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碳化硅致密陶瓷材料研究进展 被引量:30
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作者 戴培赟 周平 +2 位作者 王泌宝 李晓丽 杨建锋 《中国陶瓷》 CAS CSCD 北大核心 2012年第4期1-6,26,共7页
碳化硅材料以其优异的性能得到了越来越广泛的应用,通过简要介绍碳化硅致密陶瓷的制备方法及其性能和总结近年来国内外的研究进展,来展望碳化硅致密陶瓷材料的研究发展趋势。
关键词 碳化硅陶瓷 致密材料 陶瓷烧结
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致密陶瓷材料密度和气孔率的测试方法 被引量:10
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作者 田仕 王为民 +1 位作者 张帆 何金云 《理化检验(物理分册)》 CAS 2011年第8期476-479,共4页
对比研究了传统煮沸法和卡尺法测试致密陶瓷材料密度和气孔率的差别,结果发现卡尺法可以弥补传统煮沸法的一些缺点,减少人为操作和试验环境因素对测试数据的影响,提高了测试结果的稳定性。同时,通过扩展阿基米德原理公式,表明致密陶瓷... 对比研究了传统煮沸法和卡尺法测试致密陶瓷材料密度和气孔率的差别,结果发现卡尺法可以弥补传统煮沸法的一些缺点,减少人为操作和试验环境因素对测试数据的影响,提高了测试结果的稳定性。同时,通过扩展阿基米德原理公式,表明致密陶瓷材料的开口气孔率、闭口气孔率和真气孔率的测试值与其自身的体积密度、表观密度和真密度相关。 展开更多
关键词 致密陶瓷材料 密度 气孔率 煮沸法 卡尺法
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引入纳米Cr_2O_3前驱体对致密氧化铬材料烧结的影响 被引量:2
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作者 徐延庆 吕世坪 +3 位作者 范志辉 王金相 洪彦若 陈肇友 《耐火材料》 CAS 北大核心 2010年第1期30-33,共4页
在氧化铬材料中分别引入0.3%、0.6%、0.9%和1.2%(按Cr2O3的质量分数计)的纳米Cr2O3前驱体——氢氧化铬溶胶,通过喷雾造粒、等静压成型,将制备的致密氧化铬试样在氮气气氛中分别于1350、1400、1450℃下烧成后,测定烧后试样的显气孔率和... 在氧化铬材料中分别引入0.3%、0.6%、0.9%和1.2%(按Cr2O3的质量分数计)的纳米Cr2O3前驱体——氢氧化铬溶胶,通过喷雾造粒、等静压成型,将制备的致密氧化铬试样在氮气气氛中分别于1350、1400、1450℃下烧成后,测定烧后试样的显气孔率和常温抗折强度,并采用SEM分析烧成后试样的显微结构。结果表明:加入氢氧化铬溶胶促进了致密氧化铬材料的烧结,其加入量为w(Cr2O3)=0.3%时,材料中的气孔明显减少,常温抗折强度显著提高;加入适量氢氧化铬溶胶促进了材料的烧结致密化,使试样结构更加致密,气孔呈微细化均匀分布。 展开更多
关键词 氢氧化铬溶胶 纳米氧化铬 致密氧化铬材料 烧结 致密 微气孔
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凝胶注模成型制备致密氧化铬耐火材料 被引量:2
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作者 邸利芝 丁春辉 +1 位作者 卢丽霞 杨德安 《耐火材料》 北大核心 2017年第6期414-417,共4页
为了解决等静压法制备致密氧化铬耐火材料过程中产生大量废弃粉尘的问题,以N,N-二甲基丙烯酰胺(DMAA)为单体,以N,N-亚甲基双丙烯酰胺(MBAM)为交联剂,以AN-2000为分散剂,以2,2’-偶氮[2-(2-咪唑啉-2-基)丙烷]盐酸盐(AZIP·2HCl)为引... 为了解决等静压法制备致密氧化铬耐火材料过程中产生大量废弃粉尘的问题,以N,N-二甲基丙烯酰胺(DMAA)为单体,以N,N-亚甲基双丙烯酰胺(MBAM)为交联剂,以AN-2000为分散剂,以2,2’-偶氮[2-(2-咪唑啉-2-基)丙烷]盐酸盐(AZIP·2HCl)为引发剂,采用凝胶注模工艺制备了致密氧化铬耐火材料。研究了浆料p H(分别为4、5、6、7、8、9、10)、分散剂AN-2000用量(质量分数分别为0.1%、0.2%、0.3%、0.4%、0.5%)、固相含量(固相体积分数分别为50%、51%、52%、53%)对浆料黏度以及生坯和1 500℃保温2 h烧后试样性能和显微结构的影响。结果表明:浆料中分散剂AN-2000的最佳用量为0.4%(w),最佳p H为8,最佳固相含量为52%(φ)。以最佳条件制备的生坯的相对密度和抗折强度分别为66.7%和4.8 MPa,烧后试样的相对密度、显气孔率和抗折强度分别为85.1%、14.7%和66.7 MPa,生坯和烧后试样的显微结构均匀。 展开更多
关键词 致密氧化铬耐火材料 凝胶注模 N N-亚甲基双丙烯酰胺
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致密Cr_2O_3耐火材料及其应用 被引量:3
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作者 尹洪基 耿可明 徐延庆 《玻璃》 2007年第1期29-33,共5页
介绍了致密氧化铬耐火材料的生产工艺及性能,详细论述了其在无碱玻璃纤维及钠钙硅玻璃窑炉上的应用及注意事项。
关键词 致密氧化铬耐火材料 无碱玻璃纤维窑炉 钠钙硅玻璃熔窑
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井壁强化机理与致密承压封堵钻井液技术新进展 被引量:25
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作者 邱正松 暴丹 +2 位作者 李佳 刘均一 陈家旭 《钻井液与完井液》 CAS 北大核心 2018年第4期1-6,共6页
井壁强化钻井液技术已成为提高地层承压能力的重要手段之一,目前中国在井壁强化微观机理、模拟实验评价方法和新材料研发等方面,均有待深入研究。基于微观颗粒物质力学的力链网络结构分析基本原理,探讨了裂缝地层致密承压封堵方法。提... 井壁强化钻井液技术已成为提高地层承压能力的重要手段之一,目前中国在井壁强化微观机理、模拟实验评价方法和新材料研发等方面,均有待深入研究。基于微观颗粒物质力学的力链网络结构分析基本原理,探讨了裂缝地层致密承压封堵方法。提出了井壁强化材料特性的精细化表征参数,通过颗粒类型、粒度级配及浓度优化,利用刚性颗粒、弹性颗粒和纤维材料等协同封堵裂缝,可有效形成具有"强力链网络结构"的致密承压封堵层。利用自行研制的井壁强化钻井液封堵模拟实验装置,开展了井壁强化钻井液封堵模拟实验优化研究。模拟实验证明,新研制的井壁强化材料不仅能够有效封堵裂缝,形成致密承压裂缝封堵层,且当支撑裂缝至设计开度,可提升地层承压能力。 展开更多
关键词 井壁强化 微观机理 强力链网络结构 致密承压封堵材料 钻井液 模拟试验方法
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纳米材料
