Tensile stress-strain curves of five metallic alloys,i.e.,SKH51,STS316L,Ti-6Al-4V,Al6061and Inconel600were analyzed to investigate the working hardening behavior.The constitutive parameters of three constitutive equat...Tensile stress-strain curves of five metallic alloys,i.e.,SKH51,STS316L,Ti-6Al-4V,Al6061and Inconel600were analyzed to investigate the working hardening behavior.The constitutive parameters of three constitutive equations,i.e.,the Hollomon,Swift and Voce equations,were compared by using different methods.A new working hardening parameter was proposed to characterize the working hardening behavior in different deformation stages.It is found that Voce equation is suitable to describe stress-strain curves in large strain region.Meanwhile,the predicting accuracy of ultimate tensile strength by Voce equation is the best.The working hardening behavior of SKH51is different from the other four metallic alloys.展开更多
The aim of this paper is to analyze the change in the active structure of lignite during the process of lowtemperature oxidation by constructing a molecular structure model for lignite. Using quantum computation combi...The aim of this paper is to analyze the change in the active structure of lignite during the process of lowtemperature oxidation by constructing a molecular structure model for lignite. Using quantum computation combined with experimental results of proximate analysis, ultimate analysis, Fourier transform infrared spectroscopy(FTIR) and X-ray photoelectron spectroscopy(XPS), a structural model for the large molecular structure was constructed. By analyzing the bond lengths in the model molecule, the evolution law for the active structure of lignite was predicted for the process of low-temperature oxidation. In low-temperature oxidation,alkanes and hydroxyls are the primary active structures observed in lignite, though ether may also react. These active functional groups react with oxygen to release heat, thereby speeding up the reaction between coal and oxygen. Finally, the content of various functional groups in the process of lignite low-temperature oxidation was analyzed by infrared analysis, and the accuracy of the model was verified.展开更多
The surface of ZrO2 nanoparticles was modified by styrene coupling grafting method to improve the dispersion and interaction of the nanoparticles with the epoxy coating in which the modified ZrO2 nanoparticles were us...The surface of ZrO2 nanoparticles was modified by styrene coupling grafting method to improve the dispersion and interaction of the nanoparticles with the epoxy coating in which the modified ZrO2 nanoparticles were used as an additive. The grafting performance and microstructure of the nano- ZrO2/epoxy coating were analyzed by Fourier transformation infrared spectroscopy, X-ray diffraction, and scanning electron microscopy. The corrosion behavior of the nano-ZrO2/epoxy coating on mild steel was evaluated in neutral 3.5 wt% NaC1 solution using electrochemical impedance spectroscopy （EIS）. Both the coating capacitance and coating resistance fitted by the equivalent circuit from EIS were used to evaluate the protective performance of the coating towards the mild steel. The results show a superior stability and efficient corrosion protection by the modified ZrO2 nanoparticles. The epoxy coating containing 2 wt% modified ZrO2 nanoparticles exhibited the best corrosion performance among all the coating specimens. This research may provide an insight into the protection of mild steel using modified epoxy coatings.展开更多
The effect of temperature on the functional groups transition of N-methyl-N-nitroso-p-toluenesulfonamide （Diazald） and thermal decomposition were investigated by Fourier Transform Infrared Spectroscopy （FT-IR） and...The effect of temperature on the functional groups transition of N-methyl-N-nitroso-p-toluenesulfonamide （Diazald） and thermal decomposition were investigated by Fourier Transform Infrared Spectroscopy （FT-IR） and Differential Scanning Calorimeter （DSC）. The results showed that the functional groups transition of Diazald was temperature dependent, and thermal decomposition of Diazald was accelerated above 47.7℃. The HPLC-ESI-MS method was used for Diazald analysis, which indicated the strong hydrogen bonding between Diazald and water and instability of the NO group.展开更多
A set of discrete points obtained from audit records on a behavior session is processed with Fourier transform. The criterion of selecting Fourier transform coefficients is introduced, and is used to find a unified va...A set of discrete points obtained from audit records on a behavior session is processed with Fourier transform. The criterion of selecting Fourier transform coefficients is introduced, and is used to find a unified value from the set of coefficients. This unified value is compared with a threshold to determine whether the session is abnormal. Finally simple test results are reported.展开更多
It is of considerable importance to investigate the influence of weathering on the degradation processes of heat-treated wood. Kiln-dried （untreated）jack pine （Pinus banksiana） and jack pine heat-treated at three ...It is of considerable importance to investigate the influence of weathering on the degradation processes of heat-treated wood. Kiln-dried （untreated）jack pine （Pinus banksiana） and jack pine heat-treated at three different temperatures （190 ℃, 200 ℃, and 210 ℃） were exposed to artificial weathering for different periods in order to understand the degradation processes due to weathering. Before and after exposure, their color and wettability by water were determined. Structural changes and chemical modifications at exposed surfaces were also investigated using SEM （scanning electron spectroscopy）, FTIR （Fourier transforms infrared spectroscopy）, and XPS （X-ray photoelectron spectroscopy）. The results revealed that the photo-degradation of lignin and the presence of extractives play important roles in color change and wetting behavior of heat-treated wood surfaces during weathering. The structural changes also influence the wettability. The effects of weathering for woods heat-treated under different conditions were similar, but different from those for untreated wood.展开更多
