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大豆蛋白自凝固的实验研究
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作者 钱俊青 方型长 《西部粮油科技》 2000年第2期30-32,共3页
以大豆蛋白水提液为研究对象,试验了其自凝固的影响因素 ,由正交试验得出其最佳自凝条件。初步探讨了自凝固机理。
关键词 自凝固 大豆蛋白 提取液 实验
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多孔自凝固磷酸钙/纤维蛋白1:1比例血管化的分析研究
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作者 修金涛 崔赓 +5 位作者 卜涛 毕龙 董静静 吴剑维 李阳 雷伟 《现代生物医学进展》 CAS 2013年第16期3024-3028,共5页
目的:观察复合纤维蛋白的多孔自凝固磷酸钙的理学性能及体内血管化情况,探讨其各组份对材料生物学特性的影响,为其临床应用提供实验数据。方法:1)采用凝固时间测定和电镜观察材料表面和断面等方法对复合支架材料构造和理学性能进行分析... 目的:观察复合纤维蛋白的多孔自凝固磷酸钙的理学性能及体内血管化情况,探讨其各组份对材料生物学特性的影响,为其临床应用提供实验数据。方法:1)采用凝固时间测定和电镜观察材料表面和断面等方法对复合支架材料构造和理学性能进行分析;2)将24只新西兰白兔随机分为3组,每组8只,分别在每只实验兔腰背筋膜下植入1:1、CPC两种比例材料各一枚。术后2、4、8周进行取材,对材料及其周围组织进行组织学观察、微血管情况定量分析。结果:1)CPC/FG复合支架材料以1:1(g/ml)混合后,与单纯的CPC相比,初凝时间延长,而终凝时间没有明显的统计学差异;电镜观察发现多孔自凝固磷酸钙复合了纤维蛋白胶之后,纤维蛋白胶分布均匀贯穿多孔自凝固磷酸钙晶体之间,并将其紧密相连;2)术后2周材料外周可见幼稚的微血管。1:1组高于CPC组(P<0.05)。4周微血管密度达到高峰,相对于2周时有明显差异。1:1组高于CPC组(P<0.05)。8周时微血管密度相对4周没有显著差异。各组微血管密度与4周时没有明显变化(P>0.05)。结论:复合支架材料具有合适的凝固时间和较好的结构,纤维蛋白胶及其降解产物影响复合材料在体内的微血管密度,使复合材料血管化能力提高,其可作为细胞载体和骨缺损修复支架材料应用于临床和实验中。 展开更多
关键词 多孔自凝固磷酸钙 纤维蛋白胶 微血管密度 量化分析 凝固时间
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Effects of melt treatment temperature and isothermal holding parameter on water-quenched microstructures of A356 aluminum alloy semisolid slurry 被引量:7
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作者 Ming LI Yuan-dong LI +3 位作者 Guang-li BI Xiao-feng HUANG Ti-jun CHEN Ying MA 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2018年第3期393-403,共11页
The semisolid slurry of the A356 aluminum alloy was prepared by self-inoculation method(SIM),the effects of melt treatment temperatures and isothermal holding parameters on water-quenched microstructures of A356 alumi... The semisolid slurry of the A356 aluminum alloy was prepared by self-inoculation method(SIM),the effects of melt treatment temperatures and isothermal holding parameters on water-quenched microstructures of A356 aluminum alloy semisolid slurry were investigated,and the solidification behavior of the remaining liquid phase(secondary solidification)was analyzed.The results indicate that the melt treatment temperature has significant effects on the final semisolid microstructures.The semisolid slurry which is suitable for the rheological forming can be produced when the melt treatment temperature is between 680 and 690°C.During the isothermal holding process,the growth rate of the primary particles conforms to the dynamic equation of Dt 3-Do3=Kt,and the coarsening rate of the primary particles is the fastest when the isothermal holding temperature is 600°C.Additionally,the isothermal holding time also has obvious effect on the secondary solidification microstructures.The secondary particles are the smallest and roundest when the isothermal holding time is 3 min.The amount of the secondary particles gradually increases with the increase of isothermal holding temperature,and the eutectic reaction therefore is confined into small intergranular areas,contributing to the compactness of the final solidified eutectic structures. 展开更多
关键词 aluminum alloy SEMISOLID self-inoculation method secondary solidification primary particles eutectic structure
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Simulation on microstructure evolution of Al-Si alloy under effect of natural convection during solidification 被引量:5
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作者 Zhen-hong WANG Li-tong ZHANG +1 位作者 Bin SU Xiao-peng ZHANG 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2022年第1期79-90,共12页
