In order to enhance the mechanical properties of the selective laser-melted(SLM) high-Mg content AlSiMg1.4 alloy,the Zr element was introduced.The influence of Zr alloying on the processability,microstructure,and mech...In order to enhance the mechanical properties of the selective laser-melted(SLM) high-Mg content AlSiMg1.4 alloy,the Zr element was introduced.The influence of Zr alloying on the processability,microstructure,and mechanical properties of the alloy was systematically investigated through performing microstructure analysis and tensile testing.It was demonstrated that the SLM-fabricated AlSiMg1.4-Zr alloy exhibited high process stability with a relative density of over 99.5% at various process parameters.Besides,the strong grain refinement induced by the primary Al3Zr particle during the melt solidification process simultaneously enhanced both the strength and plasticity of the alloy.The values for the yield strength,ultimate tensile strength,and elongation of the SLM-fabricated AlSiMg1.4-Zr were(343±3) MPa,(485±4) MPa,and(10.2±0.2)%,respectively,demonstrating good strengthplasticity synergy in comparison to the AlSiMg1.4 and other Al-Si-based alloys fabricated by SLM.展开更多
[Objective]The aim was to explore effects of curing technique parameters on chemical components and aromatic material accumulation to formulate a suitable curing technique and for and to achieve tobacco scalding, dryi...[Objective]The aim was to explore effects of curing technique parameters on chemical components and aromatic material accumulation to formulate a suitable curing technique and for and to achieve tobacco scalding, drying and giving aromat- ic flavor. [Method] With tobacco variety KRK 26 as test materials, the test involved parameters of three curing-techniques in down, middle and upper parts of flue-cured tobaccos in an oven to measure chemical components and aromatic substances in tobaccos. [Result] The effects of curing techniques on total sugar and reducing sug- ar differed upon temperature and humidity. The contents of chemical components, such as total alkaloid, total N and the ratio of sugar/ alkali by moderate temperature and high humidity technique were of significant differences with those by moderate temperature and moderate humidity technique and with low temperature and low hu- midity technique; the chemical components by moderate temperature and moderate humidity were of insignificant differences with the treatment by low temperature and low humidity technique. Total amount of aroma components by different curing tech- niques from high to low was the treatment by low temperature and low humidity technique (461.72 μg/g), the treatment by moderate temperature and moderate hu- midity technique (450.06μg/g) and the treatment by moderate temperature and high humidity technique (385.12μg/g), suggesting the content of aromatic substances is high at low temperature and low humidity. [Conclusion] Moderate temperature and high humidity curing technique has significant effects on total alkaloid, total N and the ratio of sugar/ alkali of tobaccos and different curing techniques also affect the total amount of aromatic substances of flue-cured tobaccos.展开更多
To improve the poor stability of casting process of Al alloy with high Mg content, which leads to poor final product quality, the melting purification process and the influences of the refiner on the microstructure an...To improve the poor stability of casting process of Al alloy with high Mg content, which leads to poor final product quality, the melting purification process and the influences of the refiner on the microstructure and defect of 5083 alloy were studied. The results show that the optimized process for the rotary impeller degassing of 5083 alloy is as follows: a rotary speed of 250-400 r/min; a gas flow of 1.2-2.0 L/s, a refining time of 10-15 min. This optimized process can reduce the gas content in the solid alloy to 2× 10^-3 mL/g or lower. Due to the addition of grain refiner, the cast microstructure of 5083 alloy is refined. The Al-5Ti-IB wire shows the best refining effect among all the refiners. The refining effect is improved with the increase of grain refiner addition amount. And the refinement effects become stable when Ti content reaches 0.1% or higher. The surface crinkling defect of the billet can be easily found in the alloy refined with Al-5Ti-IB wire compared with the alloys refined with other refiners.展开更多
