Vertically orientated TiO2 nanotube array with diameters ranging from 60 up to 80 nm and length of 4 μm was grown on titanium by anodization.Crack initiation,propagation and saturation were studied using the substrat...Vertically orientated TiO2 nanotube array with diameters ranging from 60 up to 80 nm and length of 4 μm was grown on titanium by anodization.Crack initiation,propagation and saturation were studied using the substrate straining test.The results show that annealing obviously modifies the interfaces.With the increase of tensile strain,cracks in TiO2 nanotube films propagate rapidly and reach the saturation within a narrow strain gap.Interfacial shear strengths of TiO2 nanotube films without annealing,with 250 ℃ annealing and with 400 ℃ annealing can be estimated as 163.3,370.2 and 684.5 MPa,respectively.The critical energy release rates of TiO2 nanotube films are calculated as 49.6,102.6 and 392.7 J/m2,respectively.The fracture toughnesses of TiO2 nanotube films are estimated as 0.996,1.433 and 2.803 MPa-m1/2,respectively.The interfacial bonding mechanism of TiO2 nanotube film is chemical bonding.展开更多
Heterogeneous-structured Cu samples composed of coarse-grained(CG) and ultrafine-grained(UFG) domains with a transitional interface were fabricated by friction stir processing, in order to investigate the effect of in...Heterogeneous-structured Cu samples composed of coarse-grained(CG) and ultrafine-grained(UFG) domains with a transitional interface were fabricated by friction stir processing, in order to investigate the effect of interface constraint on the yielding and fracture behaviors. Tensile test revealed that the synergetic strengthening induced by elastic/plastic interaction between incompatible domains increases with increasing the area of constraint interface. The strain distribution near interface and the fracture morphology were characterized using digital image correlation technique and scanning electron microscopy, respectively. Fracture dimples preferentially formed at the interface, possibly due to extremely high triaxial stress and strain accumulation near the interface. Surprisingly, the CG domain was fractured by pure shear instead of the expected voids growth caused by tensile stress.展开更多
Rock blocks sliding along discontinuities can cause serious disasters,such as landslides,earthquakes,or rock bursts.The shear rate-dependent behavior is a typical time-dependent behavior of a rock discontinuity,and it...Rock blocks sliding along discontinuities can cause serious disasters,such as landslides,earthquakes,or rock bursts.The shear rate-dependent behavior is a typical time-dependent behavior of a rock discontinuity,and it is closely related to the stability of a rock block.To further study the shear rate-dependent behavior of rock discontinuities,shear tests with alternating shear rates(SASRs)were conducted on rock discontinuities with various surface morphologies.The dynamic evolution of the shear rate dependency was studied in detail based on the shear test results,and three stages were identified with respect to the shear stress and shear deformation states.The test results revealed that dynamic changes in shear stiffness and the energy storage abilities of the rock discontinuities occurred in relation to the shear rate-dependent behavior of crack growth,which increased with an increase in normal stress and/or the joint roughness coefficient.The stage of decreasing shear stiffness corresponded to a stage of noticeable shear rate-dependency,and the shear rate was found to have no influence on the initial crack stress.展开更多
The relationship among the surface fissure ratio, moisture content, seepage coefficient and deformation modulus of field unsaturated expansive soil in Nanning, Guangxi Province, China, was obtained by a direct or indi...The relationship among the surface fissure ratio, moisture content, seepage coefficient and deformation modulus of field unsaturated expansive soil in Nanning, Guangxi Province, China, was obtained by a direct or indirect method. Digital images of expansive soil of the surface fissure with different moisture contents were analyzed with the binarization statistic method. In addition, the fissure fractal dimension was computed with a self-compiled program. Combined with in situ seepage and loading plate tests, the relationship among the surface fissure ratio, moisture content, seepage coefficient and deformation modulus was initially established. The surface fissure ratio and moisture content show a linear relation, "y=-0.019 1x+1.028 5" for rufous expansive soil and "y=-0.07 1x+2.610 5" for grey expansive soil. Soil initial seepage coefficient