高温作用后混凝土抗拉强度的影响分析

对62组混凝土标准立方体试块进行劈裂抗拉强度试验,考察受火温度、冷却方式、养护龄期及静置时间对高温作用后混凝土劈裂断面形态和抗拉强度的影响规律,并针对不同情况建议了高温作用后混凝土抗拉强度的计算式.结果表明:受火温度对高温作用后混凝土劈裂断面的破坏形态和抗拉强度影响很大.当受火温度在300℃以内时,劈裂断面较为平整;随着受火温度的提高,劈裂断面越来越粗糙,当受火温度超过600℃时,劈裂断面主要经过硬化水泥浆,断面处粗骨料未发生破坏.喷水冷却后,高温作用后混凝土的抗拉强度总体上比自然冷却后的低.养护龄期越短,高温作用后混凝土的抗拉强度越低.高温作用后混凝土的抗拉强度总体上随静置时间呈先下降后上升的发展趋势,且当静置时间为28d时,混凝土的抗拉强度最低.

Anisotropic surface broken bond properties and wettability of calcite and fluorite crystals

Anisotropic surface broken bond densities of six different surfaces of calcite and three surfaces of fluorite were calculated. In terms of the calculated results, the commonly exposed surfaces of the two minerals were predicted and the relations between surface broken bonds densities and surface energies were analyzed. Then the anisotropic wettability of the commonly exposed surfaces was studied by means of contact angle measurement. The calculation results show that the （101^-4）, （213^-4）and （01 1^-8）surfaces for calcite and （111） for fluorite are the most commonly exposed surfaces and there is a good rectilinear relation between surface broken bond density and surface energy with correlation of determination （R^2） of 0.9613 and 0.9969, respectively. The anisotropic wettability of different surfaces after immersing in distilled water and sodium oleate solutions at different concentrations can be explained by anisotropic surface broken bond densities and active Ca sites densities, respectively.

Mineral cleavage nature and surface energy: Anisotropic surface broken bonds consideration

The population of surface broken bonds of some typical sulfide, oxide and salt-type minerals which may belong to cubic, tetragonal, hexagonal, or orthorhombic system, were calculated. In terms of the calculation results, the cleavage natures of these minerals were analyzed, and the relationship between surface broken bonds density and surface energy was also established. The results show that the surface broken bonds properties could be used to predict the cleavage nature of most of minerals, and the predicted cleavage planes agree well with those reported in previous literature. Moreover, this work explored a rule that, surface broken bonds density is directly related to surface energy with determination coefficient（R2） of over 0.8, indicating that the former is a dominant factor to determine the latter. Therefore, anisotropic surface broken bonds density can be used to predict the stability of mineral surface and the reactivity of surface atoms.

Effects of freeze-thaw cycles on fracture behavior of epoxy asphalt concrete

According to the winter temperature of Peking,the freeze-thaw（FT） condition in laboratory was determined.Seven groups of epoxy asphalt concrete（EAC） specimen were exposed to different FT cycles.The flexural modulus and fracture energy（G_F） of EAC exposed to different FT cycles were obtained through the 3-point bending test.Meanwhile,the plane strain fracture toughness（K_（IC）） of EAC was obtained through numerical simulation.The results show that the flexural modulus of the FT conditioned EAC samples decreases with the increase of FT cycles.The FT damage of flexural modulus is 60%after 30 FT cycles.Nevertheless,with the increase of FT cycles,the G_F and K_（IC） of EAC decrease first and then increase after 15 FT cycles.

Microstructure and property of rheocasting AZ91 slurry produced via ultrasonic vibration process

The microstructure and mechanical properties of rheocasting AZ91 magnesium alloy were investigated. The semisolid slurry of this alloy was prepared by ultrasonic vibration （USV） process and then shaped by high pressure diecasting （HPDC）. The results show that fine and spherical a-Mg particles were obtained by USV at the nucleation stage, which was mainly attributed to the cavitation and acoustic streaming induced by the USV. Extending USV treatment time increased the solid volume fraction and average particle size, the shape factors were nearly the same, about 0.7. Excellent semisolid slurry of AZ91 magnesium alloy could be obtained within 6 rain by USV near its liquidus temperature. The rheo-HPDC samples treated by USV for 6 min had the maximum ultimate tensile strength and elongation, which were 248 MPa and 7.4%, respectively. It was also found that the ductile fracture mode prevailed in the rheocasting AZ91 magnesium alloy.

