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芳基乙酮酸乙酯的合成新方法 被引量:14
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作者 向纪明 陈久存 李宝林 《有机化学》 SCIE CAS CSCD 北大核心 2009年第3期392-395,共4页
以芳烃和草酰氯单乙酯为原料,采用Friedel-Crafts酰基化反应合成了8种芳基乙酮酸乙酯,用IR,1H NMR,元素分析确认了合成化合物结构,并用高效液相色谱法分析了反应的选择性.此合成方法具有反应条件温和、操作简单、产率高的特点.
关键词 芳基乙酮酸乙酯 酰基化反应 合成
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A practical and efficient procedure for the α-bromination of arylethanones 被引量:1
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作者 邢瑞娟 潘莉 +2 位作者 温西 王健 程卯生 《Journal of Chinese Pharmaceutical Sciences》 CAS 2010年第5期400-402,共3页
A series of α-bromoarylethanones were prepared in high yields by a practical and efficient method. The arylethanones were reacted with bromine to give a mixture of α- and α, α-dibromides, which were debrominated w... A series of α-bromoarylethanones were prepared in high yields by a practical and efficient method. The arylethanones were reacted with bromine to give a mixture of α- and α, α-dibromides, which were debrominated with diethylphosphite in the presence of triethylamine to give the desired α-monobromo products. 展开更多
关键词 α-Bromoarylethanones BROMINE Diethylphosphite α-Bromination
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