O484.1 95010481GaAs上热壁外延Cd<sub>8.96</sub>Zn<sub>0.04</sub>Te薄膜=Growth ofCd<sub>0.96</sub>Zn<sub>0.04</sub>Te films on GaAs substrates byhot wall epitaxy[刊,中]/...O484.1 95010481GaAs上热壁外延Cd<sub>8.96</sub>Zn<sub>0.04</sub>Te薄膜=Growth ofCd<sub>0.96</sub>Zn<sub>0.04</sub>Te films on GaAs substrates byhot wall epitaxy[刊,中]/陶长远,刘达清（南开大学物理系.天津）//红外与激光技术.—1994,（3）.—15—17首次报道用热壁外延技术在（100）GaAs衬底上生长出Cd<sub>0.96</sub>Zn<sub>0.04</sub>Te（111）薄膜,结果表明,薄膜在15—20μm厚时X射线双晶衍射回摆曲线半高宽在100弧秒以下,其位错腐蚀坑密度等于甚至小于10<sup>3</sup>cm<sup>-2</sup>薄膜组分,层厚均匀,表面光亮如镜。展开更多
FeCrAI （Ce） stainless steel was functionalized by a conversion treatment in order to allow alumina by diffusion coatings with strong interfacial bonding. The very porous conversion coating produced in a pack alumini...FeCrAI （Ce） stainless steel was functionalized by a conversion treatment in order to allow alumina by diffusion coatings with strong interfacial bonding. The very porous conversion coating produced in a pack aluminization technique had excellent adhesion and was conductive enough to permit conditions favorable for the precipitation of alumina oxyhydroxide during aluminum diffusion coatings. In this work, the bed was prepared as a mixture of A1, NH4C1 and A1203. In the high-activity bed were heat-treated at 1,173 K in an atmosphere made up of team with subsequent air-cooling. The effect of the bed content on the coating was examined. With the high-activity, the desired Fe2Al5 was formed as the outermost coating layer. The coating presented chemical composition gradients suitable for strong adhesion. The improvement of the thermal oxidation behaviour was studied at 1,373 K. Two different aqueous environments, which are （1） NaC1 and （2） H2SO4, are employed for using the technique of potentiodynamic polarization curve. The obtained experimental electrochemical parameters （Ecorr, Jcorr etc,） were used to compare the corrosion resistance of the tested steel state complemented by MEB （electronic scanning microscopy） in combination with dispersive analysis X in energy （EDS） or X ray diffraction indicated that the elements concentration maximum was located in the vicinity of the interface especially in the FeCrAI （Ce） coated by spherical A1203 powder. These results an discussed in terms of an addition effect on the development of the microstructure of oxide films.展开更多
Deferasirox is the first-line drug for iron overload due to thalassemia in adults and pediatric patients. It is classified as a type II compound in the Biopharmaceutics Classification System, and thus the particle siz...Deferasirox is the first-line drug for iron overload due to thalassemia in adults and pediatric patients. It is classified as a type II compound in the Biopharmaceutics Classification System, and thus the particle size of its active pharmaceutical ingredient(API) should be strictly controlled during the manufacturing process. In the present study, laser diffraction was adopted to measure the particle size distribution of deferasirox API. We also developed and validated an accurate and convenient method by investigating important optical parameters and sample dispersing conditions. The relative standard deviation values, namely, d(0.1), d(0.5), d(0.9), and d(4,3), measured via methodology validation and actual sample measurement were < 3%. The dissolution curves of several batches of dispersible tablets prepared using deferasirox with different particle sizes were compared in the four dissolved media to investigate the influence of particle size on drug dissolution in vitro. Results indicated that the particle size distribution of deferasirox API significantly affected the release of its dispersible tablet.展开更多
This paper studies the asymptotic behavior of the diffractive interaction of pulses with two linear phases of length ε ≤ 1 in 2 × 2 semilinear strictly hyperbolic system with constant coefficiients. By a formal...This paper studies the asymptotic behavior of the diffractive interaction of pulses with two linear phases of length ε ≤ 1 in 2 × 2 semilinear strictly hyperbolic system with constant coefficiients. By a formal analysis, it derives problems of profiles in the expansion of the pulse like solution with respect to the length s, and obtains that the leading profile satisfies a nonlinear Schrodinger type system. The problems of profiles are solved, and the formal expansion is justified. It is observed that there is interaction between two phases starting at the third order profiles.展开更多
