Aim The several species of the genus Paris called ＂Chonglou＂ are famous traditional Chinese herbal medicines. We established the quantitative analysis method of the steroidal saponins in some species of the genus Pa...Aim The several species of the genus Paris called ＂Chonglou＂ are famous traditional Chinese herbal medicines. We established the quantitative analysis method of the steroidal saponins in some species of the genus Paris and discussed their relations. Methods We detected the contents of 11 steroidal saponins in Paris samples with a Kromasel C18 （ 150 mm× 4.6 mm ID, 5μm） column which was subjected to gradient elution with acetonitrile-water （30：70- 60：40, V/V） at a flow rate of 1 mL· min^-1 by HPLC-ELSD and established chemical cluster tree using SPSS 11 software. Results All the samples could be separated and calibration curves of 11 saponins were prepared. We successfully detected the contents of 11 steroidal saponins in 14 Paris spp. in 30 min. The recovery for the assay of saponins was between 95 % and 97 %. The RSD of precision of 11 saponins and stability of samples were below 3 %. Chemical phylogenetic tree based on saponin contents indicated that 17 samples of Paris spp. clustered separately. Conclusion The established method is accurate and convenient, and suitable for the quantitative analysis of these 11 steroidal saponins in Paris spp.. The chemical phylogenetic tree is in accordance with Takhtajian classical taxonomy.展开更多
Microlysimeters of different sizes(5 cm 10 cm and 15 cm in length)were used extensively in the present study for the measurements of soil evapondion in site in an extremely arid area in southern Israel.All of the data...Microlysimeters of different sizes(5 cm 10 cm and 15 cm in length)were used extensively in the present study for the measurements of soil evapondion in site in an extremely arid area in southern Israel.All of the data obtained from the microlysimeters were used to evaluate two conventional eVaporation models developed by Black et al.and Ritchie,respectively.Our results indicated that the models could overestimate total cumulative evaporation by about 30% in the extremely arid environment.Reducing the power factor of the conventional model by a faCtor of 0.1 produced good agreement between the measured and simulated cumulative evaporation.Microlysimeter method proved to be a simple and accurate approach for the evaluation of soil evaporstion.展开更多
The evaporation rate over South China is estimated based on the Climate Prediction Center Merged Analysis of Precipitation(CMAP)data and the NCEP/DOE reanalysis II data from 1979 to 2007. The temporal variation of eva...The evaporation rate over South China is estimated based on the Climate Prediction Center Merged Analysis of Precipitation(CMAP)data and the NCEP/DOE reanalysis II data from 1979 to 2007. The temporal variation of evaporation over South China and its relationship to precipitation are discussed. Climatologically,the evaporation rate over South China is the largest in July and smallest in March.In spring and summer,the evaporation rate is approximately one half of the precipitation rate.However,the evaporation rate is approximately equal to the precipitation rate in fall and winter.The year-to-year variation of the evaporation rate over South China is quite in phase with that of the precipitation rate in the period from February to May but out of phase with that of the precipitation rate in early winter.Over South China there is a pronounced decreasing trend in the evaporation in colder seasons and a positive correlation between the evaporation variation and the rainfall variation in spring.In summer,the abnormality of rainfall over South China is closely related to the anomalous evaporation over the northeastern part of the South China Sea and its eastern vicinity.In winter,the rainfall variation in South China has a close linkage with the evaporation variation in a belt area covering the eastern Arabian Sea,the Bay of Bengal,the southeastern periphery of the Plateau,the southern part of South China Sea and the central part of Indonesia.展开更多
Short path distillation (SPD) is a kind of high vacuum distillation method, which is suitable for the separation of high boiling, heat sensitivity and viscidity products.In this paper,through measuring the phase-avera...Short path distillation (SPD) is a kind of high vacuum distillation method, which is suitable for the separation of high boiling, heat sensitivity and viscidity products.In this paper,through measuring the phase-averaged velocity distributions with a conditional sampling method of the particle imaging velocimetry (PIV), the liquid flow field that affects the heat and mass transfer of evaporating thin-film in an SPD evaporator is investigated.Measured results show that the flow velocities decrease rapidly apart from the wiper at different wiper velocities, the maximum velocity appears before wipers, and the quicker the wiping, the larger the flow velocity. Meanwhile, the evaluation of numerical calculations is carried out.The measured velocity distributions indicate clearly the effect of the wiper both on the flow field along its moving direction and on the vortices behind the wiper.Simulation data show that the performance of liquid flow field on the heating surface not only agrees with the experimental results well,but also can give further more information, such as the distribution of turbulent kinetic energy.In this study,turbulent kinetic energy mainly distributes before wipers and laminar flow appears far away from the wipers.展开更多
Thickness of falling water film out of tubes is one of critical factors of heat transfer of evaporative air cooler. A new method of resistance measurement was developed to measure thickness of the film. When the resis...Thickness of falling water film out of tubes is one of critical factors of heat transfer of evaporative air cooler. A new method of resistance measurement was developed to measure thickness of the film. When the resistance probe on the tip of micrometer touches the surface and bottom of the film, two corresponding sudden reductions of resistance occurs, and the difference of two graduations on the micrometer displays the thickness of the film. The film thickness of eleven angles was measured in five kinds of water flows and results varies from 0.8933mm to 1.7233 mm. Mean thickness and mean heat transfer coefficient of the film out of the tube was calculated.展开更多
文摘Aim The several species of the genus Paris called ＂Chonglou＂ are famous traditional Chinese herbal medicines. We established the quantitative analysis method of the steroidal saponins in some species of the genus Paris and discussed their relations. Methods We detected the contents of 11 steroidal saponins in Paris samples with a Kromasel C18 （ 150 mm× 4.6 mm ID, 5μm） column which was subjected to gradient elution with acetonitrile-water （30：70- 60：40, V/V） at a flow rate of 1 mL· min^-1 by HPLC-ELSD and established chemical cluster tree using SPSS 11 software. Results All the samples could be separated and calibration curves of 11 saponins were prepared. We successfully detected the contents of 11 steroidal saponins in 14 Paris spp. in 30 min. The recovery for the assay of saponins was between 95 % and 97 %. The RSD of precision of 11 saponins and stability of samples were below 3 %. Chemical phylogenetic tree based on saponin contents indicated that 17 samples of Paris spp. clustered separately. Conclusion The established method is accurate and convenient, and suitable for the quantitative analysis of these 11 steroidal saponins in Paris spp.. The chemical phylogenetic tree is in accordance with Takhtajian classical taxonomy.
