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复方解热凝胶溶出度方法研究 被引量:3
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作者 白学敏 张雪萍 孙建枢 《医药导报》 CAS 2004年第11期853-854,共2页
目的 :建立复方解热凝胶的溶出度标准。方法 :采用《中华人民共和国药典》(2 0 0 0年版 )二部附录X溶出度测定第二法 ,以 0 .0 62mol·L 1 盐酸为溶剂 ,测定复方解热凝胶溶出度。结果 :复方解热凝胶溶出度均一性好 ,累积溶出百分率... 目的 :建立复方解热凝胶的溶出度标准。方法 :采用《中华人民共和国药典》(2 0 0 0年版 )二部附录X溶出度测定第二法 ,以 0 .0 62mol·L 1 盐酸为溶剂 ,测定复方解热凝胶溶出度。结果 :复方解热凝胶溶出度均一性好 ,累积溶出百分率在 3 0min内达 89.8%;经后差检验 ,C =0 .0 0 0 98,P =1。结论 :该剂型溶出度标准 3 0min内确定为标示量的 85 .0 %。 展开更多
关键词 解热凝胶 复方 溶出度 后差检验
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经典恒温法考察复方解热凝胶的稳定性 被引量:1
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作者 孙建枢 张雪萍 白学敏 《中国药业》 CAS 2003年第5期29-30,共2页
目的:研究半固体制剂复方解热凝胶的稳定性。方法:用差示分光光度法于波长266nm处测对乙酰氨基酚的含量,通过经典恒温法对复方解热凝胶作稳定性试验,并与留样观察作对照。结果:经典恒温法测得的复方解热凝胶的室温贮存期为2年,与留样观... 目的:研究半固体制剂复方解热凝胶的稳定性。方法:用差示分光光度法于波长266nm处测对乙酰氨基酚的含量,通过经典恒温法对复方解热凝胶作稳定性试验,并与留样观察作对照。结果:经典恒温法测得的复方解热凝胶的室温贮存期为2年,与留样观察结果相符。结论:半固体制剂复方解热凝胶可以通过经典恒温法预测有效期。 展开更多
关键词 经典恒温法 考察 复方解热凝胶 稳定性
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络合萃取-分光光度法测定复方解热凝胶中马来酸氯苯那敏含量 被引量:2
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作者 张雪萍 《沈阳药科大学学报》 CAS CSCD 2000年第1期55-57,共3页
创立了测定复方解热凝胶中马来酸氯苯那敏含量的络合萃取分光光度法.实验表明,马来酸氯苯那敏在8 ~18 μg/mL范围内呈现良好的线性关系.A= 0-043 8 C- 0-016 6 ,r= 0-999 7( n = 5),RSD... 创立了测定复方解热凝胶中马来酸氯苯那敏含量的络合萃取分光光度法.实验表明,马来酸氯苯那敏在8 ~18 μg/mL范围内呈现良好的线性关系.A= 0-043 8 C- 0-016 6 ,r= 0-999 7( n = 5),RSD 为0-74 % ,回收率99-9 % . 展开更多
关键词 解热凝胶 马来酸氯苯那敏 锌试剂 分光光度法
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复方解热凝胶的稳定性试验
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作者 孙建枢 张雪萍 白学敏 《黑龙江医药》 CAS 2002年第3期184-185,共2页
目的:预测复方解热凝胶的有效期。方法:采用经典恒温加速试验法,选用67,72,77,82℃时,测量本品中对乙酰基酚的相对含量。结果:在此温度下,对乙酰基酚相对含量变化符合一级动力学过程。结论:复方解热凝胶的有效期为2年。
关键词 解热 稳定性试验 复方解热凝胶 对乙酰基酚
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Crystallization Behavior and Properties of B-Doped ZnO Thin Films Prepared by Sol-Gel Method with Different Pyrolysis Temperatures
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作者 文斌 刘超前 +6 位作者 王楠 王华林 刘世民 姜薇薇 丁万昱 费维栋 柴卫平 《Chinese Journal of Chemical Physics》 SCIE CAS CSCD 2016年第2期229-233,I0002,共6页
Boron-doped zinc oxide transparent (BZO) films were prepared by sol-gel method. The effect of pyrolysis temperature on the crystallization behavior and properties was systematically investigated. XRD patterns reveal... Boron-doped zinc oxide transparent (BZO) films were prepared by sol-gel method. The effect of pyrolysis temperature on the crystallization behavior and properties was systematically investigated. XRD patterns revealed that the BZO films had wurtzite structure with a preferential growth orientation along the c-axis. With the increase of pyrolysis temperature, the particle size and surface roughness of the BZO films increased, suggesting that pyrolysis temperature is the critical factor for determining the crystallization behavior of the BZO films. Moreover, the carrier concentration and the carrier mobility increased with increasing the pyrolysis temperature, and the mean transmittance for every film is over 90% in the visible range. 展开更多
关键词 Transparent conduction oxide Thin film Boron-doped ZnO Pyrolysis tem-perature SOLGEL
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Isolation and Characterization of a Thermophilic Oil-Degrading Bacterial Consortium 被引量:2
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作者 Gu Guizhou Li Zheng +1 位作者 Zhao Dongfeng Zhao Chaocheng 《China Petroleum Processing & Petrochemical Technology》 SCIE CAS 2013年第2期82-90,共9页
In this study, a thermophilic oil-degrading bacterial consortium KO8-2 growing within the temperature range of 45--65℃ (with 55℃ being the optimum temperature) was isolated from oil-contaminated soil of Karamay in... In this study, a thermophilic oil-degrading bacterial consortium KO8-2 growing within the temperature range of 45--65℃ (with 55℃ being the optimum temperature) was isolated from oil-contaminated soil of Karamay in Xinjiang, China. Denaturing gradient gel electrophoresis (DGGE) showed that there were nine strains included in KO8-2, which originated from the genera of Bacillus, Geobacillus and Clostridium. They all belonged to thermophilic bacteria, and had been previously proved as degraders of at least one petroleum fraction. The crude oil degraded by KO8-2 was analyzed by infrared spectrophotometry, hydrocarbon group type analysis and gas chromatography. The results indicated that the bacterial consortium KO8-2 was able to utilize 64.33% of saturates, 27.06% of aromatics, 13.24% of resins and the oil removal efficiency reached up to 58.73% at 55 ~C when the oil concentration was 10 g/L. Detailed analysis showed that KO8-2 was able to utilize the hydrocarbon components before C19, and the n-alkanes ranging from C20--C33 were signifi- cantly degraded. The ratios of nC17/Pr and nC18/Ph were 3.12 and 3.87, respectively, before degradation, whereas after degradation the ratios reduced to 0.21 and 0.38, respectively. Compared with the control sample, the oil removal efficiency in KO8-2 composting reactor reached 50.12% after a degradation duration of 60 days. 展开更多
关键词 thermophilic bacteria bacterial consortium oil-contaminated soil BIODEGRADATION DGGE
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