文摘O484.1 95010481GaAs上热壁外延Cd<sub>8.96</sub>Zn<sub>0.04</sub>Te薄膜=Growth ofCd<sub>0.96</sub>Zn<sub>0.04</sub>Te films on GaAs substrates byhot wall epitaxy[刊,中]/陶长远,刘达清（南开大学物理系.天津）//红外与激光技术.—1994,（3）.—15—17首次报道用热壁外延技术在（100）GaAs衬底上生长出Cd<sub>0.96</sub>Zn<sub>0.04</sub>Te（111）薄膜,结果表明,薄膜在15—20μm厚时X射线双晶衍射回摆曲线半高宽在100弧秒以下,其位错腐蚀坑密度等于甚至小于10<sup>3</sup>cm<sup>-2</sup>薄膜组分,层厚均匀,表面光亮如镜。
文摘FeCrAI （Ce） stainless steel was functionalized by a conversion treatment in order to allow alumina by diffusion coatings with strong interfacial bonding. The very porous conversion coating produced in a pack aluminization technique had excellent adhesion and was conductive enough to permit conditions favorable for the precipitation of alumina oxyhydroxide during aluminum diffusion coatings. In this work, the bed was prepared as a mixture of A1, NH4C1 and A1203. In the high-activity bed were heat-treated at 1,173 K in an atmosphere made up of team with subsequent air-cooling. The effect of the bed content on the coating was examined. With the high-activity, the desired Fe2Al5 was formed as the outermost coating layer. The coating presented chemical composition gradients suitable for strong adhesion. The improvement of the thermal oxidation behaviour was studied at 1,373 K. Two different aqueous environments, which are （1） NaC1 and （2） H2SO4, are employed for using the technique of potentiodynamic polarization curve. The obtained experimental electrochemical parameters （Ecorr, Jcorr etc,） were used to compare the corrosion resistance of the tested steel state complemented by MEB （electronic scanning microscopy） in combination with dispersive analysis X in energy （EDS） or X ray diffraction indicated that the elements concentration maximum was located in the vicinity of the interface especially in the FeCrAI （Ce） coated by spherical A1203 powder. These results an discussed in terms of an addition effect on the development of the microstructure of oxide films.
基金CAMS Innovation Fund for Medical Sciences(CIFMS No.2016-I2M-3-010 and CIFMS No.2017-I2M-1-011)。
文摘Deferasirox is the first-line drug for iron overload due to thalassemia in adults and pediatric patients. It is classified as a type II compound in the Biopharmaceutics Classification System, and thus the particle size of its active pharmaceutical ingredient(API) should be strictly controlled during the manufacturing process. In the present study, laser diffraction was adopted to measure the particle size distribution of deferasirox API. We also developed and validated an accurate and convenient method by investigating important optical parameters and sample dispersing conditions. The relative standard deviation values, namely, d(0.1), d(0.5), d(0.9), and d(4,3), measured via methodology validation and actual sample measurement were < 3%. The dissolution curves of several batches of dispersible tablets prepared using deferasirox with different particle sizes were compared in the four dissolved media to investigate the influence of particle size on drug dissolution in vitro. Results indicated that the particle size distribution of deferasirox API significantly affected the release of its dispersible tablet.
基金the National Natural Science Foundation of China (No. 10131050)the Educational Ministry of China and the Shanghai Science and Technology Committee Foundation (No. 03QMH1407)
文摘This paper studies the asymptotic behavior of the diffractive interaction of pulses with two linear phases of length ε ≤ 1 in 2 × 2 semilinear strictly hyperbolic system with constant coefficiients. By a formal analysis, it derives problems of profiles in the expansion of the pulse like solution with respect to the length s, and obtains that the leading profile satisfies a nonlinear Schrodinger type system. The problems of profiles are solved, and the formal expansion is justified. It is observed that there is interaction between two phases starting at the third order profiles.