A new severe plastic deformation (SPD) method that is extrusion-shearing (ES), which includes initial forward extrusion and shearing process subsequently, was developed to fabricate the fine grained AZ31 Mg alloys...A new severe plastic deformation (SPD) method that is extrusion-shearing (ES), which includes initial forward extrusion and shearing process subsequently, was developed to fabricate the fine grained AZ31 Mg alloys. The components of ES die were manufactured and installed to gleeble1500D thermo-mechanical simulator. Microstructure observations were carried out in different positions of ES formed rods. The results show that homogeneous microstructures with mean grain size of 2 μm are obtained at lower temperature as the accumulated true strain is 2.44. Occurring of continuous dynamic recrystallization (DRX) is the main reason for grain refinement during ES process. The experimental results show that the ES process effectively refines the grains of AZ31 magnesium. The production results of ES extrusion with industrial extruder under different extrusion conditions show that the ES extrusion can be applied in large-scale industry.展开更多
The optimal process for orange vinegar was investigated in order to explore the effect of process parameters and obtain the superior process parameters.The process for orange vinegar was optimized using single-factor ...The optimal process for orange vinegar was investigated in order to explore the effect of process parameters and obtain the superior process parameters.The process for orange vinegar was optimized using single-factor methodology and Box-behnken methodology, and the effect of process parameters was analyzed in the light of response surface plots. Results were as follows. The optimal process of alcohol fermentation was as follows: original sugar degree of 16%, yeast inoculum size of 5% and p H value of 3.5 through single-factor experiment. The optimal fermentation process of acetic acid optimized by response surface methodology was as follows: inoculum size of 8.52%, original alcohol content of 6.0% and p H value of 3.3, in the optimal condition the yield of acetic acid was 53.11 g/L. Single factor action and the interaction of two factors were presented on the yield of acetic acid.The effects of inoculum size and p H were extremely significant, and that of original alcohol content significant. The interaction of inoculum size and original alcohol content was non-significant, that of inoculum size and p H also non-significant. On contrast, original alcohol content and p H had significant interaction.展开更多
The layered Li[Ni1/3Mn1/3Co1/3]O2 was separately synthesized by pretreatment process of ball mill method and solution phase route, using [Ni1/3Co1/3Mn1/3]3O4 and lithium hydroxide as raw materials. The physical and el...The layered Li[Ni1/3Mn1/3Co1/3]O2 was separately synthesized by pretreatment process of ball mill method and solution phase route, using [Ni1/3Co1/3Mn1/3]3O4 and lithium hydroxide as raw materials. The physical and electrochemical behaviors of Li[Ni1/3Mn1/3Co1/3]O2 were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), field emission scanning electron microscopy (FESEM) and electrochemical charge/discharge cycling tests. The results show that the difference in pretreatment process results in the difference in compound Li[Ni1/3Co1/3Mn1/3]O2 structure, morphology and the electrochemical characteristics. The Li[Ni1/3Mn1/3Co1/3]O2 prepared by solution phase route maintains the uniform spherical morphology of the [Ni1/3Co1/3Mn1/3]3O4, and it exhibits a higher capacity retention and better rate capability than that prepared by ball mill method. The initial discharge capacity of this sample reaches 178 mA-h/g and the capacity retention after 50 cycles is 98.7% at a current density of 20 mA/g. Moreover, it delivers high discharge capacity of 135 mA-h/g at a current density of 1 000 mA/g.展开更多
In order to solve the problems of low production efficiency,great loss and low yield,Millet Research Institute of Hebei Academy of Agriculture and Forestry Sciences integrated the plastic film mulching technique and m...In order to solve the problems of low production efficiency,great loss and low yield,Millet Research Institute of Hebei Academy of Agriculture and Forestry Sciences integrated the plastic film mulching technique and mechanized production technique,forming a foxtail millet production technique combining machinery and agronomy.The foxtail millet production technique combining machinery and agronomy regulates millet production from the links of soil preparation,fertilization,variety selection,seeding,intertillage and fertilization and harvest,so as to achieve the effects of promoting the matching between agro-machinery and agronomy,improving the level of millet production mechanization,realizing light simplified production and saving labor cost.This technical regulation has a broad application prospect.展开更多
