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高效液相色谱法测定西黄片中人工牛黄的胆红素含量测定 被引量:8
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作者 吴红霞 付锦光 《当代医学》 2009年第4期124-125,共2页
目的建立HPLC法测定西黄片中人工牛黄的含量。方法色谱柱:C18柱(4.6×150mm);流动相:甲醇-三氯甲烷-1%磷酸溶液(84:9:7)检测波长为453nm;柱温为25℃;流速为1.0ml/min,进样量10μl。结果在3.228~16.14μg/ml范围内与峰面积呈良好的... 目的建立HPLC法测定西黄片中人工牛黄的含量。方法色谱柱:C18柱(4.6×150mm);流动相:甲醇-三氯甲烷-1%磷酸溶液(84:9:7)检测波长为453nm;柱温为25℃;流速为1.0ml/min,进样量10μl。结果在3.228~16.14μg/ml范围内与峰面积呈良好的线性关系,r=0.9998;平均回收率为98.59%,RSD1.3%(n=6)。结论本法简便快速、定量准确,可用于西黄片中人工牛黄的含量测定。 展开更多
关键词 HPLC法 西黄片 人工牛黄 含量测定
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Substrate Type Affects Growth, Yield and Mineral Composition of Cucumber and Zucchini Squash
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作者 Mariateresa Cardarelli Youssef Rouphae +3 位作者 Salem Darwich Elvira Rea Antonio Fiorillo Giuseppe Colla 《Journal of Life Sciences》 2012年第7期766-770,共5页
The expansion of hydroponics in many countries of the world in the last few decades may be ascribed to the ability of soilless growing systems to avoid various problems arising from the use of the soil. Cucumber (Cuc... The expansion of hydroponics in many countries of the world in the last few decades may be ascribed to the ability of soilless growing systems to avoid various problems arising from the use of the soil. Cucumber (Cucurnis sativus L.) and zucchini (Cucurbita pepo L.) plants were grown in closed-soilless culture under unheated-greenhouse conditions at the experimental farm of University of Tuscia, Central Italy to evaluate the effects of four substrates (rockwool, pumice, perlite, and cocofiber) on growth, yield and plant mineral composition. For both cultures, plants grown in cocofiber, perlite and pumice yielded more than those grown in rockwool. The better temperature regime in cocofiber, perlite and pumice was due to the greater thermal inertia compared to rockwool slabs. Thc concentration of N in zucchini and cucumber leaves was significantly higher in cocofiber, perlite and pumice in comparison to the rockwool treatment. The concentration of K was significantly affected by the substrate only for the zucchini squash with the highest value recorded on the organic substrate (cocofiber), whereas the Ca concentration was significantly influenced by the growing media only for cucumber with the highest value observed on pumice. Finally, the lowest Mg concentration in leaf tissue was observed on plants grown with the rockwool substrate for both zucchini squash and cucumber. We can conclude that cocofiber, perlite and pumice are suitable for zucchini and cucumber production in closed soilless system, whereas the use of rockwool is more suitable for crops grown under heated greenhouse conditions. 展开更多
关键词 Substrate type YIELD mineral composition CUCUMBER zucchini squash.
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