission spectroscopy (OES) diagnosis on VHF-generated H2 + SiH4 plasmas,and with the measurements of deposition rate and structure of μc-Si. H thin films fabricated with VHFPECVD technique at... With in situ optical emission spectroscopy (OES) diagnosis on VHF-generated H2 + SiH4 plasmas,and with the measurements of deposition rate and structure of μc-Si. H thin films fabricated with VHFPECVD technique at different substracte temperature, influence of substrate temperature on the deposition of μc-Si.H thin film and on its structural properties have been investigated. The results show that with the increase of substrate temperature,the crystalline volume fraction Xc and average grain size d are enhanced monotonously, but the deposition rate increases firstly and then decreases. The optimized substrate temperature for μc-Si:H thin films deposition under our current growth system is about 210 ℃ ,at which deposition rate O. 8 nm/s of pc-Si;H thin film with Xc-60% and d-9 nm can be obtained. 展开更多
关键词 μc-Si: H薄膜 晶体结构 沉积作用 温度条件 生长系统
下载PDF
Formation of nanocrystalline microstructure in arc ion plated CrN films 被引量:4
20
作者 Qi-min WANG Se-Hun KWON Kwang-Ho KIM 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2011年第A01期73-77,共5页
Applying negative bias voltages caused significant microstructure changes in arc ion plated CrN films. Nanocrystalline microstructures were obtained by adjusting the negative bias voltage. Structural characterizations... Applying negative bias voltages caused significant microstructure changes in arc ion plated CrN films. Nanocrystalline microstructures were obtained by adjusting the negative bias voltage. Structural characterizations of the films were carried out using X-ray diffractometry (XRD) and high-resolution transmission electron microscopy (HR-TEM). The results indicated that increasing ion bombardment by applying negative bias voltages resulted in the formation of defects in the CrN films, inducing microstructure evolution from micro-columnar to nanocrystalline. The microhardness and residual stresses of the films were also affected. Based on the experimental results, the evolution mechanisms of the film microstructure and properties were discussed by considering ion bombardment effects. 展开更多
关键词 CRN thin films DEPOSITION microstructure arc ion plating ion bombardment
下载PDF
上一页 1 2 下一页 到第
使用帮助 返回顶部