The solidification microstructure of Al-Si alloy was observed in the experiment,the second dendrite arm spacing(SDAS)was measured,and the effect of temperature on the microstructure was analyzed.Phase-field(PF)model i... The solidification microstructure of Al-Si alloy was observed in the experiment,the second dendrite arm spacing(SDAS)was measured,and the effect of temperature on the microstructure was analyzed.Phase-field(PF)model incorporating natural convection caused by gravity was employed to simulate the microstructure evolution of Al-Si alloy under the experimental conditions.Good agreements between the experimental and simulation results verified the reliability of the simulation approach proposed in this study.Based on the proposed model,a series of simulation cases(2D and 3D)were performed to investigate the evolution of columnar and equiaxed dendritic structures.It was found that the solute content of the alloy had little impact on the microstructure evolution,while the solute expansion coefficient had obvious effect on the dendrite tip velocities.Significant improvement of computational efficiency was achieved via novel algorithms,making it possible to perform massive simulation for studying the evolution of solidification microstructures,which is hard to be directly observed in experiments via synchrotron radiation for Al-Si alloy. 展开更多
关键词 Al-Si alloy solidification microstructure natural convection phase-field simulation
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Numerical simulation of solidification morphologies of Cu-0.6Cr casting alloy using modified cellular automaton model 被引量:9
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作者 TSAI De-chang HWANG Weng-sing 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2010年第6期1072-1077,共6页
The purpose of this study is to predict the morphologies in the solidification process for Cu-0.6Cr(mass fraction,%)alloy by vacuum continuous casting(VCC)and verify its accuracy by the observed experimental results.I... The purpose of this study is to predict the morphologies in the solidification process for Cu-0.6Cr(mass fraction,%)alloy by vacuum continuous casting(VCC)and verify its accuracy by the observed experimental results.In numerical simulation aspect, finite difference(FD)method and modified cellular automaton(MCA)model were used to simulate the macro-temperature field, micro-concentration field,nucleation and grain growth of Cu-0.6Cr alloy using real data from actual casting operations.From the observed casting experiment,the preliminary grain morphologies are the directional columnar grains by the VCC process.The solidification morphologies by MCAFD model are in agreement with the result of actual casting experiment well. 展开更多
关键词 Cu-Cr alloy vacuum continuous casting solidification morphology simulation modified cellular automaton model finite difference method
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Two-dimensional numerical simulation of thermocapillary convection in detached solidification 被引量:3
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作者 PENG Lan FAN JuYan +1 位作者 LI YouRong MENG HaiYong 《Science China(Technological Sciences)》 SCIE EI CAS 2012年第2期527-536,共10页
Numerical simulations of flow in the melt(CdZnTe) with different conditions are conducted using the finite-difference method.When the top surface of the melt is solid wall under microgravity condition,the thermocapill... Numerical simulations of flow in the melt(CdZnTe) with different conditions are conducted using the finite-difference method.When the top surface of the melt is solid wall under microgravity condition,the thermocapillary convection is caused in the melt by the surface tension gradient on the free surface.As the Marangoni number is small,the flow is steady thermocapillary convection.As the Marangoni number exceeds the critical value,the steady flow transits into unstable thermocapillary convection.When the top surface of the melt is free surface under microgravity,two roll cells are observed in the melt,which are driven by both the surface tension gradients on the upper and lower free surfaces.When the top surface of the melt is free surface under gravity condition,the effect of the buoyancy on the flow is little as the Marangoni number is small.With the Marangoni number increasing,the effect of the buoyancy increases,which makes the upper roll cell weaken and the lower roll cell strengthen. 展开更多
关键词 detached solidification thermocapillary convection BUOYANCY CDZNTE numerical simulation
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