The high temperature deformation behaviors of α+β type titanium alloy TC11 (Ti-6.5Al-3.5Mo-1.5Zr-0.3Si) with coarse lamellar starting microstructure were investigated based on the hot compression tests in the tem...The high temperature deformation behaviors of α+β type titanium alloy TC11 (Ti-6.5Al-3.5Mo-1.5Zr-0.3Si) with coarse lamellar starting microstructure were investigated based on the hot compression tests in the temperature range of 950-1100 ℃ and the strain rate range of 0.001-10 s-1. The processing maps at different strains were then constructed based on the dynamic materials model, and the hot compression process parameters and deformation mechanism were optimized and analyzed, respectively. The results show that the processing maps exhibit two domains with a high efficiency of power dissipation and a flow instability domain with a less efficiency of power dissipation. The types of domains were characterized by convergence and divergence of the efficiency of power dissipation, respectively. The convergent domain in a+fl phase field is at the temperature of 950-990 ℃ and the strain rate of 0.001-0.01 s^-1, which correspond to a better hot compression process window of α+β phase field. The peak of efficiency of power dissipation in α+β phase field is at 950 ℃ and 0.001 s 1, which correspond to the best hot compression process parameters of α+β phase field. The convergent domain in β phase field is at the temperature of 1020-1080 ℃ and the strain rate of 0.001-0.1 s^-l, which correspond to a better hot compression process window of β phase field. The peak of efficiency of power dissipation in ℃ phase field occurs at 1050 ℃ over the strain rates from 0.001 s^-1 to 0.01 s^-1, which correspond to the best hot compression process parameters of ,8 phase field. The divergence domain occurs at the strain rates above 0.5 s^-1 and in all the tested temperature range, which correspond to flow instability that is manifested as flow localization and indicated by the flow softening phenomenon in stress-- strain curves. The deformation mechanisms of the optimized hot compression process windows in a+β and β phase fields are identified to be spheroidizing and dynamic recrystallizing controlled by self-diffusion mechanism, respectively. The microstructure observation of the deformed specimens in different domains matches very well with the optimized results.展开更多
Microstructure, precipitate and magnetic characteristic of fmal products with different normalizing cooling processes for Fe-3.2%Si low-temperature hot-rolled grain-oriented silicon steel were analyzed and compared wi...Microstructure, precipitate and magnetic characteristic of fmal products with different normalizing cooling processes for Fe-3.2%Si low-temperature hot-rolled grain-oriented silicon steel were analyzed and compared with the hot-rolled plate by optical microscopy (OM), transmission electron microscopy (TEM), and energy dispersive spectrometry (EDS). The results show that, the surface microstructure is uniform, the proportion of recrystallization in matrix increases, and the banding textures are narrowed; the precipitates, whose quantity in normalized plate is more than that in hot-rolled plate greatly, are mainly A1N, MnS, composite precipitates (Cu,Mn)S and so on. Normalizing technology with a temperature of 1120 ℃, holding for 3 min, and a two-stage cooling is a most advantaged method to obtain oriented silicon steel with sharper Goss texture and higher magnetic properties, owing to the uniform surface microstructures and the obvious inhomogeneity of microstructures along the thickness. The normalizing technology with the two-stage cooling is the optimum process, which can generate more fine precipitates dispersed over the matrix, and be beneficial for finished products to get higher magnetic properties.展开更多
In order to minimize the crystal phase in Al-Cu-Ti amorphous powder,Al65Cu35-xTix amorphous powders were optimized via ball milling through adjusting the amount of Cu and Ti elements and the ball milling time.The resu...In order to minimize the crystal phase in Al-Cu-Ti amorphous powder,Al65Cu35-xTix amorphous powders were optimized via ball milling through adjusting the amount of Cu and Ti elements and the ball milling time.The results show that increasing the mole fraction of Ti can decrease the amount of Al Cu2Ti,Cu9Al4,and Al2Cu intermetallics formed during the process of ball milling;and prolonging the ball milling time can reduce the element crystalline phase to almost none.The optimal composition is determined to be Al65Cu16.5Ti18.5.TiH2 forms in all selected Al65Cu35-xTix amorphous powders during the process of optimization.H atom is decomposed from toluene and reacts with Ti during ball milling,leading to the formation of TiH2.The volume fraction of TiH2 in Al65Cu16.5Ti18.5 amorphous powder is measured to be 4.30%.展开更多