文摘Microlysimeters of different sizes(5 cm 10 cm and 15 cm in length)were used extensively in the present study for the measurements of soil evapondion in site in an extremely arid area in southern Israel.All of the data obtained from the microlysimeters were used to evaluate two conventional eVaporation models developed by Black et al.and Ritchie,respectively.Our results indicated that the models could overestimate total cumulative evaporation by about 30% in the extremely arid environment.Reducing the power factor of the conventional model by a faCtor of 0.1 produced good agreement between the measured and simulated cumulative evaporation.Microlysimeter method proved to be a simple and accurate approach for the evaluation of soil evaporstion.
基金National Key Program for Developing Basic Research(2009CB421404)Key Program of National Science Foundation of China(40730951)
文摘The evaporation rate over South China is estimated based on the Climate Prediction Center Merged Analysis of Precipitation(CMAP)data and the NCEP/DOE reanalysis II data from 1979 to 2007. The temporal variation of evaporation over South China and its relationship to precipitation are discussed. Climatologically,the evaporation rate over South China is the largest in July and smallest in March.In spring and summer,the evaporation rate is approximately one half of the precipitation rate.However,the evaporation rate is approximately equal to the precipitation rate in fall and winter.The year-to-year variation of the evaporation rate over South China is quite in phase with that of the precipitation rate in the period from February to May but out of phase with that of the precipitation rate in early winter.Over South China there is a pronounced decreasing trend in the evaporation in colder seasons and a positive correlation between the evaporation variation and the rainfall variation in spring.In summer,the abnormality of rainfall over South China is closely related to the anomalous evaporation over the northeastern part of the South China Sea and its eastern vicinity.In winter,the rainfall variation in South China has a close linkage with the evaporation variation in a belt area covering the eastern Arabian Sea,the Bay of Bengal,the southeastern periphery of the Plateau,the southern part of South China Sea and the central part of Indonesia.
文摘Short path distillation (SPD) is a kind of high vacuum distillation method, which is suitable for the separation of high boiling, heat sensitivity and viscidity products.In this paper,through measuring the phase-averaged velocity distributions with a conditional sampling method of the particle imaging velocimetry (PIV), the liquid flow field that affects the heat and mass transfer of evaporating thin-film in an SPD evaporator is investigated.Measured results show that the flow velocities decrease rapidly apart from the wiper at different wiper velocities, the maximum velocity appears before wipers, and the quicker the wiping, the larger the flow velocity. Meanwhile, the evaluation of numerical calculations is carried out.The measured velocity distributions indicate clearly the effect of the wiper both on the flow field along its moving direction and on the vortices behind the wiper.Simulation data show that the performance of liquid flow field on the heating surface not only agrees with the experimental results well,but also can give further more information, such as the distribution of turbulent kinetic energy.In this study,turbulent kinetic energy mainly distributes before wipers and laminar flow appears far away from the wipers.
基金Acknowledgments： The study is one of branches of a key project of Chinese National Programs for Foundation Research and Development, thanks for the supporting from the National Nature Science Foundation. The new method to measure thickness of wager film has applied an utility model patent in China （No. 200620098211.4）.
文摘Thickness of falling water film out of tubes is one of critical factors of heat transfer of evaporative air cooler. A new method of resistance measurement was developed to measure thickness of the film. When the resistance probe on the tip of micrometer touches the surface and bottom of the film, two corresponding sudden reductions of resistance occurs, and the difference of two graduations on the micrometer displays the thickness of the film. The film thickness of eleven angles was measured in five kinds of water flows and results varies from 0.8933mm to 1.7233 mm. Mean thickness and mean heat transfer coefficient of the film out of the tube was calculated.