Otoliths are biogenic carbonate minerals whose microstructure and microchemistry have been used for age determination, stock identification, life history and environmental tracing. Using X-ray diffraction （XRD） and ...Otoliths are biogenic carbonate minerals whose microstructure and microchemistry have been used for age determination, stock identification, life history and environmental tracing. Using X-ray diffraction （XRD） and Fourier transform infrared （FTIR） spectroscopy, we have determined the mineral types and crystalline characteristics of three pairs of otoliths from naked carp Gymnocypris przewalskii, the predominant fish in Lake Qinghai. The results indicate that the mineral of both lapillus and sagitta of the naked carp is aragonite, and that of asteriscus is vaterite. The aragonite of lapillus has prefect crystallization. Given the shape of lapillus and the sensitivity of its aragonite to water chemistry, lapillus was used to analyze temporal Sr/Ca ratios along the maximal growth axis by an electron probe microanalyzer （EPMA）. Consistent variations of Sr/Ca ratios with a range of 1.0x10-3-5.0~10-3 on the long and short radii indicate that Sr/Ca ratios of lapillus potentially respond to the chemical compositions of the host waters during the period of the naked carp＇s growth and migration. Discontinuous （dark） zones of lapillus were formed during fall and winter when the naked carp grows slowly in Lake Qinghai, resulting in similar low Sr/Ca ratios to lake water, whereas incremental zones with higher St/Ca ratios respond to its migratory river waters during spring and summer. Various Sr/Ca ratios of incremental zones suggest that the migratory pattern of the naked carp may be much more flexible, rather than in a single river. Therefore, high-resolution otolith microchemistry of the naked carp can be used to trace its migratory behavior, which is of significance for determining its migratory pattern and life history of this precious species inhabiting the Tibetan Plateau.展开更多
The integrable nonlocal Lakshmanan–Porsezian–Daniel(LPD) equation which has the higher-order terms(dispersions and nonlinear effects) is first introduced. We demonstrate the integrability of the nonlocal LPD equatio...The integrable nonlocal Lakshmanan–Porsezian–Daniel(LPD) equation which has the higher-order terms(dispersions and nonlinear effects) is first introduced. We demonstrate the integrability of the nonlocal LPD equation,provide its Lax pair, and present its rational soliton solutions and self-potential function by using the degenerate Darboux transformation. From the numerical plots of solutions, the compression effects of the real refractive index profile and the gain-or-loss distribution produced by δ are discussed.展开更多
Graph transformation systems have become a general formal modeling language to describe many models in software development process.Behavioral modeling of dynamic systems and model-to-model transformations are only a ...Graph transformation systems have become a general formal modeling language to describe many models in software development process.Behavioral modeling of dynamic systems and model-to-model transformations are only a few examples in which graphs have been used to software development.But even the perfect graph transformation system must be equipped with automated analysis capabilities to let users understand whether such a formal specification fulfills their requirements.In this paper,we present a new solution to verify graph transformation systems using the Bogor model checker.The attributed graph grammars(AGG)-like graph transformation systems are translated to Bandera intermediate representation(BIR),the input language of Bogor,and Bogor verifies the model against some interesting properties defined by combining linear temporal logic(LTL) and special-purpose graph rules.Experimental results are encouraging,showing that in most cases our solution improves existing approaches in terms of both performance and expressiveness.展开更多
This paper is concerned with oscillatory and asymptotic behavior of solutions of a class of second order nonlinear functional differential equations.By using the generalized Riccati transformation and the integral ave...This paper is concerned with oscillatory and asymptotic behavior of solutions of a class of second order nonlinear functional differential equations.By using the generalized Riccati transformation and the integral averaging technique,new oscillation criteria and asymptotic behavior are obtained for all solutions of the equation.Our results generalize and improve some known theorems.展开更多
基金Project(51275414)supported by the National Natural Science Foundation of ChinaProject(3102015BJ(Ⅱ)ZS007)supported by the Fundamental Research Funds for the Central Universities,ChinaProject(130-QP-2015)supported by the Research Fund of the State Key Laboratory of Solidification Processing(NWPU),China
文摘Tensile stress-strain curves of five metallic alloys,i.e.,SKH51,STS316L,Ti-6Al-4V,Al6061and Inconel600were analyzed to investigate the working hardening behavior.The constitutive parameters of three constitutive equations,i.e.,the Hollomon,Swift and Voce equations,were compared by using different methods.A new working hardening parameter was proposed to characterize the working hardening behavior in different deformation stages.It is found that Voce equation is suitable to describe stress-strain curves in large strain region.Meanwhile,the predicting accuracy of ultimate tensile strength by Voce equation is the best.The working hardening behavior of SKH51is different from the other four metallic alloys.
