Concrete in reinforced concrete structure (RC) is generally under significant compressive stress load. To guarantee required quality and ductility, various tests have to be conducted to measure the concrete’s compres...Concrete in reinforced concrete structure (RC) is generally under significant compressive stress load. To guarantee required quality and ductility, various tests have to be conducted to measure the concrete’s compressive strength based on ACI (American Concrete Institute) code. Investigations of recent devastating collapses of structures around the world showed that some of the collapses directly resulted from the poor quality of the concrete. The lesson learned from these tragedies is that guaranteeing high quality of concrete is one of the most important factors ensuring the safety of the reinforced concrete structure. In order to ensure high quality of concrete, a new method for analyzing and evaluating the concrete production process is called for. In this paper, the indices of fit and stable degree are proposed as basis to evaluate the fitness and stability of concrete’s compressive strength. These two indices are combined to define and evaluate the quality index of the compressive strength of concrete. Prin-ciples of statistics are used to derive the best estimators of these indices. Based on the outcome of the study, a concrete compres-sive strength quality control chart is proposed as a tool to help the evaluation process. Finally, a new evaluation procedure to assess the quality control capability of the individual concrete manufacturer is also proposed.展开更多
Sequential chemical extraction procedure has been widely used to partition particulate trace metals into various fractions and to describe the distribution and the statue of trace metals in geo environment. One sequen...Sequential chemical extraction procedure has been widely used to partition particulate trace metals into various fractions and to describe the distribution and the statue of trace metals in geo environment. One sequential chemical extraction procedure was employed here to partition various fractions of Mn in soils. The experiment was designed with quality controlling concept in order to show sampling and analytical error. Experimental results obtained on duplicate analysis of all soil samples demonstrated that the precision was less than 10%(at 95%confidence level). The accuracy was estimated by comparing the accepted total concentration of Mn in standard reference materials (SRMs) with the measured sum of the individual fractions. The recovery of Mn from SRM1 and SRM2 was 94.1%and 98.4%, respectively. The detection limit, accuracy and precision of the sequential chemical extraction procedure were discussed in detailed. All the results suggest that the trueness of the analytical method is satisfactory.展开更多
As direct measure of learners' communicative language ability, performance assessment (typically writing and speaking assessment) claims construct validity and a strong power for predictive utility of test scores....As direct measure of learners' communicative language ability, performance assessment (typically writing and speaking assessment) claims construct validity and a strong power for predictive utility of test scores. However, it is also of common concern that the subjectivity of rating process and the potential unfairness for test takers who encounter different writing prompts and speaking tasks would constitute threats to reliability and validity of test scores, especially in those large-scale and high-stakes tests. Therefore, appropriate means for quality control of subjective scoring should be held essential in test administration and validation. Based upon raw scores from one administration of speaking test in PETS Band3 held in Hangzhou, the present study investigates and models possible sources of score variability within the framework of Many-Facet Rasch Model (MFRM). MFRM conceptualizes the possibility of a examinee being awarded a certain score as a function of several facets — examinee ability, rater severity, domain difficulty and step difficulty between the adjacent score categories and provides estimates of the extent to which the examinee's test score is influenced by those facets. Model construction and data analysis was carried out in FACETS Version 3.58, computer program for conducting MFRM analysis. The results demonstrate statistically significant differences within each facet. Despite the generally acceptable rater consistency across examinees and rating domains, fit statistics indicate some unexpected rating patterns in certain raters such as inconsistency and central tendency, to be avoided through future rater training. Fair scores for each examinee are also provided, minimizing the variability due to facets other than examinees' ability. MFRM manifests itself as effective in detecting whether each test method facet functions as intended in performance assessment and providing useful feedback for quality control of subjective scoring.展开更多
In this paper,an HPLC-DAD-ELSD method was developed to determine main 20 components of Ginkgo biloba L.leaves from different ages and sources,including six flavonol glycosides,five terpene lactones and nine organic ac...In this paper,an HPLC-DAD-ELSD method was developed to determine main 20 components of Ginkgo biloba L.leaves from different ages and sources,including six flavonol glycosides,five terpene lactones and nine organic acids.Using statistics method and establishing relevant mathematics models,the measured data has proceeded correlation analysis,principal component analysis,and regression statistics and the results showed generality and specific characteristics.We defined p-hydroxybenzoic acid,catechinic,KRcG and ginkgolide A as characteristic indexes representing commonness and speciality of Ginkgo biloba L.leaf.The four characteristic indexes can reflect the quality of Ginkgo biloba L.leaf,and the intermal relations between them are significant.The contents of other compounds could define the quantity relation with characteristic markers.It simplified the approach of quality control,and provided a basis for quality control of Ginkgo biloba L.展开更多
基金Project (No. NSC92-2213-e-167-001) supported by the National Science Council, Taiwan, China
文摘Concrete in reinforced concrete structure (RC) is generally under significant compressive stress load. To guarantee required quality and ductility, various tests have to be conducted to measure the concrete’s compressive strength based on ACI (American Concrete Institute) code. Investigations of recent devastating collapses of structures around the world showed that some of the collapses directly resulted from the poor quality of the concrete. The lesson learned from these tragedies is that guaranteeing high quality of concrete is one of the most important factors ensuring the safety of the reinforced concrete structure. In order to ensure high quality of concrete, a new method for analyzing and evaluating the concrete production process is called for. In this paper, the indices of fit and stable degree are proposed as basis to evaluate the fitness and stability of concrete’s compressive strength. These two indices are combined to define and evaluate the quality index of the compressive strength of concrete. Prin-ciples of statistics are used to derive the best estimators of these indices. Based on the outcome of the study, a concrete compres-sive strength quality control chart is proposed as a tool to help the evaluation process. Finally, a new evaluation procedure to assess the quality control capability of the individual concrete manufacturer is also proposed.
