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定向凝固镍基单晶高温合金螺旋选晶过程显微组织与晶体的生长 被引量:3
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作者 徐莽 张相龙 +4 位作者 耿小奇 刘国怀 王晔 王昭东 郭景杰 《特种铸造及有色合金》 CAS 北大核心 2021年第7期831-836,共6页
采用选晶法制备DD4单晶高温合金试棒,研究引晶段和选晶段显微组织演变及晶体竞争生长过程。结果表明,随着引晶段高度增加,一次枝晶间距增加,晶粒密度显著降低,<001>织构增强。引晶段高度在20mm时,初始晶粒取向偏转角均小于10... 采用选晶法制备DD4单晶高温合金试棒,研究引晶段和选晶段显微组织演变及晶体竞争生长过程。结果表明,随着引晶段高度增加,一次枝晶间距增加,晶粒密度显著降低,<001>织构增强。引晶段高度在20mm时,初始晶粒取向偏转角均小于10°,且最终约有35个明显尺寸且取向良好的晶粒进入螺旋段。位于螺旋通道内侧的晶粒,在螺旋选晶过程中最容易被选出。在约1/3螺旋高度处实现了单晶的筛选过程,制备出<001>生长方向与铸件轴向约8.9°偏差角的单晶体。 展开更多
关键词 定向凝固 镍基单高温合金 螺旋选晶 竞争生长 粒取向
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单晶高温合金DD6不同状态下的元素分布与力学行为
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作者 蒋睿哲 顾玉丽 何玉怀 《材料导报》 EI CAS CSCD 北大核心 2017年第12期93-97,共5页
选择3mm/min和8mm/min两种抽拉速率通过螺旋选晶法制备[001]方向的DD6单晶高温合金,测试合金枝晶间与枝晶干的元素分布,研究了两种工艺合金的持久性能和断裂特征;利用EPMA电子探针测试了3mm/min抽拉速率DD6合金经0.1%、0.2%、0.5%蠕变... 选择3mm/min和8mm/min两种抽拉速率通过螺旋选晶法制备[001]方向的DD6单晶高温合金,测试合金枝晶间与枝晶干的元素分布,研究了两种工艺合金的持久性能和断裂特征;利用EPMA电子探针测试了3mm/min抽拉速率DD6合金经0.1%、0.2%、0.5%蠕变应变后枝晶间与枝晶干的元素分布,并通过纳米压痕仪测试了枝晶间与枝晶干的弹性模量和硬度。结果表明,抽拉速率较小时DD6合金枝晶组织更粗大,元素偏析程度较大,抽拉速率对合金持久寿命的影响不大;随着蠕变应变的增加,合金枝晶间与枝晶干弹性模量和硬度的差值逐渐增大,这与合金元素的再分布紧密相关,特别是与难熔元素Ta、Hf、Mo和Nb随着蠕变应变的变化而发生再分布有关。 展开更多
关键词 镍基单高温合金 元素分布 抽拉速率 蠕变 持久 螺旋选晶
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Influence of spiral crystal selector on crystal orientation of single crystal superalloy 被引量:3
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作者 张如林 陈丽娜 +3 位作者 李重河 王宁 鲁雄刚 任忠鸣 《Transactions of Nonferrous Metals Society of China》 SCIE EI CAS CSCD 2012年第5期1092-1095,共4页
To increase efficiency and improve performance, reducing cost and emissions, advanced single crystal Ni-based superalloys are required in aerospace propulsion and power generating gas turbines. With the development of... To increase efficiency and improve performance, reducing cost and emissions, advanced single crystal Ni-based superalloys are required in aerospace propulsion and power generating gas turbines. With the development of alloy, significant improvements in casting techniques have been achieved by introducing the directionally solidified (DS) casting process followed by single crystal (SX) technique. The deviation of preferred orientation of single crystal superalloys is one of the most important defects in casting. In directional solidification equipment with high temperature gradient, single crystal specimens of DZ417G alloy were prepared successfully by the modified Bridgeman method with spiral grain selector. The orientation was investigated by means of X-ray diffraction (XRD) and electron backscattered diffraction (EBSD).The results show that the crystal selector with a smaller angle can effectively reduce the deviation of preferred orientation. 展开更多
关键词 nickel-base superalloy directional solidification single crystal superalloy crystal orientation spiral grain selector
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Effects of directional solidification parameters and crystal selector on microstructure of single crystal of Ni-base superalloys 被引量:5
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作者 LI Chong-he WEI Chao +3 位作者 ZHANG Ru-lin WANG Hong-bin REN Zhong-ming LU Xiong-gang 《Journal of Central South University》 SCIE EI CAS CSCD 2018年第1期1-8,共8页
The single crystal of nickel-base super alloy is widely used for making turbine blades.The microstructure of the alloy,especially the deviation of preferred orientation of single crystal,possesses the most important e... The single crystal of nickel-base super alloy is widely used for making turbine blades.The microstructure of the alloy,especially the deviation of preferred orientation of single crystal,possesses the most important effects on the mechanical properties of the blades.In this study,the single crystal ingot and blade of DZ417G alloy are prepared by means of the spiral crystal selector as well as the directional solidification method,and the effect of the parameters(i.e.,the shape of samples,the withdrawal rate)and the structure of the spiral crystal selector on the formation of single crystal and the crystal orientation are investigated.This method can prepare not only the single crystal ingot with simple shape but also the single crystal blades with the complex shape,the simple with rod-shape can form the single crystal easily with a relatively fast withdrawal rate,but the blade with complex shape requires much slower withdrawal rate to form single crystal.The length of the crystal selector almost has no effect on the crystal orientation.However,the angle of selector plays an obvious role on the orientation;the selector with a smaller angle can effectively reduce the deviation of preferred orientation;the appropriate angle of selector to obtain optimal orientation is found to be around30°and the deviation of preferred orientation is about30°for this selector. 展开更多
关键词 DZ417G alloy high rapid solidification crystal orientation single crystal superalloy spiral grain selector
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