Step channel direct injection(SCDI) flash memory device is successfully achieved by 1 2μm CMOS technology,moreover good performance is obtained.At the bias condition of V g=6V, V d=5V,the programming speed ...Step channel direct injection(SCDI) flash memory device is successfully achieved by 1 2μm CMOS technology,moreover good performance is obtained.At the bias condition of V g=6V, V d=5V,the programming speed of SCDI device is 42μs.Under the condition of V g=-8V, V s=8V,the erasing speed is 24ms.Compared with the same size of conventional flash memory device whose corresponding parameters are 500μs and 24ms,respectively,the performance of SCDI device is remarkably improved.During manufacturing of SCDI device,the key technologies are to make the shallow step with appropriate depth and angle,along with eliminating the etch damage during the process of Si 3N 4 spacer.展开更多
The processes of flooding—water flooding, polymer flooding and ternary combination flooding—were simulated respectively on a 2-D positive rhythm profile geological model by using the ASP numerical modeling softw...The processes of flooding—water flooding, polymer flooding and ternary combination flooding—were simulated respectively on a 2-D positive rhythm profile geological model by using the ASP numerical modeling software developed by RIPED (Yuan, et al. 1995). The recovery coefficient, remaining oil saturation, sweep efficiency and displacement efficiency were calculated and correlated layer by layer. The results show that the sweep efficiency and displacement efficiency work different effects on different layers in the severely heterogeneous reservoir. The study shows that the displacement efficiency and sweep efficiency play different roles in different layers for severely heterogeneous reservoirs. The displacement efficiency contributes mainly to the high permeability zones, the sweep efficiency to the low permeability zones, both of which contribute to the middle permeable zones. To improve the sweep efficiency in the low permeability zones is of significance for enhancing the whole recovery of the reservoir. It is an important path for improving the effectiveness of chemical flooding in the severely heterogeneous reservoirs to inject ternary combination slug after profile control.展开更多
基金supported by the National Natural Science Foundation of China (Nos.51801079, 52001140)。
文摘In order to enhance the mechanical properties of the selective laser-melted(SLM) high-Mg content AlSiMg1.4 alloy,the Zr element was introduced.The influence of Zr alloying on the processability,microstructure,and mechanical properties of the alloy was systematically investigated through performing microstructure analysis and tensile testing.It was demonstrated that the SLM-fabricated AlSiMg1.4-Zr alloy exhibited high process stability with a relative density of over 99.5% at various process parameters.Besides,the strong grain refinement induced by the primary Al3Zr particle during the melt solidification process simultaneously enhanced both the strength and plasticity of the alloy.The values for the yield strength,ultimate tensile strength,and elongation of the SLM-fabricated AlSiMg1.4-Zr were(343±3) MPa,(485±4) MPa,and(10.2±0.2)%,respectively,demonstrating good strengthplasticity synergy in comparison to the AlSiMg1.4 and other Al-Si-based alloys fabricated by SLM.
基金Supported by China National Tobacco Corporation General Project(〔2012〕122)Chongqing Branch Company S&T Project of China National Tobacco Corporation(NY20110601070010)~~
文摘[Objective]The aim was to explore effects of curing technique parameters on chemical components and aromatic material accumulation to formulate a suitable curing technique and for and to achieve tobacco scalding, drying and giving aromat- ic flavor. [Method] With tobacco variety KRK 26 as test materials, the test involved parameters of three curing-techniques in down, middle and upper parts of flue-cured tobaccos in an oven to measure chemical components and aromatic substances in tobaccos. [Result] The effects of curing techniques on total sugar and reducing sug- ar differed upon temperature and humidity. The contents of chemical components, such as total alkaloid, total N and the ratio of sugar/ alkali by moderate temperature and high humidity technique were of significant differences with those by moderate temperature and moderate humidity technique and with low temperature and low hu- midity technique; the chemical components by moderate temperature and moderate humidity were of insignificant differences with the treatment by low temperature and low humidity technique. Total amount of aroma components by different curing tech- niques from high to low was the treatment by low temperature and low humidity technique (461.72 μg/g), the treatment by moderate temperature and moderate hu- midity technique (450.06μg/g) and the treatment by moderate temperature and high humidity technique (385.12μg/g), suggesting the content of aromatic substances is high at low temperature and low humidity. [Conclusion] Moderate temperature and high humidity curing technique has significant effects on total alkaloid, total N and the ratio of sugar/ alkali of tobaccos and different curing techniques also affect the total amount of aromatic substances of flue-cured tobaccos.