基金Supported by the Fundamental Research Funds for the Central Universities(2017XKQY066)
文摘The aim of this paper is to analyze the change in the active structure of lignite during the process of lowtemperature oxidation by constructing a molecular structure model for lignite. Using quantum computation combined with experimental results of proximate analysis, ultimate analysis, Fourier transform infrared spectroscopy(FTIR) and X-ray photoelectron spectroscopy(XPS), a structural model for the large molecular structure was constructed. By analyzing the bond lengths in the model molecule, the evolution law for the active structure of lignite was predicted for the process of low-temperature oxidation. In low-temperature oxidation,alkanes and hydroxyls are the primary active structures observed in lignite, though ether may also react. These active functional groups react with oxygen to release heat, thereby speeding up the reaction between coal and oxygen. Finally, the content of various functional groups in the process of lignite low-temperature oxidation was analyzed by infrared analysis, and the accuracy of the model was verified.
基金Supported by the National Department Public Benefit Research Foundation(No.201005028)the National Key Technology Research and Development Program during the Twelfth Five-Year Plan Period of China(No.2012BAB15B01)
文摘The surface of ZrO2 nanoparticles was modified by styrene coupling grafting method to improve the dispersion and interaction of the nanoparticles with the epoxy coating in which the modified ZrO2 nanoparticles were used as an additive. The grafting performance and microstructure of the nano- ZrO2/epoxy coating were analyzed by Fourier transformation infrared spectroscopy, X-ray diffraction, and scanning electron microscopy. The corrosion behavior of the nano-ZrO2/epoxy coating on mild steel was evaluated in neutral 3.5 wt% NaC1 solution using electrochemical impedance spectroscopy （EIS）. Both the coating capacitance and coating resistance fitted by the equivalent circuit from EIS were used to evaluate the protective performance of the coating towards the mild steel. The results show a superior stability and efficient corrosion protection by the modified ZrO2 nanoparticles. The epoxy coating containing 2 wt% modified ZrO2 nanoparticles exhibited the best corrosion performance among all the coating specimens. This research may provide an insight into the protection of mild steel using modified epoxy coatings.
文摘The effect of temperature on the functional groups transition of N-methyl-N-nitroso-p-toluenesulfonamide （Diazald） and thermal decomposition were investigated by Fourier Transform Infrared Spectroscopy （FT-IR） and Differential Scanning Calorimeter （DSC）. The results showed that the functional groups transition of Diazald was temperature dependent, and thermal decomposition of Diazald was accelerated above 47.7℃. The HPLC-ESI-MS method was used for Diazald analysis, which indicated the strong hydrogen bonding between Diazald and water and instability of the NO group.
基金Supported by the Tianjin Natural Science Fund (003700211) and 863 High Technology Plan (2002AA142010)
文摘A set of discrete points obtained from audit records on a behavior session is processed with Fourier transform. The criterion of selecting Fourier transform coefficients is introduced, and is used to find a unified value from the set of coefficients. This unified value is compared with a threshold to determine whether the session is abnormal. Finally simple test results are reported.
