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气相色谱法对乙醛多聚体的质量全分析 被引量:2
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作者 沈新安 《辽宁化工》 CAS 2004年第7期426-428,共3页
采用气相色谱法 ,结合校正因子 ,研究了四聚乙醛、三聚乙醛、乙醛和烟酰胺的测定条件。该方法科学 ,操作易行、快速 ,准确度达到工业分析的要求。
关键词 气相色谱 四聚乙醛 校正因子 质量全分析
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气相色谱法对乙醛多聚体的质量全分析
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作者 沈新安 《化工文摘》 2004年第4期59-60,共2页
用气相色谱法,结合校正因子,研究了四聚乙醛、三聚乙醛、乙醛和烟酰胺的测定条件。方法科学,操作易行、快速,准确度达到工业分析的要求。
关键词 气相色谱 乙醛多聚体 四聚乙醛 校正因子 质量全分析
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盐酸普鲁卡因原料药质量标准全分析的混合式实验教学设计 被引量:1
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作者 原媛 上官璟芳 +2 位作者 刘宇飞 高一乔 孙祥德 《中国继续医学教育》 2022年第15期12-16,共5页
在“互联网+”背景下,信息技术与传统教育手段优劣互补、相辅相成,越来越多地应用于教学中。文章以盐酸普鲁卡因的分析为例,从案例设计、教学设计和考核评价等方面设计了原料药质量标准全分析的线上线下混合式实验教学方案。原料药质量... 在“互联网+”背景下,信息技术与传统教育手段优劣互补、相辅相成,越来越多地应用于教学中。文章以盐酸普鲁卡因的分析为例,从案例设计、教学设计和考核评价等方面设计了原料药质量标准全分析的线上线下混合式实验教学方案。原料药质量标准中的检验项目所涉及的知识点和操作技术信息量大而有代表性,全分析又体现了药检工作的系统性,教学方法结合了线下课堂教学和新兴互联网学习的优势,有利于激发学生的学习热情,课前学习、课上讨论、课后总结各环节均体现了以学生为中心的理念,可作为其他原料药质量标准全分析实验混合式教学设计的参考和模板,也是药物分析实验教学改革的有益探索。 展开更多
关键词 线上线下 混合式教学 药物分析 盐酸普鲁卡因 原料药 质量标准分析 实验教学 教育
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Quality prediction of batch process using the global-local discriminant analysis based Gaussian process regression model
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作者 卢春红 顾晓峰 《Journal of Southeast University(English Edition)》 EI CAS 2015年第1期80-86,共7页
The conventional single model strategy may be ill- suited due to the multiplicity of operation phases and system uncertainty. A novel global-local discriminant analysis (GLDA) based Gaussian process regression (GPR... The conventional single model strategy may be ill- suited due to the multiplicity of operation phases and system uncertainty. A novel global-local discriminant analysis (GLDA) based Gaussian process regression (GPR) approach is developed for the quality prediction of nonlinear and multiphase batch processes. After the collected data is preprocessed through batchwise unfolding, the hidden Markov model (HMM) is applied to identify different operation phases. A GLDA algorithm is also presented to extract the appropriate process variables highly correlated with the quality variables, decreasing the complexity of modeling. Besides, the multiple local GPR models are built in the reduced- dimensional space for all the identified operation phases. Furthermore, the HMM-based state estimation is used to classify each measurement sample of a test batch into a corresponding phase with the maximal likelihood estimation. Therefore, the local GPR model with respect to specific phase is selected for online prediction. The effectiveness of the proposed prediction approach is demonstrated through the multiphase penicillin fermentation process. The comparison results show that the proposed GLDA-GPR approach is superior to the regular GPR model and the GPR based on HMM (HMM-GPR) model. 展开更多
关键词 quality prediction global-local discriminantanalysis Gaussian process regression hidden Markov model soft sensor
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Water Analysis for Heavy Metals Content in Selected Boreholes in Port Harcourt Metropolis (A Case Study during 2010-2011) 被引量:1
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作者 Kalagbor Ihesinachi Appolonia Mgbodom-Okah Chidinma Juliet 《Journal of Environmental Science and Engineering(A)》 2013年第7期418-426,共9页
Underground water (Borehole) has been the main alternative source of drinking water for most communities in my country. Previous studies have revealed high levels of contamination. The origin of which can be attribu... Underground water (Borehole) has been the main alternative source of drinking water for most communities in my country. Previous studies have revealed high levels of contamination. The origin of which can be attributed to geochemical processes, combustion of fossil fuels, mining and anthropogenic activities. Most borehole water and well water in local communities of Nigeria are not safe for drinking due to heavy industrial and environmental pollution. This study was undertaken to assess the quality in some selected boreholes in the Port Harcourt metropolis for a period of two years. Borehole water samples were randomly collected from thirteen boreholes in a local community in plastic bottles (100 mL) in the months of September for the years of study (2010 & 2011). Four out of the seven heavy metals analyzed were found to be present in the first year of study. These were Fe, Cu, Mn and Zn. In the second year of study, Pb, Cr, Fe and Co were not detected in all of the samples except Cu and Fe which were present in only two samples. Mn and Zn were found to be present in all of the samples for both years of study. 展开更多
关键词 GROUNDWATER BOREHOLE geochemical processes.
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