Effect of heat treatment on microstructure and mechanical property of extruded 7090/SiC_p composite

The ultra high strength SiC particles （SiCp） reinforced Al-10%Zn-3.6%Mg-1.8%Cu-0.36%Zr-0.15% Ni composite was prepared by spray co-deposition. Microstructures of the extruded and different heat-treated bars were analyzed by transmission electron microscopy （TEM） and energy dispersive spectrometry （EDS）. Grain size of the composites prepared by two-stage solution is smaller than that by single-stage solution. After single-stage solution aging treatment, fine precipitates of both η and AlZnMgCu-rich phase can be found both intragranularly and intergranularly. While after the two-stage solution, an amorphous Si-Cu-Al-O （5 nm） layer appears at the interface. The addition of Ni and Zr modified the influence of the two-stage solution and inhibited the growth of the 7090/SiCp composite grain size. Heat treatments can significantly improve the fracture toughness of the composite. The fracture toughness first decreases then increases with the elongation of the aging time.

Static and dynamic mechanical behaviour of ECO-RPC

Ecological reactive powder concrete (ECO-RPC) with small sized and differentvolume fraction steel fibers was prepared by substitution of ultra-fine industrial waste powder for50% to 60% cement by weight and replacement of ground fine quartz sand with natural fine aggregate.The effect of steel fiber volume fraction and curing ages on the static mechanical behaviour ofECO-RPC was studied. Using the split Hopkinson pressure bar technique, the dynamic mechanicalbehaviour of ECO-RPC was investigated under different strain rates. The results show that the staticmechanical behaviour of ECO-RPC increases with the increase of steel fiber volume fraction andcuring ages. The type of ECO-RPC with the substitution of 25% ultra-fine slag, 25% ultra-fine flyash and 10% silica fume is better than the others with compressive strength, flexural strength, andfracture energy more than 200 MPa, 60 MPa and 30 kJ/m^2, respectively. ECO-RPC has excellent strainrate stiffening effects under dynamic load. Its peak stress, peak strain and the area understrain-stress curve increase with the increase of strain rate. Its fracture pattern changes frombrittleness to toughness under high strain rates.

副叶胎盘残留致产后大出血1例

患者女,27岁.于1996年5月21日在本地某医院足月顺产一女婴.胎盘完整,婴儿发育良好.2天后出院,在出院后第5天,因突然的大出血而再次入院.体检:T38.5℃、P130次/分、BP70/30mmHg,贫血貌,全身皮肤粘膜无出血点.B超显示宫腔胎盘残留.血象:Hb60g/L、WBC15×10~9/L、RBC2.9×10~12/L、BPC260×10~9/L.临床诊断:出血性休克.随即给予输血及抗休克治疗,待病情稳定后,行清宫术.最后将胎盘及宫内残留组织送检,大体可见两个胎盘均完整,只是大小有别,较大的约7×5cm,小的4×3cm.较大的胎盘边缘可见血管撕裂断面,残留胎盘由于被凝血包绕。

Microstructure and mechanical properties of TC4 titanium alloy K-TIG welded joints

The 12 mm-thick Ti−6Al−4V(TC4)titanium alloy plates were welded using keyhole tungsten inert gas(K-TIG)welding at various heat inputs.The microstructure,grain boundary(GB)characteristics and mechanical properties of the weld metal zone(WMZ)were analyzed.The test results show that the K-TIG welds are well formed,and no obvious defects are observed when the heat input is 2.30−2.62 kJ/mm.When the heat input gradually increases,αlaths increase in length,andα′phase and residualβphase are reduced.The electron backscatter diffraction(EBSD)test results indicate that the high-angle GB proportion in the WMZ increases with the increase of heat input.The tensile strength of the WMZ gradually decreases and the elongation of the WMZ increases when the heat input increases from 2.30 to 2.62 kJ/mm.The impact toughness of the WMZ increases as the heat input increases.