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作者 王辰光 《阜阳师范学院学报(自然科学版)》 2002年第3期71-75,共5页
本文介绍了纳米材料的研究现状和发展前景,以及制备纳米材料的一些方法。
关键词 纳米材料 纳米科技 制备方法 纳米粉末材料 纳米多孔材料 纳米致密材料 纳米复合材料
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喷射沉积耐热铝合金管材挤压过程的数值模拟 被引量:1
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作者 谭敦强 黎文献 +3 位作者 肖于德 唐建成 周浪 张迎元 《中国有色金属学报》 EI CAS CSCD 北大核心 2005年第12期1992-1997,共6页
采用DEFORM有限元软件研究了非致密大规格喷射沉积耐热铝合金管材挤压制备的外径为417 mm、内径为340 mm管材的变形过程,并模拟了挤压过程中应力场、应变场、致密度以及挤压力的变化情况。模拟结果表明:挤压初期为压实阶段,挤压力增加缓... 采用DEFORM有限元软件研究了非致密大规格喷射沉积耐热铝合金管材挤压制备的外径为417 mm、内径为340 mm管材的变形过程,并模拟了挤压过程中应力场、应变场、致密度以及挤压力的变化情况。模拟结果表明:挤压初期为压实阶段,挤压力增加缓慢;随着挤压过程的不断进行,从挤压尾部到挤压头部,管坯的致密度呈阶梯式增加,等效应变、应力和应变速率的变化规律与致密度相类似;在挤压变形区应变、应力和应变速率变化剧烈;挤压后的管材为致密材料,最大挤压力为6.45×104kN,与实际挤压过程中挤压力和致密度相比较,计算机模拟结果与实验结果基本相符。 展开更多
关键词 耐热铝合金 致密材料 高温变形 数值模拟 喷射沉积
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DSHCC加固钢筋混凝土梁抗剪性能试验研究 被引量:3
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作者 谢海波 田仲初 《铁道科学与工程学报》 CAS CSCD 北大核心 2017年第3期520-527,共8页
采用致密化方法对普通"应变硬化水泥基复合材料(SHCC)"进行改进得到的"致密应变硬化水泥基复合材料(DSHCC)"具有更高的抗压、抗拉强度和弹性模量。已有研究证明DSHCC比SHCC具有更加优异的抗弯加固性能。基于RC梁抗... 采用致密化方法对普通"应变硬化水泥基复合材料(SHCC)"进行改进得到的"致密应变硬化水泥基复合材料(DSHCC)"具有更高的抗压、抗拉强度和弹性模量。已有研究证明DSHCC比SHCC具有更加优异的抗弯加固性能。基于RC梁抗剪原理,抗拉强度较高的DSHCC对加固梁抗剪性能也将非常有利。为此,对剪跨比分别为3.2和2.2两组共6根试验梁进行试验研究。对比分析加固梁和RC基准梁剪切破坏模式、承载力、变形能力以及裂缝分布等方面的不同;结合有限元和桁-拱理论分析,推导斜截面极限承载简化计算公式,并用试验结果验证该简化公式的可靠性。研究成果将为DSHCC材料及其在桥梁加固方面的工程应用和推广提供理论依据和参考。 展开更多
关键词 钢筋混凝土梁 加固 致密应变硬化水泥基复合材料 试验研究 剪切性能
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Densification process of 10%B_4C-AA2024 matrix composite strips by semi-solid powder rolling 被引量:1
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作者 莫灼强 刘允中 +1 位作者 贾惠芳 吴敏 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2015年第10期3181-3188,共8页
Semi-solid powder rolling(SSPR) is a novel strip manufacturing process,which includes the features of semi-solid rolling and powder rolling.In this work,densification process and deformation mechanisms of B4 C and A... Semi-solid powder rolling(SSPR) is a novel strip manufacturing process,which includes the features of semi-solid rolling and powder rolling.In this work,densification process and deformation mechanisms of B4 C and AA2024 mixed powders in the presence of liquid phase were investigated.The relationships between relative densities and rolling forces were analyzed as well.The results show that liquid fraction plays an important role in the densification process which can be divided into three stages.Rolling deformation is the main densification mechanism in deformation area when the liquid fraction is lower than 20%.When the liquid fraction is equal to or higher than 20%,the flowing and filling of liquid phase are the densification mechanisms in deformation area.The relative densities increase with increasing rolling forces.The relative density–rolling force curves are similar at 550 °C and 585 °C.The characteristics of the curve shapes are apparently different at 605 °C and 625 °C. 展开更多
关键词 semi-solid powder rolling composite strip densification process rolling deformation
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The effect of modification of matrix on densification efficiency of pitch based carbon composites 被引量:3