and surface fissure ratio show a power function relation, "y=1× 10^-9exp(15.472x)" for rufous expansive soil and "y=5× 10^-7exp(4.209 6x)" for grey expansive soil. Grey expansive soil deformation modulus and surface fissure ratio show a power fimction relation of "y=3.935 7exp(0.993 6x)". Based on the binarization and fractal dimension methods, the results show that the surface fissure statistics can depict the fissure distribution in the view of two dimensions. And the evolvement behaviors of permeability and the deformation modulus can indirectly describe the developing state of the fissure. The analysis reflects that the engineering behaviors of unsaturated expansive soil are objectively influenced by fissure.展开更多
When stepped coal getting technology was applied to high seam mining working face, with field observations the following aspects of working face were analyzed based on the inherent conditions of extremely soft thick s...When stepped coal getting technology was applied to high seam mining working face, with field observations the following aspects of working face were analyzed based on the inherent conditions of extremely soft thick seam mined by Liangbei Mine, such as the brokenness and activity law of rock seam in the working face, the law of load-bearing of its supports, and the instability character of coal or rock in tip-to-face area. The following are the major laws. Pressure intensity of roof in high seam mining with extremely soft thick seam is stronger than one in slicing and sublevel-caving as a whole. But the greater crushing deformation of coal side makes pressure intensity of roof in the middle of working face be equivalent to one in sublevel-caving. In the middle of working face the roof brokenness has less dynamic load effect than roof brokenness in the two ends of working face. The brokenness instability of distinct pace of roof brings several load-bearings to supports. In condition of extremely soft thick seam, the ratio of resistance increment of supports in two ends of working face is obviously greater than that of supports in the middle. Most sloughing in coal side is triangular slop sloughing caused by shear slipping in high seam mining with extremely soft thick seam. Ultrahigh mining is the major reason for roof fall. Instability of coal or rock in tip-to-face area can be controlled effectively with the methods such as improving setting load of supports, mining along roof by reinforcing floor and protecting the immediate roof in time, and so on.展开更多
基金Project(50604017) supported by the National Natural Science Foundation of ChinaProject(20110946Z) supported by the State Key Laboratory of Powder Metallurgy,China
文摘Vertically orientated TiO2 nanotube array with diameters ranging from 60 up to 80 nm and length of 4 μm was grown on titanium by anodization.Crack initiation,propagation and saturation were studied using the substrate straining test.The results show that annealing obviously modifies the interfaces.With the increase of tensile strain,cracks in TiO2 nanotube films propagate rapidly and reach the saturation within a narrow strain gap.Interfacial shear strengths of TiO2 nanotube films without annealing,with 250 ℃ annealing and with 400 ℃ annealing can be estimated as 163.3,370.2 and 684.5 MPa,respectively.The critical energy release rates of TiO2 nanotube films are calculated as 49.6,102.6 and 392.7 J/m2,respectively.The fracture toughnesses of TiO2 nanotube films are estimated as 0.996,1.433 and 2.803 MPa-m1/2,respectively.The interfacial bonding mechanism of TiO2 nanotube film is chemical bonding.
基金Projects(11672195,51301092) supported by the National Natural Science Foundation of ChinaProject(2016JQ0047) supported by Sichuan Youth Science and Technology Foundation,China
文摘Heterogeneous-structured Cu samples composed of coarse-grained(CG) and ultrafine-grained(UFG) domains with a transitional interface were fabricated by friction stir processing, in order to investigate the effect of interface constraint on the yielding and fracture behaviors. Tensile test revealed that the synergetic strengthening induced by elastic/plastic interaction between incompatible domains increases with increasing the area of constraint interface. The strain distribution near interface and the fracture morphology were characterized using digital image correlation technique and scanning electron microscopy, respectively. Fracture dimples preferentially formed at the interface, possibly due to extremely high triaxial stress and strain accumulation near the interface. Surprisingly, the CG domain was fractured by pure shear instead of the expected voids growth caused by tensile stress.