文摘It is of considerable importance to investigate the influence of weathering on the degradation processes of heat-treated wood. Kiln-dried （untreated）jack pine （Pinus banksiana） and jack pine heat-treated at three different temperatures （190 ℃, 200 ℃, and 210 ℃） were exposed to artificial weathering for different periods in order to understand the degradation processes due to weathering. Before and after exposure, their color and wettability by water were determined. Structural changes and chemical modifications at exposed surfaces were also investigated using SEM （scanning electron spectroscopy）, FTIR （Fourier transforms infrared spectroscopy）, and XPS （X-ray photoelectron spectroscopy）. The results revealed that the photo-degradation of lignin and the presence of extractives play important roles in color change and wetting behavior of heat-treated wood surfaces during weathering. The structural changes also influence the wettability. The effects of weathering for woods heat-treated under different conditions were similar, but different from those for untreated wood.
基金supported by National Basic Research Program of China (Grant No. 2010CB833400)National Natural Science Foundation of China (Grant No. 40873082)
文摘Otoliths are biogenic carbonate minerals whose microstructure and microchemistry have been used for age determination, stock identification, life history and environmental tracing. Using X-ray diffraction （XRD） and Fourier transform infrared （FTIR） spectroscopy, we have determined the mineral types and crystalline characteristics of three pairs of otoliths from naked carp Gymnocypris przewalskii, the predominant fish in Lake Qinghai. The results indicate that the mineral of both lapillus and sagitta of the naked carp is aragonite, and that of asteriscus is vaterite. The aragonite of lapillus has prefect crystallization. Given the shape of lapillus and the sensitivity of its aragonite to water chemistry, lapillus was used to analyze temporal Sr/Ca ratios along the maximal growth axis by an electron probe microanalyzer （EPMA）. Consistent variations of Sr/Ca ratios with a range of 1.0x10-3-5.0~10-3 on the long and short radii indicate that Sr/Ca ratios of lapillus potentially respond to the chemical compositions of the host waters during the period of the naked carp＇s growth and migration. Discontinuous （dark） zones of lapillus were formed during fall and winter when the naked carp grows slowly in Lake Qinghai, resulting in similar low Sr/Ca ratios to lake water, whereas incremental zones with higher St/Ca ratios respond to its migratory river waters during spring and summer. Various Sr/Ca ratios of incremental zones suggest that the migratory pattern of the naked carp may be much more flexible, rather than in a single river. Therefore, high-resolution otolith microchemistry of the naked carp can be used to trace its migratory behavior, which is of significance for determining its migratory pattern and life history of this precious species inhabiting the Tibetan Plateau.
基金Supported by the National Natural Science Foundation of China under Grant No.11271210the K.C.Wong Magna Fund in Ningbo University
文摘The integrable nonlocal Lakshmanan–Porsezian–Daniel(LPD) equation which has the higher-order terms(dispersions and nonlinear effects) is first introduced. We demonstrate the integrability of the nonlocal LPD equation,provide its Lax pair, and present its rational soliton solutions and self-potential function by using the degenerate Darboux transformation. From the numerical plots of solutions, the compression effects of the real refractive index profile and the gain-or-loss distribution produced by δ are discussed.
文摘Graph transformation systems have become a general formal modeling language to describe many models in software development process.Behavioral modeling of dynamic systems and model-to-model transformations are only a few examples in which graphs have been used to software development.But even the perfect graph transformation system must be equipped with automated analysis capabilities to let users understand whether such a formal specification fulfills their requirements.In this paper,we present a new solution to verify graph transformation systems using the Bogor model checker.The attributed graph grammars(AGG)-like graph transformation systems are translated to Bandera intermediate representation(BIR),the input language of Bogor,and Bogor verifies the model against some interesting properties defined by combining linear temporal logic(LTL) and special-purpose graph rules.Experimental results are encouraging,showing that in most cases our solution improves existing approaches in terms of both performance and expressiveness.
基金Supported by the Natural Science Foundation of Shandong Province of China under Grant Nos. ZR2010AM031 and ZR2011AL001the Development Program in Science and Technology of Shandong Province of China under Grant No. 2010GWZ20401
文摘This paper is concerned with oscillatory and asymptotic behavior of solutions of a class of second order nonlinear functional differential equations.By using the generalized Riccati transformation and the integral averaging technique,new oscillation criteria and asymptotic behavior are obtained for all solutions of the equation.Our results generalize and improve some known theorems.