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作者 MOHAMMAD Mahdi Sotoudehnia ALI Khalife Soltani +1 位作者 AMIR Maghsouipour FATOLLAH Moztarzadeh 《Journal of Coal Science & Engineering(China)》 2010年第4期408-414,共7页
Using coal tar pitch as a matrix precursor to prepare carbon materials is widelyused by impregnation/carbonization processing technology.Four different grades of coaltar pitch and a natural pitch were characterized in... Using coal tar pitch as a matrix precursor to prepare carbon materials is widelyused by impregnation/carbonization processing technology.Four different grades of coaltar pitch and a natural pitch were characterized in terms of carbon yield, density, viscosity,and fractionation with solvents, as well as by thermal analysis methods.The suitability ofthese commercially available matrices for densification of 3 dimensional carbon-carboncomposites was examined.The theoretical results compared with experimental results.The highest density after impregnation was obtained using one of the coal tar pitches.Thepredicted results are in reasonable agreement with experiment data.The significance ofthis research is that a special heat treatment regime was conducted.The effects of modificationtemperature on the densification efficiency of composites were investigated andthen structure and characteristics of the composites were determined by scanning electronmicroscopy (SEM), Transmission electron microscopy (TEM) and X-Ray Diffraction (XRD). 展开更多
关键词 PITCH CARBONIZATION IMPREGNATION C/C composites
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Fabrication of flexible organic light-emitting diodes with Alq_3 as emitting layer
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作者 SUN Yuan-yuan HUA Yu-lin +4 位作者 XU Feng YIN Shou-gen ZHENG Jia-jin WANG Shu-guo FENG Xiu-lan 《Optoelectronics Letters》 EI 2005年第1期13-16,共4页
Fabrication of flexible organic light-emitting diodes(FOLEDs) with ITO/PVK:TPD/Alq3/Al configuration prepared on PET substrates is reported.Alq3 is used as the light-emitting material.The curves of the current densi... Fabrication of flexible organic light-emitting diodes(FOLEDs) with ITO/PVK:TPD/Alq3/Al configuration prepared on PET substrates is reported.Alq3 is used as the light-emitting material.The curves of the current density vs.voltage,optical current vs.voltage and quantum efficiency vs.current density of the devices are investigated.Compared the devices with the ones that have the same configuration and are fabricated under the same conditions but on glass substrates,the characteristics of the two kinds of devices are very similar except that the threshold voltage of the flexible FOLEDs is a little higher.Under the driving voltage of 20V,the corresponding brightness and the external quantum efficiency are 1000 cd/m2 and 0.27%,respectively.In addition,the anti-bend ability of the devices is tested and the reasons of failure of the devices are analyzed. 展开更多
关键词 二极管 发光材料 光致发光 ALQ3 光密度
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遨游在神奇纳米世界的人——记青年博士卢柯
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作者 杨洪颖 《科技成果纵横》 1999年第5期15-17,共3页
关键词 纳米材料 致密纳米材料 研究 卢柯 制备
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Highly densified carbon electrode materials towards practical supercapacitor devices 被引量:10