基金Projects(42002266,51908288)supported by the National Natural Science Foundation of ChinaProject(2020M673654)supported by the Chinese Postdoctoral Science FoundationProject(2019K284)supported by Jiangsu Post-doctoral Research Funding Program,China。
文摘Rock blocks sliding along discontinuities can cause serious disasters,such as landslides,earthquakes,or rock bursts.The shear rate-dependent behavior is a typical time-dependent behavior of a rock discontinuity,and it is closely related to the stability of a rock block.To further study the shear rate-dependent behavior of rock discontinuities,shear tests with alternating shear rates(SASRs)were conducted on rock discontinuities with various surface morphologies.The dynamic evolution of the shear rate dependency was studied in detail based on the shear test results,and three stages were identified with respect to the shear stress and shear deformation states.The test results revealed that dynamic changes in shear stiffness and the energy storage abilities of the rock discontinuities occurred in relation to the shear rate-dependent behavior of crack growth,which increased with an increase in normal stress and/or the joint roughness coefficient.The stage of decreasing shear stiffness corresponded to a stage of noticeable shear rate-dependency,and the shear rate was found to have no influence on the initial crack stress.
基金Projects(41102229,51109208)supported by the National Natural Science Foundation of ChinaProject(2011CDB407)supported by Natural Science Foundation of Hubei Province,ChinaProject supported by Qing Lan Project of Jiangsu Province,China
文摘The relationship among the surface fissure ratio, moisture content, seepage coefficient and deformation modulus of field unsaturated expansive soil in Nanning, Guangxi Province, China, was obtained by a direct or indirect method. Digital images of expansive soil of the surface fissure with different moisture contents were analyzed with the binarization statistic method. In addition, the fissure fractal dimension was computed with a self-compiled program. Combined with in situ seepage and loading plate tests, the relationship among the surface fissure ratio, moisture content, seepage coefficient and deformation modulus was initially established. The surface fissure ratio and moisture content show a linear relation, "y=-0.019 1x+1.028 5" for rufous expansive soil and "y=-0.07 1x+2.610 5" for grey expansive soil. Soil initial seepage coefficient and surface fissure ratio show a power function relation, "y=1× 10^-9exp(15.472x)" for rufous expansive soil and "y=5× 10^-7exp(4.209 6x)" for grey expansive soil. Grey expansive soil deformation modulus and surface fissure ratio show a power fimction relation of "y=3.935 7exp(0.993 6x)". Based on the binarization and fractal dimension methods, the results show that the surface fissure statistics can depict the fissure distribution in the view of two dimensions. And the evolvement behaviors of permeability and the deformation modulus can indirectly describe the developing state of the fissure. The analysis reflects that the engineering behaviors of unsaturated expansive soil are objectively influenced by fissure.
文摘When stepped coal getting technology was applied to high seam mining working face, with field observations the following aspects of working face were analyzed based on the inherent conditions of extremely soft thick seam mined by Liangbei Mine, such as the brokenness and activity law of rock seam in the working face, the law of load-bearing of its supports, and the instability character of coal or rock in tip-to-face area. The following are the major laws. Pressure intensity of roof in high seam mining with extremely soft thick seam is stronger than one in slicing and sublevel-caving as a whole. But the greater crushing deformation of coal side makes pressure intensity of roof in the middle of working face be equivalent to one in sublevel-caving. In the middle of working face the roof brokenness has less dynamic load effect than roof brokenness in the two ends of working face. The brokenness instability of distinct pace of roof brings several load-bearings to supports. In condition of extremely soft thick seam, the ratio of resistance increment of supports in two ends of working face is obviously greater than that of supports in the middle. Most sloughing in coal side is triangular slop sloughing caused by shear slipping in high seam mining with extremely soft thick seam. Ultrahigh mining is the major reason for roof fall. Instability of coal or rock in tip-to-face area can be controlled effectively with the methods such as improving setting load of supports, mining along roof by reinforcing floor and protecting the immediate roof in time, and so on.