文摘Sequential chemical extraction procedure has been widely used to partition particulate trace metals into various fractions and to describe the distribution and the statue of trace metals in geo environment. One sequential chemical extraction procedure was employed here to partition various fractions of Mn in soils. The experiment was designed with quality controlling concept in order to show sampling and analytical error. Experimental results obtained on duplicate analysis of all soil samples demonstrated that the precision was less than 10%(at 95%confidence level). The accuracy was estimated by comparing the accepted total concentration of Mn in standard reference materials (SRMs) with the measured sum of the individual fractions. The recovery of Mn from SRM1 and SRM2 was 94.1%and 98.4%, respectively. The detection limit, accuracy and precision of the sequential chemical extraction procedure were discussed in detailed. All the results suggest that the trueness of the analytical method is satisfactory.
基金Educational Measurement Research Project sponsored by 2006 National Education Science Research Plan of National Education Examinations Authority~~
文摘As direct measure of learners' communicative language ability, performance assessment (typically writing and speaking assessment) claims construct validity and a strong power for predictive utility of test scores. However, it is also of common concern that the subjectivity of rating process and the potential unfairness for test takers who encounter different writing prompts and speaking tasks would constitute threats to reliability and validity of test scores, especially in those large-scale and high-stakes tests. Therefore, appropriate means for quality control of subjective scoring should be held essential in test administration and validation. Based upon raw scores from one administration of speaking test in PETS Band3 held in Hangzhou, the present study investigates and models possible sources of score variability within the framework of Many-Facet Rasch Model (MFRM). MFRM conceptualizes the possibility of a examinee being awarded a certain score as a function of several facets — examinee ability, rater severity, domain difficulty and step difficulty between the adjacent score categories and provides estimates of the extent to which the examinee's test score is influenced by those facets. Model construction and data analysis was carried out in FACETS Version 3.58, computer program for conducting MFRM analysis. The results demonstrate statistically significant differences within each facet. Despite the generally acceptable rater consistency across examinees and rating domains, fit statistics indicate some unexpected rating patterns in certain raters such as inconsistency and central tendency, to be avoided through future rater training. Fair scores for each examinee are also provided, minimizing the variability due to facets other than examinees' ability. MFRM manifests itself as effective in detecting whether each test method facet functions as intended in performance assessment and providing useful feedback for quality control of subjective scoring.
基金National Administration of Traditional Chinese Medicine Standardization Project(Grant No.ZYBZH-C-HEB-16)
文摘In this paper,an HPLC-DAD-ELSD method was developed to determine main 20 components of Ginkgo biloba L.leaves from different ages and sources,including six flavonol glycosides,five terpene lactones and nine organic acids.Using statistics method and establishing relevant mathematics models,the measured data has proceeded correlation analysis,principal component analysis,and regression statistics and the results showed generality and specific characteristics.We defined p-hydroxybenzoic acid,catechinic,KRcG and ginkgolide A as characteristic indexes representing commonness and speciality of Ginkgo biloba L.leaf.The four characteristic indexes can reflect the quality of Ginkgo biloba L.leaf,and the intermal relations between them are significant.The contents of other compounds could define the quantity relation with characteristic markers.It simplified the approach of quality control,and provided a basis for quality control of Ginkgo biloba L.
