基于激光微技术的光谱检测“集成缩微”的研究

为了满足μ-TAS领域对光谱微检测提出的'功能集成与结构缩微'的技术要求,利用激光微技术获得了光谱微检测技术的核心部件,即百微米级微光波导管,并对光谱微检测在μ-TAS生化芯片中的应用方案进行了研究.结果表明,利用激光微加工技术将微检测系统集成到微型全分析系统生化芯片中具有非常广阔的应用前景.

μ-TAS领域光谱检测“集成缩微”现状及激光微技术的研究

光谱微检测技术是微全分析系统（μ-TAS）生化芯片的常用核心技术之一。对国内外相关文献进行分析表明，“功能集成与结构缩微”技术是当前μ-TAS领域对光谱微检测提出的迫切要求。对“集成与缩微”方面研究现状进行了综述，并对与此有关的激光微技术研究作了展望。

现代农业设施缩微教学模型的研究与开发

建设社会主义新农村,大力培育新型农民,是十一五规划的重要内容.现代农业设施缩微模型教具的研究与开发就是要研究一种具有普遍性和区域代表性的现代农业设施的仿真缩微教学模型,该模型的外形与实物相同,按一定比例缩小,可用于课堂教学,所有的操作部件和自动控制方式完全仿真。

Insight into fouling behavior of poly(vinylidene fluoride)(PVDF)hollow fiber membranes caused by dextran with different pore size distributions

Membrane fouling is the key problem that occurs in membrane process for water treatment. However, how membrane microstructure influences the fouling behavior is still not clear. In this study, fouling behavior caused by dextran was deeply and systematically investigated by employing four poly（vinylidene fluoride） （PVDF） membranes with different pore sizes, ranging from 24 to 94 nm. The extent of fouling by dextran was accurately characterized by pore reduction, flux decline, and the change of critical flux. The result shows that membrane with the smallest pore size of 24 nm experienced the smallest fouling rate and the lowest fouling extent. As the membrane pore size increased, the critical flux ranges were 105-114, 63-73, 38-44 and 34- 43 L. m 2. h t, respectively. The critical flux and fouling resistances indicated that the fouling propensity in- creases with the increase of membrane pore size. Two pilot membrane modules with mean pore size of 25 nm and 60 nm were applied in membrane filtration of surface water treatment. The results showed that serious ir- reversible membrane fouling occurred on the membrane with pore size of 60 nm at the permeate flux of 40.5 L.m 2.h 1. On the other hand, membrane with pore size of 25 nm exhibited much better anti-fouling per- formance when permeate flux was set to 40.5, 48 and 60 L-m 2-h- 1.

Laboratory study on geotechnical characteristics of marine coral clay

The hydraulic reclamation coral clay is a new type of clay,formed during the sorting process of coral island reef reclamation.The foundation of the hydraulic reclamation coral reef consists of coral sand,silt,and clay.The part of the particles with particle size less than 0.075 mm contain more than 50%forms clay.As a new type of clay,the geotechnical properties were rarely reported in previous studies.In this paper,the physical and mechanical properties,microstructure and mineral composition were comprehensively researched by a series of laboratory tests.The results show that coral clay is a low liquid limit clay with high pore ratio and high saturation.From the aspect of mineral compositions,the coral clay studied consists of calcite and aragonite,while the chemical composition of it is calcium carbonate.The void ratio has a significant effect on the compressive properties of coral clay.With the increase of the void ratio,the compression coefficient a_(1-2) and compression index C_(c) gradually increase,and the compression modulus Es gradually decreases.The undrained stress−strain curve of coral clay shows a strain-softening behavior,and the peak strength and residual strength are positively linear correlated with confining pressure.

Microstructure and texture characteristics of ZK60 Mg alloy processed by cyclic extrusion and compression

The microstructure and crystallographic texture characteristics of an extruded ZK60 Mg alloy subjected to cyclic extrusion and compression(CEC) up to 8 passes at 503 K were investigated.The local crystallographic texture,grain size and distribution,and grain boundary character distributions were analyzed using high-resolution electron backscatter diffraction(EBSD).The results indicate that the microstructure is refined significantly by the CEC processing and the distributions of grain size tend to be more uniform with increasing CEC pass number.The fraction of low angle grain boundaries(LAGBs) decreases after CEC deformation,and a high fraction of high angle grain boundaries(HAGBs) is revealed after 8 passes of CEC.Moreover,the initial fiber texture becomes random during CEC processing and develops a new texture.

Microstructures and compressive properties of AZ91D/fly-ash cenospheres composites

Novel AZ91D Mg alloy/fly-ash cenospheres(AZ91D/FACs)composites were fabricated by melt stir technique.Fly-ash cenosphere particles with 4%,6%,8%,10%in mass fraction and 100μm in size were used.Hardness and compressive strength of the composites were measured.The effects of mass fraction of cenospheres on the microstructure and compressive properties were characterized.The results show that the cenospheres are uniformly distributed in the matrix and there is no sign of cenosphere cluster or residual pore.The densities of the composites are 1.85-1.92 g/cm 3 .By comparing with matrix,the compressive yield strength of the composites is improved,and the cenospheres is filled with Mg matrix alloy.SEM,XRD and EDX results of the composites show clear evidence of reaction product at cenosphere/matrix interface.On the basis of XRD and EDX,composition, structure and thermodynamic analysis,the main interfacial phase between the cenosphere and AZ91D Mg alloy was identified to be MgAl2O4.

Phase structure of ZK60-1Er magnesium alloy compressed at 450℃

The phase structure of ZK60-1Er magnesium alloy thermally compressed at the temperature of 450℃ and the strain rate of 1×10 -4 s -1 was determined by transmission electron microscopy(TEM)and high-resolution electron microscopy(HREM).The results show that this magnesium alloy contains many new W phases(Mg3Zn3Er2,FCC structure)in the matrix.Those new W phases have two morphologies,either irregularly rectangular or rod morphology·Lattice constants of the two new W phases are slightly higher than those of W Phase(Mg3Zn3Y2)containing rare earth element of yttrium.

Effects of strain rate and temperature on microstructure and texture for AZ31 during uniaxial compression

In order to investigate the effects of strain rate and temperature on the microstructure and texture evolution during warm deformation of wrought Mg alloy,AZ31 extruded rods were cut into cylinder samples with the dimension of d8 mm×12 mm.The samples were compressed using a Gleeble 1500D thermo-mechanical simulation machine at various strain rates(0.001,0.01,0.1,1 and 5 s- 1)and various temperatures(300,350,400 and 450℃).The microstructure and texture of the compressed samples at the same strain under different deformation conditions were studied and compared by electron backscatter diffraction(EBSD)in scanning electron microscope(SEM).The results show that the size of recrystallized grains in the deformed samples generally increases with the decrease of strain rate and the increase of temperature.After 50%reduction,most basal planes are aligned perpendicular to the compression direction at relatively high strain rate(>0.01 s- 1)or low temperature(<350℃).The optimized strain rate is 0.1 s- 1for uniaxial compression at 300℃,which produces about 80%of small grains(<5μm).