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作者 Shuilin Wu 《Science China Materials》 SCIE EI CSCD 2017年第1期25-38,共14页
Supercapacitors are expected to bridge the gap between conventional electrostatic capacitors and batteries, but have not found significant application in primary energy devices, partly due to some unsolved problems in... Supercapacitors are expected to bridge the gap between conventional electrostatic capacitors and batteries, but have not found significant application in primary energy devices, partly due to some unsolved problems in the elec- trode materials. A wide range of novel materials such as novel carbons have been investigated to increase the energy den- sity of the electrodes and the volumetric merits of the materi- als need to be specifically considered and evaluated, towards the practical application of these novel materials. In obser- vation of the intense research activity to improve the volu- metric performance of carbon electrodes, the density or mass loading is particularly important and shall be further opti- mized, both for commercially applied activated carbons and in novel carbon electrode materials such as graphene. In this review, we presented a brief overview of the recent progress in improving the volumetric performance of carbon-based su- percapacitor electrodes, particularly highlighting the devel- opment of densified electrodes by various technical strategies including the controlled assembly of carbon building blocks, developing carbon based hybrid composites and constructing micro- supercapacitors. 展开更多
关键词 GRAPHENE SUPERCAPACITORS microsupercapacitors electrode materials CARBONS
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Advances in dielectric elastomer actuation technology 被引量:8
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作者 WANG NianFeng CUI ChaoYu +2 位作者 GUO Hao CHEN BiCheng ZHANG XianMin 《Science China(Technological Sciences)》 SCIE EI CAS CSCD 2018年第10期1512-1527,共16页
Dielectric elastomer actuators(DEAs) have attracted much interest over the past decades due to the inherent flexibility, large strain, high efficiency, high energy density, and fast response of the material, which are... Dielectric elastomer actuators(DEAs) have attracted much interest over the past decades due to the inherent flexibility, large strain, high efficiency, high energy density, and fast response of the material, which are known as one of the most promising candidates for artificial muscle. In this paper, we first introduce the actuation principle and electromechanical modeling approaches of dielectric elastomers(DEs). Then, the performance of different DEs material and existing compliant electrodes that are widely utilized for DEAs are presented. We also highlight the compatibility of DEs, which is suitable for a variety of actuator designs and applications. Lastly, we summarize the challenges and future development in terms of electromechanical modeling, improvement of materials including compliant electrodes and dielectric elastomer, designs and applications of novel dielectric elastomer actuators. 展开更多
关键词 dielectric elastomer electromechanical modeling compliant electrodes ACTUATOR