Mechanical properties and stress corrosion cracking behaviour of AZ31 magnesium alloy laser weldments

An AZ31 HP magnesium alloy was laser beam welded in autogenous mode with AZ61 filler using Nd-YAG laser system.Microstructural examination revealed that the laser beam weld metals obtained with or without filler material had an average grain size of about 12 μm.The microhardness and the tensile strength of the weldments were similar to those of the parent alloy.However,the stress corrosion cracking （SCC） behaviour of both the weldments assessed by slow strain rate tensile （SSRT） tests in ASTM D1384 solution was found to be slightly inferior to that of the parent alloy.It was observed that the stress corrosion cracks originated in the weld metal and propagated through the weld metal-HAZ regions in the autogenous weldment.On the other hand,in the weldment obtained with AZ61 filler material,the crack initiation and propagation was in the HAZ region.The localized damage of the magnesium hydroxide/oxide film formed on the surface of the specimens due to the exposure to the corrosive environment during the SSRT tests was found to be responsible for the SCC.

Compressive response and microstructural evolution of in-situ TiB_(2)particle-reinforced 7075 aluminum matrix composite

The hot forming behavior,failure mechanism,and microstructure evolution of in-situ TiB_(2)particle-reinforced 7075 aluminum matrix composite were investigated by isothermal compression test under different deformation conditions of deformation temperatures of 300−450℃ and strain rates of 0.001^(−1)s^(−1).The results demonstrate that the failure behavior of the composite exhibits both particle fracture and interface debonding at low temperature and high strain rate,and dimple rupture of the matrix at high temperature and low strain rate.Full dynamic recrystallization,which improves the composite formability,occurs under conditions of high temperature(450℃)and low strain rate(0.001 s^(−1));the grain size of the matrix after hot compression was significantly smaller than that of traditional 7075Al and ex-situ particle reinforced 7075Al matrix composite.Based on the flow stress curves,a constitutive model describing the relationship of the flow stress,true strain,strain rate and temperature was proposed.Furthermore,the processing maps based on both the dynamic material modeling(DMM)and modified DMM(MDMM)were established to analyze flow instability domain of the composite and optimize hot forming processing parameters.The optimum processing domain was determined at temperatures of 425−450℃ and strain rates of 0.001−0.01 s^(−1),in which the fine grain microstructure can be gained and particle crack and interface debonding can be avoided.

Fabrication of AA2024−TiO2 nanocomposites through stir casting process

Given the nonuse of TiO2 nanoparticles as the reinforcement of AA2024 alloy in fabricating composites by ex-situ casting methods,it was decided to process the AA2024−xTiO2(np)(x=0,0.5 and 1 vol.%)nanocomposites by employing the stir casting method.The structural properties of the produced samples were then investigated by optical microscopy and scanning electron microscopy;their mechanical properties were also addressed by hardness and tensile tests.The results showed that adding 1 vol.%TiO2 nanoparticles reduced the grain size and dendrite arm spacing by about 66%and 31%,respectively.Also,hardness,ultimate tensile strength,yield strength,and elongation of AA2024−1vol.%TiO2(np)composite were increased by about 25%,28%,4%and 163%,respectively,as compared to those of the monolithic component.The agglomerations of nanoparticles in the structure of nanocomposites were found to be a factor weakening the strength against the strengthening mechanisms.Some agglomerations of nanoparticles in the matrix were detected on the fractured surfaces of the tension test specimens.

