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苯乙酸对甲苯酯的改进合成 被引量:2
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作者 尹文清 佘志刚 陈育平 《湖北师范学院学报(自然科学版)》 2002年第3期80-81,共2页
苯乙酸和对甲酚在二环己基碳二酰亚胺 (DCC)存在下 ,用 4-二甲氨基吡啶 (DMAP)作催化剂合成苯乙酸对甲苯酯 ,反应时间短 ,反应条件温和 ,后处理容易 。
关键词 苯乙酸对甲苯酯 合成 苯乙酸 对甲酚 4-二甲氨基吡啶 催化剂 反应条件
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Properties of Surface Cyclic Oligomers Present on Polyester Fiber
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作者 郑敏 宋心远 《Journal of Donghua University(English Edition)》 EI CAS 2003年第1期22-26,共5页
The effects of different treatments, such as dry heat,wet heat, solvent vapor and ultrasonic, on propertiesof the cyclic oligomers on the surface of polyester fiberare studied. The components of surface oligomers area... The effects of different treatments, such as dry heat,wet heat, solvent vapor and ultrasonic, on propertiesof the cyclic oligomers on the surface of polyester fiberare studied. The components of surface oligomers areanalyzed through Thin-Layer Chromatograph. Theresult shows that: all of the treatment, especially solvent vapor treatment,call significantly increase the content of surface cyclic oligomers.The content of cyclic triIner is increased more considerably than other oligomers. Moreover,the morphology and thedistribution of surface cyclic oligomers are also different from different treatments:Dry heat and wet heat cause larger polygonal solids distributed evenly on the surface of fiber;solvent vapor nlakes fiber surface exhibit irregular rodlike crystal shapes randomly;ultrasonic treatment induces some obscureand smaller deposi^on the surface of fiber. 展开更多
关键词 heat treatment solvent vapor ULTRASONIC cyclic oligomers thin—layer chromatograph
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