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Giant magnetostrictive materials 被引量:8
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作者 LIU JingHua JIANG ChengBao XU HuiBin 《Science China(Technological Sciences)》 SCIE EI CAS 2012年第5期1319-1326,共8页
Giant magnetostrictive materials are a kind of functional materials developed since 1970s, known as their large magnetostrain and high energy density. In this paper, an introduction of magnetostriction and the history... Giant magnetostrictive materials are a kind of functional materials developed since 1970s, known as their large magnetostrain and high energy density. In this paper, an introduction of magnetostriction and the history of magnetostrictive materials are described firstly. Then we review the recent developments of both rare earth and non-rare earth magnetostrictive materials. Finally, the tendency of developing new giant magnetostrictive materials is presented. 展开更多
关键词 giant magnetostrictive materials MAGNETOSTRICTION MAGNETIZATION
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Preparation,characterization and densification studies of W-Ag nanocomposites produced by chemical route
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作者 M.Venkat Reddy A.Krishnaiah P.Venkateshwar Reddy 《Low-carbon Materials and Green Construction》 2023年第1期254-262,共9页
W-Ag has applications in a wide range of cutting-edge fields,counting heat sinks and microwave absorbers for micro—electronic components,electric arc ends,and filaments for welding processes,electrical contacts,and d... W-Ag has applications in a wide range of cutting-edge fields,counting heat sinks and microwave absorbers for micro—electronic components,electric arc ends,and filaments for welding processes,electrical contacts,and durable electronic connections.Chemical methods provide a number of benefits,including improved purity,and controlled particle size.The present study focused on the fabrication of W-Ag nano composites using chemical synthesis.W-Ag nanocomposites with average size less than 50 nm were synthesized using Tungsten hexacarbonyl(W(CO)_(6),and silver acetate(CH_(3)-COOAg)as metal precursors in the present study.The W-Ag composites were sintered using conventional sintering.X-ray diffraction studies of as-prepared powders showed amorphous W-phase and FCC Ag,while sintered W-Ag composites exhibited crystalline BCC W and FCC Ag phase.The effect of sintering temperature on relative density and mechanical properties of W-Ag sintered compacts was investigated.Relative density in excess of 97.6%,98.2%and 98.8%was achieved for W-20.3 wt.%Ag,W-30.1 wt.%Ag and W-39.8 wt.%Ag composites on conventional sintering at 1000℃ for 1 h.Vickers hardness of 364±10 and 320±8 Hv and 279±6 were achieved for W-20.3 wt.%Ag,W-30.1 wt.%Ag and W-39.8 wt.%Ag composite compacts respectively.The hardness value of W-Ag composites decreased with an increase in Ag content.The combination of properties realized in this study renders the composites suitable for automotive and heat sink applications. 展开更多
关键词 W-Ag nanocomosites DENSIFICATION Vickers Hardness Friction coefficient Conventional sintering
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