Influence of Mg addition and T6 heat treatment on microstructure,mechanical and tribological properties of Al-12Si-3Cu based alloy

The aim of the present study was to investigate the influence of Mg addition and T6 heat treatment on microstructure,mechanical and tribological properties of the Al-Si-Cu-Mg alloys.In this context,a series of Al-12Si-3Cu-(0.5-2.5)Mg(wt.%)alloys were produced by permanent mould casting,and then subjected to T6 treatment.Their microstructure and mechanical properties were investigated using OM,XRD,SEM,EDS along with hardness,tension,compression and Charpy impact tests.Dry sliding friction and wear properties of the alloys were studied using a ball-on-disk type tester.It was observed that the microstructure of as-cast Al-12Si-3 Cu-Mg alloys consisted of a(Al),Si,O-CuAb,0-Mg_(2)Si,0-AbMg_(8)Cu(2)Si_(6) and π-AhMg_(3)FeSi_(6) phases.T6 heat treatment gave rise to nearly spherodization of eutectic Si particles,formation of finer 0-CuAH and 0-Mg_(2)Si precipitates and elimination of Chinese script morphology of 0-Mg_(2)Si phase.The addition of Mg up to 2.5 wt.%decreased the hardness,tensile and compressive strengths,tensile elongation and impact toughness of the as-cast and T6-treated alloys and increased their friction coefficient and volume loss.T6 treatment,on the other hand,led to a significant increase in mechanical properties and wear resistance of as-cast alloys.

Influences of pre-existing fracture on ground deformation induced by normal faulting in mixed ground conditions

Physical model tests have been conducted by various researchers to investigate fault rupture propagation and ground deformation induced by bedrock faulting. However, the effects of pre-existing fracture on ground deformation are not fully understood. In this work, six centrifuge tests are reported to investigate the influence of pre-existing fracture on ground deformation induced by normal faulting in sand, clay and nine-layered soil with interbedded sand and clay layers. Shear box tests were conducted to develop a filter paper technique, which was adopted in soil model preparation to simulate the effects of pre-existing fracture in centrifuge tests. Centrifuge test results show that ground deformation mechanism in clay, sand and nine-layered soil strata is classified as a stationary zone, a shearing zone and a rigid body zone. Inclination of the strain localization is governed by the dilatancy of soil material. Moreover, the pre-existing fracture provides a preferential path for ground deformation and results in a scarp at the ground surface in sand. On the contrary, fault ruptures are observed at the ground surface in clay and nine-layered soil strata.

Distribution of stress and strain between adjacent particles in particulate reinforced metal matrix composites

The distribution of stress and strain between adjacent particles in particulate reinforced metal matrix composites wasinvestigated using cohesive zone models. It is found that the strain of the composite is concentrated in the matrix, and there is aregion with higher strain along the loading path, which can promote the formation of a void near the particles pole. The stress andstrain in matrix near the particles gradually decrease with the increase of the distance between particles. And it is calculated that thereis a critical distance within which the stress and strain fields of the neighboring particles can influence with each other. This criticaldistance increases with the increase of particle size. It is also found that the angle between the tensile direction and the center line ofparticles plays an important role in the stress and strain distribution. The model with the angle of 0° has the greatest influence on thedistribution of stress and strain in the matrix, while the model with the angle of 45° has the least influence on the distribution of stressand strain in the matrix.

Effects of continuous casting mould fluxes on reducing longitudinal and star cracks on a slab surface

In the continuous casting production of medium carbon steel (whose mass fraction of carbon is 0.09 % to 0.16 %) and high strength low alloy steel (whose mass fraction of Mn is 0.90 % to 1.40 %), flecks occurring the most often are usually longitudinal and star cracks. In additional to the employment of a galvanized plate mould, two kinds of fluxes with special properties were studied and used to harmonize the conflicts between the function of heat transfer and lubrication. An industrial application revealed that the crystallizing temperature (Tc) and crystal ratio (R) of fluxes have a crucible effect on impeding the occurrence of above defects on a slab surface. In the case of slab section (180 to 240) mm(1000 to 1400) mm and casting speed Vc of (0.7 to 1.2) m/min, the optimized parameters of fluxes are Tc of (1170 to 1190) ℃, R of 80 % to 95 % for medium carbon steel, and Tc of (1100 to 1150) ℃, plus R of 40 % to 60 % for high strength low alloy steel.