基金Project(12511075)supported by the Foundation of Heilongjiang Education Committee,China
文摘To improve the poor stability of casting process of Al alloy with high Mg content, which leads to poor final product quality, the melting purification process and the influences of the refiner on the microstructure and defect of 5083 alloy were studied. The results show that the optimized process for the rotary impeller degassing of 5083 alloy is as follows: a rotary speed of 250-400 r/min; a gas flow of 1.2-2.0 L/s, a refining time of 10-15 min. This optimized process can reduce the gas content in the solid alloy to 2× 10^-3 mL/g or lower. Due to the addition of grain refiner, the cast microstructure of 5083 alloy is refined. The Al-5Ti-IB wire shows the best refining effect among all the refiners. The refining effect is improved with the increase of grain refiner addition amount. And the refinement effects become stable when Ti content reaches 0.1% or higher. The surface crinkling defect of the billet can be easily found in the alloy refined with Al-5Ti-IB wire compared with the alloys refined with other refiners.
基金Project (2007CB613700) supported by the National Basic Research Program of ChinaProject (50725413)supported by the National Natural Science Foundation of China+2 种基金Project (CQ CSTC,2010BB4301)supported by National Science Foundation of Chongqing, ChinaProject (CSTC2009AB4008) supported by Chongqing Sci & Tech Development Program, ChinaProject (2010CSTC-HDLS)supported by Chongqing Sci & Tech Commission, China
文摘A new severe plastic deformation (SPD) method that is extrusion-shearing (ES), which includes initial forward extrusion and shearing process subsequently, was developed to fabricate the fine grained AZ31 Mg alloys. The components of ES die were manufactured and installed to gleeble1500D thermo-mechanical simulator. Microstructure observations were carried out in different positions of ES formed rods. The results show that homogeneous microstructures with mean grain size of 2 μm are obtained at lower temperature as the accumulated true strain is 2.44. Occurring of continuous dynamic recrystallization (DRX) is the main reason for grain refinement during ES process. The experimental results show that the ES process effectively refines the grains of AZ31 magnesium. The production results of ES extrusion with industrial extruder under different extrusion conditions show that the ES extrusion can be applied in large-scale industry.
基金financially supported in part by Guangdong Province Ministry of industry university research project (No. 2013B090600032)Science and Technology Project Program of Guangdong Province (No. 2014B040404027)
文摘The optimal process for orange vinegar was investigated in order to explore the effect of process parameters and obtain the superior process parameters.The process for orange vinegar was optimized using single-factor methodology and Box-behnken methodology, and the effect of process parameters was analyzed in the light of response surface plots. Results were as follows. The optimal process of alcohol fermentation was as follows: original sugar degree of 16%, yeast inoculum size of 5% and p H value of 3.5 through single-factor experiment. The optimal fermentation process of acetic acid optimized by response surface methodology was as follows: inoculum size of 8.52%, original alcohol content of 6.0% and p H value of 3.3, in the optimal condition the yield of acetic acid was 53.11 g/L. Single factor action and the interaction of two factors were presented on the yield of acetic acid.The effects of inoculum size and p H were extremely significant, and that of original alcohol content significant. The interaction of inoculum size and original alcohol content was non-significant, that of inoculum size and p H also non-significant. On contrast, original alcohol content and p H had significant interaction.
