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五虎壳聚糖凝胶剂的制备与临床应用 被引量:5
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作者 王志朝 孙卓琳 +1 位作者 刘祖雄 余敦良 《中国药业》 CAS 2006年第2期48-49,共2页
目的:研究五虎壳聚糖凝胶剂的制备方法与临床应用。方法:含挥发油的药材采用蒸馏法提取挥发油,其他药材采用水煎煮法提取, 以壳聚糖为凝胶材料制备五虎壳聚糖凝胶剂;用薄层层析法进行鉴别,用高效液相色谱法测定含量。结果:该凝胶剂制备... 目的:研究五虎壳聚糖凝胶剂的制备方法与临床应用。方法:含挥发油的药材采用蒸馏法提取挥发油,其他药材采用水煎煮法提取, 以壳聚糖为凝胶材料制备五虎壳聚糖凝胶剂;用薄层层析法进行鉴别,用高效液相色谱法测定含量。结果:该凝胶剂制备工艺简单,质量控制方法可行,临床疗效可靠。结论:该制剂符合《中国药典》凝胶剂项下有关规定。 展开更多
关键词 壳聚糖凝 制备 临床应用
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虎黄烧伤凝胶剂的制备及质量控制 被引量:3
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作者 杨君 张洪 魏丹芸 《中国医药导报》 CAS 2015年第6期82-85,114,共5页
目的确定虎黄烧伤凝胶剂的制备工艺并建立其质量控制的方法。方法通过单因素实验以凝胶剂的成型性和稳定性为考察指标,筛选出最适宜的载药基质。采用高效液相色谱法同时测定该制剂中虎杖苷和盐酸小檗碱的含量。结果虎黄烧伤凝胶剂的最... 目的确定虎黄烧伤凝胶剂的制备工艺并建立其质量控制的方法。方法通过单因素实验以凝胶剂的成型性和稳定性为考察指标,筛选出最适宜的载药基质。采用高效液相色谱法同时测定该制剂中虎杖苷和盐酸小檗碱的含量。结果虎黄烧伤凝胶剂的最佳基质材料为2.5%的羟丙甲基纤维素;虎杖苷质量浓度与峰面积的线性回归方程为Y=79415X-444889(r=0.9994),线性范围为15.6-78.0μg/mL;盐酸小檗碱质量浓度与峰面积的线性回归方程为Y=65 576X-583 154(r=0.9996),线性范围为34.75-173.75μg/mL;平均加样回收率分别为99.34%、99.64%(n=6)。结论本研究制剂制备工艺简单,性质稳定,含量测定方法准确可靠,重现性好,促进了该制剂在临床上的应用。 展开更多
关键词 黄烧伤凝 制备 质量控制 高效液相色谱法
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农药安全使用技术
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作者 默涛 陈树欣 +1 位作者 张少军 王莉 《现代农村科技》 1992年第7期16-17,共2页
关键词 农药安全使用 小菜蛾 施药量 菜螟 细菌性角斑病 虎胶 瑞毒霉 可湿性粉剂 白粉虱 桃蚜
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陶业富西洋
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作者 吴永春 苏卫军 《老区建设》 1992年第8期14-15,共2页
西洋,雄踞在浙南山区的泰顺县老鹰岩山脚下。西洋乡公路两旁,一条条烟囱耸立云天,一幢幢楼房鳞次栉比,一块块晶莹洁白、五光十色的白面砖、彩釉砖、墙地砖从这里运往四面八方。
关键词 墙地砖 老鹰岩 乡公路 尤德 浙南山区 虎胶 陶瓷产品 房屋外墙 流钢砖 外贸部门
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五虎凝胶贴膏质量标准研究 被引量:2
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作者 陈敏 邓萌萌 +1 位作者 伍蕊嗣 潘晓鹃 《中国现代应用药学》 CAS CSCD 北大核心 2021年第20期2530-2536,共7页
目的建立五虎凝胶贴膏的质量标准。方法采用薄层色谱法(TLC)对处方中白芷、当归、防风、红花、制天南星进行定性鉴别;采用HPLC同时测定处方中羟基红花黄色素A、阿魏酸、升麻素苷、5-O-甲基维斯阿米醇苷、欧前胡素、异欧前胡素的含量,色... 目的建立五虎凝胶贴膏的质量标准。方法采用薄层色谱法(TLC)对处方中白芷、当归、防风、红花、制天南星进行定性鉴别;采用HPLC同时测定处方中羟基红花黄色素A、阿魏酸、升麻素苷、5-O-甲基维斯阿米醇苷、欧前胡素、异欧前胡素的含量,色谱柱为Agilent Eclipse Plus C18(250 mm×4.6 mm,5μm),流动相甲醇-0.025%磷酸,梯度洗脱,流速为1.0 mL·min^(-1);柱温28℃;检测波长403,300,254 nm。结果处方中所有药味薄层斑点清晰,分离度好,阴性无干扰;6种化合物在各自的范围内线性关系良好(r≥0.9995),平均加样回收率96.30%~100.56%,RSD为1.06%~1.65%。结论建立的TLC鉴别方法专属性强、分离度好;HPLC测定方法准确稳定、重复性好,可用于五虎凝胶贴膏的质量控制。 展开更多
关键词 贴膏 薄层色谱法 高效液相色谱法 质量标准
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PVC gel bio-inspired adhesives with variable modulus and its application in a gripper 被引量:2
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作者 ZHANG Hao HE Qing-song +3 位作者 TIAN Cheng-bo WU Yu-wei ZHAO Ze-fang YU Min 《Journal of Central South University》 SCIE EI CAS CSCD 2022年第6期1778-1787,共10页