Brazing of TiB_w/TC4 composite and Ti60 alloy using TiZrNiCu amorphous filler alloy

TiBw/TC4composite was brazed to Ti60alloy successfully using TiZrNiCu amorphous filler alloy,and the interfacialmicrostructures and mechanical properties were characterized by SEM,EDX,XRD and universal tensile testing machine.The typicalinterfacial microstructure was TiBw/TC4composite/β-Ti+TiB whiskers/(Ti,Zr)2(Ni,Cu)intermetallic layer/β-Ti/Ti60alloy whenbeing brazed at940°C for10min.The interfacial microstructure evolution was influenced strongly by the diffusion and reactionbetween molten fillers and the substrates.Increasing brazing temperature decreased the thickness of brittle(Ti,Zr)2(Ni,Cu)intermetallic layer,which disappeared finally when the brazing temperature exceeded1020°C.Fracture analyses indicated thatcracks were initialized in the brittle intermetallic layer when(Ti,Zr)2(Ni,Cu)phase existed in the brazing seam.The maximumaverage shear strength of joints reached368.6MPa when brazing was conducted at1020°C.Further increasing brazing temperatureto1060°C,the shear strength was decreased due to the formation of coarse lamellar(α+β)-Ti structure.

Failure analysis of air fan blades

The failure of all 12 blades of an air fan was investigated by metallurgical and mechanical experiments and an examina-tion of the fracture surface. The experimental results show that the cast aluminium-silicon alloy without any modification had a number of material defects, such as coarse grains, a loose structure, a large number of shrinkage holes, a long and thin bold-pin shaped silicon-phase, poor material strength and serious brittleness. In addition, installed on the spindle without elastic conjunction, blade No.10 vibrated and inevitably.spun off due to the large centrifugal force. Therefore, blade No.10 first cracked at the locking handle, then broke at the root, which caused all the other 11 blades to be broken by the crack of blade No.10.

Effect of cyclic heat treatment on microstructure and mechanical properties of 50CrV4 steel

An annealed 50 Cr V4 steel was subjected to cyclic heat treatment process that consists of repeated short-duration(200 s)held at 840 °C(above Ac3 temperature of 790 °C) and short-duration(100 s) held at 700 °C(below Ac1 temperature of 710 °C). The spheroidization ratio of cementite and the average size of particles increase with increasing the cyclic number of heat treatment. After5-cycle heat treatment, the spheroidization ratio of cementite is 100%, and the average size of the cementite particles is about0.53 μm. After cyclic heat treatment, the hardness, ultimate tensile strength and yield strength of the experimental steel gradually decrease with increasing cyclic number of heat treatment. The elongation of the as-received specimens is about 7.4%, the elongation of the 1-cycle specimen is 14.3%, and the elongation of 5-cycle specimen reaches a peak value of 22.5%, thereafter marginally decreases to 18.3% after 6-cycle heat treatment. Accordingly, the fractured surface initially exhibits the regions of wavy lamellar fracture. By increasing the cyclic number of heat treatment cycles, the regions of dimples consume the entire fractured surface gradually. Some large dimples can be found in the fracture surface of the specimen subjected to six heat treatment cycles.

Control effect of fracture on hard coal cracking in a fully mechanized longwall top coal caving face

Through theoretical analysis, simulation test and practice, the law of a fracture'sinfluence on hard top coal press cracking was studied. The study focused on the relationbetween fracture and coal strength, top coal caving ability and work face layout. Based onthe investigation of the fracture system, the control of press cracking was achieved bymatching working face to fracture orientation to improve top-coal caving ability and recovery. The matching principle was pointed out: The top-coal caving working face should beperpendicular to or obliquely cross the primary fracture at a large angle, and cross thesecondary fracture at a small angle. The rational match can increase the recovery ratio oftop-coal and avoid rib spalling. The application of control technology on hard top coalpress cracking was introduced at the Iongwall top-coal caving face.