基金Project(20871101)supported by the National Natural Science Foundation of ChinaProject(2009WK2007)supported by Key Project of Science and Technology Department of Hunan Province,ChinaProject(CX2009B133)supported by Colleges and Universities in Hunan Province Plans to Graduate Research and Innovation,China
文摘The layered Li[Ni1/3Mn1/3Co1/3]O2 was separately synthesized by pretreatment process of ball mill method and solution phase route, using [Ni1/3Co1/3Mn1/3]3O4 and lithium hydroxide as raw materials. The physical and electrochemical behaviors of Li[Ni1/3Mn1/3Co1/3]O2 were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), field emission scanning electron microscopy (FESEM) and electrochemical charge/discharge cycling tests. The results show that the difference in pretreatment process results in the difference in compound Li[Ni1/3Co1/3Mn1/3]O2 structure, morphology and the electrochemical characteristics. The Li[Ni1/3Mn1/3Co1/3]O2 prepared by solution phase route maintains the uniform spherical morphology of the [Ni1/3Co1/3Mn1/3]3O4, and it exhibits a higher capacity retention and better rate capability than that prepared by ball mill method. The initial discharge capacity of this sample reaches 178 mA-h/g and the capacity retention after 50 cycles is 98.7% at a current density of 20 mA/g. Moreover, it delivers high discharge capacity of 135 mA-h/g at a current density of 1 000 mA/g.
文摘In order to solve the problems of low production efficiency,great loss and low yield,Millet Research Institute of Hebei Academy of Agriculture and Forestry Sciences integrated the plastic film mulching technique and mechanized production technique,forming a foxtail millet production technique combining machinery and agronomy.The foxtail millet production technique combining machinery and agronomy regulates millet production from the links of soil preparation,fertilization,variety selection,seeding,intertillage and fertilization and harvest,so as to achieve the effects of promoting the matching between agro-machinery and agronomy,improving the level of millet production mechanization,realizing light simplified production and saving labor cost.This technical regulation has a broad application prospect.
基金Project (51005112) supported by the National Natural Science Foundation of ChinaProject (2010ZF56019) supported by the Aviation Science Foundation of China+1 种基金Project (GJJ11156) supported by the Education Commission of Jiangxi Province, ChinaProject(GF200901008) supported by the Open Fund of National Defense Key Disciplines Laboratory of Light Alloy Processing Science and Technology, China
文摘The high temperature deformation behaviors of α+β type titanium alloy TC11 (Ti-6.5Al-3.5Mo-1.5Zr-0.3Si) with coarse lamellar starting microstructure were investigated based on the hot compression tests in the temperature range of 950-1100 ℃ and the strain rate range of 0.001-10 s-1. The processing maps at different strains were then constructed based on the dynamic materials model, and the hot compression process parameters and deformation mechanism were optimized and analyzed, respectively. The results show that the processing maps exhibit two domains with a high efficiency of power dissipation and a flow instability domain with a less efficiency of power dissipation. The types of domains were characterized by convergence and divergence of the efficiency of power dissipation, respectively. The convergent domain in a+fl phase field is at the temperature of 950-990 ℃ and the strain rate of 0.001-0.01 s^-1, which correspond to a better hot compression process window of α+β phase field. The peak of efficiency of power dissipation in α+β phase field is at 950 ℃ and 0.001 s 1, which correspond to the best hot compression process parameters of α+β phase field. The convergent domain in β phase field is at the temperature of 1020-1080 ℃ and the strain rate of 0.001-0.1 s^-l, which correspond to a better hot compression process window of β phase field. The peak of efficiency of power dissipation in ℃ phase field occurs at 1050 ℃ over the strain rates from 0.001 s^-1 to 0.01 s^-1, which correspond to the best hot compression process parameters of ,8 phase field. The divergence domain occurs at the strain rates above 0.5 s^-1 and in all the tested temperature range, which correspond to flow instability that is manifested as flow localization and indicated by the flow softening phenomenon in stress-- strain curves. The deformation mechanisms of the optimized hot compression process windows in a+β and β phase fields are identified to be spheroidizing and dynamic recrystallizing controlled by self-diffusion mechanism, respectively. The microstructure observation of the deformed specimens in different domains matches very well with the optimized results.