Inspired by the microstructure of gecko’s toe,two kinds of polyvinyl chloride(PVC)gels with different modulus were poured on a silicon mold with micropillars,and then a bio-inspired adhesive with variable modulus was... Inspired by the microstructure of gecko’s toe,two kinds of polyvinyl chloride(PVC)gels with different modulus were poured on a silicon mold with micropillars,and then a bio-inspired adhesive with variable modulus was manufactured in this study.The adhesions of variable modulus and fixed modulus bio-inspired adhesives were tested,respectively,on a smooth glass and a printed circuit board(PCB)with different surface structures.The results show that PVC gel bio-inspired adhesives with variable modulus have many advantages compared with the fixed modulus bioinspired adhesives.The adhesion of variable modulus bio-inspired adhesives on the rough PCB surface increased by 2−5 times,and due to the use of variable modulus of PVC gel,the surface micropillars can maintain high aspect ratio and flexible tips at the same time.Moreover,the use of PVC gel makes it easier to demold during the bio-inspired adhesives preparation.An adhesion-desorption device was made according to the movement of the gecko toes,and the PCB was successfully grasped. 展开更多
关键词 bio-inspired adhesives GECKO PVC gel variable modulus
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Development, manufacture and application of Beta-Cypermethrin aqueous capsule suspension
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作者 郎子建 苏元吉 +1 位作者 王志英 陈立平 《Journal of Forestry Research》 SCIE CAS CSCD 2004年第3期218-222,共5页
The optimal formula of Beta-Cypermethrin aqueous capsule suspension was screened out through the experiment, preparation and manufacture of basic formulas, which has no sedimentation, suspended drops of oil, peels and... The optimal formula of Beta-Cypermethrin aqueous capsule suspension was screened out through the experiment, preparation and manufacture of basic formulas, which has no sedimentation, suspended drops of oil, peels and agglomerating and the diameter of capsule is in range of 10-30 靘, conformed to the technical requirement. The aftereffect of the 3.3% Beta-Cypermethrin aqueous capsule suspension which was manufactured according to the optimal formula was up more than 25 days. The experiments on controlling the larvae of Dendrolinmus superans Butler and the adults of Xylotrechus rusticus L were carried out with different concentrations of this chemical. The death rate reached 80% when 250 times solution of the chemical was sprayed on stem to control the larvae of D. superans. For control of the adults of X. rusticus, 200, 400 and 600 times solution of the chemical were applied and their control effects (death rate) reached 85.23%, 74.21% and 66.59% respec-tively. Two kinds of solution (200 times and 300 times) of the chemical were used to control the larvae of D. superans in large area, and the control effect for both concentrations was over 90%. 展开更多
关键词 Aqueous capsule suspension Cypermethrin-capsule Pest control Dendrolinmus superans Xylotrechus rusticus.
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