基金Projects(51274083,51074062)supported by the National Natural Science Foundation of China
文摘Microstructure, precipitate and magnetic characteristic of fmal products with different normalizing cooling processes for Fe-3.2%Si low-temperature hot-rolled grain-oriented silicon steel were analyzed and compared with the hot-rolled plate by optical microscopy (OM), transmission electron microscopy (TEM), and energy dispersive spectrometry (EDS). The results show that, the surface microstructure is uniform, the proportion of recrystallization in matrix increases, and the banding textures are narrowed; the precipitates, whose quantity in normalized plate is more than that in hot-rolled plate greatly, are mainly A1N, MnS, composite precipitates (Cu,Mn)S and so on. Normalizing technology with a temperature of 1120 ℃, holding for 3 min, and a two-stage cooling is a most advantaged method to obtain oriented silicon steel with sharper Goss texture and higher magnetic properties, owing to the uniform surface microstructures and the obvious inhomogeneity of microstructures along the thickness. The normalizing technology with the two-stage cooling is the optimum process, which can generate more fine precipitates dispersed over the matrix, and be beneficial for finished products to get higher magnetic properties.
基金Projects(51271036,51471035,51101018)supported by the National Natural Science Foundation of ChinaProject supported by the Program of"One Hundred Talented People"of the Chinese Academy of Sciences
文摘In order to minimize the crystal phase in Al-Cu-Ti amorphous powder,Al65Cu35-xTix amorphous powders were optimized via ball milling through adjusting the amount of Cu and Ti elements and the ball milling time.The results show that increasing the mole fraction of Ti can decrease the amount of Al Cu2Ti,Cu9Al4,and Al2Cu intermetallics formed during the process of ball milling;and prolonging the ball milling time can reduce the element crystalline phase to almost none.The optimal composition is determined to be Al65Cu16.5Ti18.5.TiH2 forms in all selected Al65Cu35-xTix amorphous powders during the process of optimization.H atom is decomposed from toluene and reacts with Ti during ball milling,leading to the formation of TiH2.The volume fraction of TiH2 in Al65Cu16.5Ti18.5 amorphous powder is measured to be 4.30%.
文摘Step channel direct injection(SCDI) flash memory device is successfully achieved by 1 2μm CMOS technology,moreover good performance is obtained.At the bias condition of V g=6V, V d=5V,the programming speed of SCDI device is 42μs.Under the condition of V g=-8V, V s=8V,the erasing speed is 24ms.Compared with the same size of conventional flash memory device whose corresponding parameters are 500μs and 24ms,respectively,the performance of SCDI device is remarkably improved.During manufacturing of SCDI device,the key technologies are to make the shallow step with appropriate depth and angle,along with eliminating the etch damage during the process of Si 3N 4 spacer.
基金This project is supported by the China National Key Basis Research Project (No: G1999022512)
文摘The processes of flooding—water flooding, polymer flooding and ternary combination flooding—were simulated respectively on a 2-D positive rhythm profile geological model by using the ASP numerical modeling software developed by RIPED (Yuan, et al. 1995). The recovery coefficient, remaining oil saturation, sweep efficiency and displacement efficiency were calculated and correlated layer by layer. The results show that the sweep efficiency and displacement efficiency work different effects on different layers in the severely heterogeneous reservoir. The study shows that the displacement efficiency and sweep efficiency play different roles in different layers for severely heterogeneous reservoirs. The displacement efficiency contributes mainly to the high permeability zones, the sweep efficiency to the low permeability zones, both of which contribute to the middle permeable zones. To improve the sweep efficiency in the low permeability zones is of significance for enhancing the whole recovery of the reservoir. It is an important path for improving the effectiveness of chemical flooding in the severely heterogeneous reservoirs to inject ternary combination slug after profile control.